微束分析测试技术十年(2011~2020)进展与展望     

陈意  胡兆初  贾丽辉  李金华  李秋立  李晓光  李展平  龙涛  唐旭  王建  夏小平  杨蔚  原江燕  张迪  李献华 《矿物岩石地球化学通报》2021,40(1):前插2-前插3,1-35

现代地球科学研究的重大突破在很大程度上取决于观测和分析技术的创新。新世纪以来,我国地球科学领域引进了一批高性能新型微束分析仪器设备,建立了一批高规格的实验室。本文回顾了近十年来微束分析技术与方法的主要进展及其在地球科学研究中的应用实例,包括电子探针、扫描电镜、透射电镜、大型离子探针、纳米离子探针、飞行时间二次离子质谱、激光剥蚀等离子体质谱、激光诱导原子探针、原子探针技术、显微红外光谱、同步辐射等,这些分析技术的进步和广泛应用极大地提高了我们对地球和行星演化历史及许多地质过程的理解。今后,应加快微束分析的新技术、新方法和新标准的开发,特别是高水平人才队伍建设,提高创新能力并在国际学术舞台上发挥重要作用。  相似文献   

ASTER mapping of gypsum deposits of Thumrait region of southern Oman     

Sankaran Rajendran  Sobhi Nasir 《Resource Geology》2021,71(1):41-62

This study demonstrates the use of ASTER data for the mapping of gypsum deposits and associated geological formations that occurred in the Thumrait region of southern Oman. The measurement of spectra over samples of gypsum in the 1,300–2,500 nm wavelength using a PIMA spectrometer showed the presence of distinct absorptions at 1400–1600, 1750, 1940, 2,100, and 2,400 nm characteristics to O? H stretching, H₂O combinations, and S? O bending overtones and stretching, respectively. Studying the unique spectral absorption characters of gypsum samples, we developed a false color composite (FCC) and an image by decorrelation stretch using the spectral bands 7, 3, and 2 of ASTER. The results FCC showed the regions of gypsum occurrences, and the decorrelated image discriminated the gypsum occurrences from other geological formations of the area. The study of surface mineralogy of the region using the VNIR‐SWIR bands by the spectral angle mapper method showed the presence of sulfate, carbonate, and clay minerals of the geological formations in the study area. We compared the results of ASTER with the results obtained using spectral bands 12, 8, and 4 of Sentinel‐2A processed by the same methods. The study showed that the spectral bands of ASTER can be used for mapping the gypsum and associated geological formations.  相似文献   

Rapid U‐Pb Geochronology by Laser Ablation Multi‐Collector ICP‐MS     

Kurt E. Sundell  George E. Gehrels  Mark E. Pecha 《Geostandards and Geoanalytical Research》2021,45(1):37-57

Detrital zircon (DZ) U‐Pb laser ablation‐inductively coupled plasma‐mass spectrometry (LA‐ICP‐MS) has revolutionised the way geologists approach many Earth science questions. Although recent research has focused on rapid sample throughput, acquisition rates are limited to 100–300 analyses h^?1. We present a method to acquire zircon U‐Pb dates at rates of 120, 300, 600 and 1200 analyses h^?1 (30, 12, 6 and 3 s per analysis) by multi‐collector LA‐ICP‐MS. We demonstrate the efficacy of this method by analysing twelve zircon reference materials with dates from ~ 3465 to ~ 28 Ma. Mean offset from high‐precision dates increases with faster rates from 0.9% to 1.1%; mean random 1s uncertainty increases from 0.6% to 1.3%. We tested this new method on a sandstone sample previously characterised by large‐n DZ geochronology. Quantitative comparison shows increased correspondence among age distributions comprising > 300 dates. This new method holds promise for DZ geochronology because (a) it requires no major changes to hardware, but rather modifications to software; (b) it yields robust age distributions well‐suited for quantitative analysis and maximum depositional age calculations; (c) there is only a minor sacrifice of accuracy and measurement uncertainty; and (d) there is less burden to researchers in terms of time investment and analytical cost.  相似文献   

基于三维激光扫描技术的岩质边坡泥化夹层空间分布和几何形态     

刘文连  张家明  王志强  徐则民 《吉林大学学报(地球科学版)》2021,51(4):1139-1151

为了定量研究泥化夹层的空间分布和几何形态,以云南省玉溪市生活垃圾焚烧发电厂高边坡局部开挖剖面为对象,利用徕卡ScanStation C10三维激光扫描仪和瑞典ROMER RA-7520-2六轴关节臂三维测量仪进行扫描,得到了开挖剖面和泥化夹层的原始点云数据;然后采用Cyclone和Geomagic Wrap软件对点云数据进行一系列处理,分析了泥化夹层的三维空间分布、层面产状、间距、层面粗糙度和几何形态。结果表明：大部分泥化夹层横向分布于整个扫描剖面,少数呈局部分布;泥化夹层的平均倾向为196.41°±5.51°,平均倾角为22.27°±2.23°,间距在3.7~49.1 cm之间,平均值为（20.4±12.0）cm;不同层位及同一层位不同横向位置的泥化夹层厚度都不等,最厚约20 mm,最薄小于1 mm;泥化夹层顶面局部典型区域的平面拟合偏差在-22.4~32.5 mm之间,沿夹层倾向的粗糙度系数在5.67~16.77之间,平均值为10.11±3.25;泥化夹层的表面积与体积之比在5.14~5.86 cm^-1之间。运用三维激光扫描技术研究泥化夹层的空间分布和几何形态是可行的。玉溪市生活垃圾焚烧发电厂高边坡的泥化夹层具有宏观整体上相对平直、相互近似平行、非等距分布、间距小、层数多、厚度薄,细观上顶面粗糙底面相对光滑、三维形态复杂的特点。  相似文献   

激光实时干涉计量技术和雷达差分干涉技术测量形变的对比研究及其意义          下载免费PDF全文

毛先进  许昭永  钱家栋  胡毅力  杨润海  王彬 《地震学报》2006,28(3):313-322

分别叙述了激光干涉技术和雷达差分干涉技术的原理及应用. 采用激光实时干涉计量技术实验室观测试样在加压过程中的形变,研究不同破裂孕育区所表现的不同应变异常场特征. 采用雷达差分干涉技术可以测量地形及地表形变,并且有西藏玛尼、张北——尚义等地震前后的形变测量结果. 指出激光实时干涉计量技术与雷达差分干涉技术相似,都是以条纹变化图研究形变异常场特征. 因此, 对雷达差分干涉技术测量的孕震过程中的形变场,特别是临近大震发生前的形变场特征进行观测和以激光干涉技术进行实验及对比研究均将很有意义.   相似文献   

TROS-Ⅰ型流动人卫激光测距仪光学系统设计     

李翠霞  李家明  蔡庆福 《大地测量与地球动力学》2006,26(1):124-127

介绍了车载流动型人卫激光测距仪光学系统(包括激光发射系统、接收系统及微光电视监视系统)的设计思想和方法,着重叙述了光学系统的结构设计、关键部件几何尺寸的确定及重要元器件的选取。设计基于流动型仪器应满足的防振、体积小、调校方便、抗环境干扰能力强等特点。多年的实测证明,这种光学系统不仅能满足流动型人卫激光测距仪总体设计要求,而且经济实用。  相似文献   

四渡河特大桥GPS控制网的布设及成果分析     

苏勤龙  赵正刚  程礼恒 《地理空间信息》2006,4(1):67-68

介绍四渡河特大桥GPS控制网,采用一种新颖的平差计算方式,解决了与周边控制网的接边精度问题,解决了大山区大高差对GPS施工控制网的精度影响。实际验证了国产单频静态GPS接受机,也能进行高精度的施工控制测量。  相似文献   

桂东南荔枝生长营养元素农业地球化学研究   总被引：6，自引：0，他引：6  

叶荣  李蔚萍 《地学前缘》2006,13(1):119-127

桂东南是中国重要的荔枝产区,以梧州地区为例,重点对沙头和古凤两处荔枝种植园进行了生态地球化学调查,采集了荔枝园施肥圈内、外土壤,出露的代表性基岩,以及荔枝叶、青果和熟果样品,实测了大量和微量矿质元素、稀土元素,以及土壤营养元素有效态的含量。通过计算荔枝对土壤营养元素的吸收率及荔枝生长与结果期对营养元素的需求,查明本区荔枝生长的特征营养元素为Ca、K、Mg、Mn、P、Zn、Cu、B、Fe和REE。荔枝结果期的特需营养元素为P、Mg、Mo、Cu、Zn、Ko荔枝结果早和晚期特需元素分别为Ca、Si、B和Cu、Fe、K。在岩石-土壤-荔枝株生态循环系统中,本区营养元素在土壤中保持一定的积累,提供荔枝生长的需求,因此为荔枝宜种区;但全区土壤B缺乏,Zn、Mo局部不足。Ca、K、Zn在两区岩石土壤中分布不同,可能是造成沙头荔枝比古凤荔枝迟熟的主要农业地球化学因素。研究区有害元素Pb、Cd在土壤中积累是值得关注的土壤环境问题。  相似文献   

Absorption of Arsenite on Several Iron （Hydro-）Oxides and Impact from Pre-processing Methods     

YE Ying JI Shanshan WU Daidai LI Jun ZHANG Weirui 《《地质学报》英文版》2006,80(2):200-205

The absorption reactions of arsenite on Fe （hydro-）oxides are studied. The three absorbent types are Fe（OH）3 gel and two Fe （hydro-）oxides, in which the Fe（OH）3 gel was dried in a microwave oven under vacuum at 80℃. It is found that pH changes from 9.71 to 10.36 in 6 minutes after the Fe （OH）3 gel was mixed with NaAsO2 solution, as the arsenite replaces the OH- in goethite and Fe（OH）3. At the 40th minute after the start of the reaction, pH decreases, which is most probably because that the monodentate surface complex of absorbed arsenite has changed into mononuclear-bidentate complex and released proton. The decline in pH values indicates not the end of the absorption but a change in the reaction type. Temperature and dissolved gas has little effect on these two types of reactions. The total absorption of arsenite increases after the absorbent is irradiated with ultrasound, which also lead to difficulty in separating the solids from solution. The absorption capacity for arsenite of Fe（OH）3 gel dried in a microwave oven under vacuum is 53.18% and 17.22% respectively better than that of Fe （OH）3 gel and gel dried at 80℃. The possible reasons are that the water molecules in the gel vibrates with high frequency under the effect of microwave irradiation, thereby producing higher porosity and improved surface activity.  相似文献   

电镀金刚石钻头镀前超声清洗机理及工艺研究   总被引：4，自引：0，他引：4  

刘晓东  霍宇翔  李子章 《地质与勘探》2006,42(1):89-92

电镀金刚石钻头镀前清洗是钻头生产的关键制造工艺.超声清洗作为一种精清洗技术,在不少领域获得了成功.本文阐述了超声波对金刚石钻头镀前清洗工艺的适应性,分析了电镀金刚石钻头中的主要清洗对象及超声清洗机理,对超声清洗中的各项工艺参数及工艺流程进行了研究,说明了超声清洗的经济适用性及可操作性.  相似文献