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21.
Lutz Nasdala Wolfgang Hofmeister Nicholas Norberg James M. Martinson Fernando Corfu Wolfgang Dörr Sandra L. Kamo Allen K. Kennedy Andreas Kronz Peter W. Reiners Dirk Frei Jan Kosler Yusheng Wan Jens Götze Tobias Häger Alfred Kröner John W. Valley 《Geostandards and Geoanalytical Research》2008,32(3):247-265
We introduce and propose zircon M257 as a future reference material for the determination of zircon U‐Pb ages by means of secondary ion mass spectrometry. This light brownish, flawless, cut gemstone specimen from Sri Lanka weighed 5.14 g (25.7 carats). Zircon M257 has TIMS‐determined, mean isotopic ratios (2s uncertainties) of 0.09100 ± 0.00003 for 206pb/238U and 0.7392 ± 0.0003 for 207pb/235U. Its 206pb/238U age is 561.3 ± 0.3 Ma (unweighted mean, uncertainty quoted at the 95% confidence level); the U‐Pb system is concordant within uncertainty of decay constants. Zircon M257 contains ~ 840 μg g?1 U (Th/U ~ 0.27). The material exhibits remarkably low heterogeneity, with a virtual absence of any internal textures even in cathodoluminescence images. The uniform, moderate degree of radiation damage (estimated from the expansion of unit‐cell parameters, broadening of Raman spectral parameters and density) corresponds well, within the “Sri Lankan trends”, with actinide concentrations, U‐Pb age, and the calculated alpha fluence of 1.66 × 1018 g?1. This, and a (U+Th)/He age of 419 ± 9 Ma (2s), enables us to exclude any unusual thermal history or heat treatment, which could potentially have affected the retention of radiogenic Pb. The oxygen isotope ratio of this zircon is 13.9%o VSMOW suggesting a metamorphic genesis in a marble or calc‐silicate skarn. 相似文献
22.
Martin Rosner Michael Wiedenbeck Thomas Ludwig 《Geostandards and Geoanalytical Research》2008,32(1):27-38
An analytical artefact is reported here related to differences in instrumental mass fractionation between NIST SRM glasses and natural geological glasses during SIMS boron isotope determinations. The data presented demonstrated an average 3.4‰ difference between the NIST glasses and natural basaltic to rhyolitic glasses mainly in terms of their sputtering-induced fractionation of boron isotopes. As no matrix effect was found among basaltic to rhyolitic glasses, instrumental mass fractionation of most natural glass samples can be corrected by using appropriate glass reference materials. In order to confirm the existence of the compositionally induced variations in boron SIMS instrumental mass bias, the observed offset in SIMS instrumental mass bias has been independently reproduced in two laboratories and the phenomenon has been found to be stable over a period of more than one year. This study highlights the need for a close match between the chemical composition of the reference material and the samples being investigated. 相似文献
23.
Taeko Shinonaga Helmuth Aigner Dilani Klose Peter Spinder Heinz Fröschl David Donohue 《Geostandards and Geoanalytical Research》2008,32(1):93-101
The recommended concentrations of 239Pu, 240Pu and 239+240Pu in reference material IAEA‐315 (marine sediment) were estimated by three analytical methods: isotope dilution thermal ionisation mass spectrometry (TIMS), isotope dilution inductively coupled plasma‐mass spectrometry (ICP‐MS) and alpha spectrometry. The determination of 239Pu and 240Pu (239+240Pu by alpha spectrometry) was carried out with samples from randomly selected bottles using each method. Plutonium‐238 was also measured by alpha spectrometry. A plutonium‐242 reference material was used as a spike for the quantitative analysis. The influence of 242Pu in the samples was therefore calculated; however, this contribution was less than the range of uncertainty and did not influence the final results. The obtained data were statistically analysed using variance component analysis and paired comparison. The combined standard uncertainties from “method/measurement”, “bottle” and “sub‐sample” were in the order of 3 to 6%. The main contributions to the uncertainty were from the material heterogeneity and from systematic differences between methods. Based on this study with twenty‐seven analyses using 10–14 g sample mass, concentrations of (38 ± 3) Bq kg?1, (28 ± 3) Bq kg?1 and (66 ± 4) Bq kg?1 are proposed as recommended values for 239Pu, 240Pu and 239+240Pu, respectively, and (9.5 ± 0.4) Bq kg?1 for 238Pu as an information value in reference material IAEA‐315. In mass concentration units, these amount to (16.4 ± 1.2) ng kg?1, (3.3 ± 0.4) ng kg?1 and (0.015 ± 0.003) ng kg?1 for 239Pu, 240Pu and 238Pu, respectively. The certified reference materials NIST 4350B and NIST 4354 were also analysed by TIMS for quality assurance of the method used in this study. 相似文献
24.
Janet M. Hergt L. Paul Bédard Etienne Deloule Klaus Peter Jochum Kathryn L. Linge Paul J. Sylvester Matthias Willbold Jon D. Woodhead 《Geostandards and Geoanalytical Research》2006,30(3):141-142
In 2005 Geostandards and Geoanalytical Research embarked upon a new initiative for its readers. Key researchers in various fields of geoanalytical technique development and their application were identified and invited to provide reviews pertinent to their expertise. As noted in the first of these publications "…instead of revisiting the historical context or decades of development in each analytical technique, the goal here has been to capture a snapshot of "hot topics" across a range of fields as represented in the… literature" (Hergt et al . 2005). Rather than prepare an annual review, a decision was taken earlier this year to provide a biennial summary of progress and accomplishments, in this case for the years 2004–2005. The principal techniques employed in Earth and environmental sciences are covered here, and include laser ablation and multicollector ICP-MS, ICP-AES, thermal ionisation and secondary ion mass spectrometry, as well as neutron activation analysis, X-ray fluorescence and atomic absorption spectrometry. A comprehensive review of the development of reference materials, often essential to these techniques, is also provided. The contributions assembled serve both to keep readers informed of advances they may be unfamiliar with, but also as a means of showcasing examples of the breadth and depth of work being conducted in these fields. 相似文献
25.
This review gives an overview of the use and development of reference materials of geochemical and environmental interest in the literature of the years 2004 and 2005. In these years the performance of existing methods has been improved and new geochemical applications using new techniques have been developed. Accordingly, there was an increasing need for new reference materials, especially for in situ microanalysis and for precise stable isotope measurements. In addition, there was a notable trend for further characterisation of existing reference materials, mainly for the platinum-group elements. This review focuses on five topics: reference materials for platinum-group elements, reference glasses for in situ microanalysis, zircon reference materials, isotopic reference materials, and the development and certification of reference materials. 相似文献
26.
湿地功能快速评价中的若干理论问题 总被引:9,自引:5,他引:9
针对目前湿地功能快速评价中存在的不足之处,分析了产生这些不足的原因及湿地功能快速评价过程中存在的一些基本理论问题。分析表明:湿地功能快速评价方法是为了达到“湿地功能无净损失”目的,是在需要评价的湿地如此之多而从事湿地功能评价的专业人员又极其缺乏的情况下发展起来的。它对于湿地恢复与重建以及湿地受人类活动干扰程度的评价是非常有效的;在湿地功能快速评价过程中,把相对未受人类干扰的参照湿地的功能指数规定为1,这就使得快速评价方法不能对参照湿地的功能进行评价,而目前最需要评价其功能的湿地往往就是这些相对未受人类活动干扰的湿地;在相同水文地貌的湿地类型内评价湿地功能之间的差异,这使得快速评价方法不能评价湿地的水文地貌功能;由于快速评价的结果都是相对的功能指数,并不能说明湿地所提供的功能量是否满足人们的需求,因而在决策中不能单独使用;快速评价都是“一次调查就获得结果”,同时由于快速评价过程中指标选择的主观性、指标赋值的主观性、采样点空间设置的主观性以及采样时间的主观性,对于具有时空变化特征的湿地功能的评价结果的可重复性和科学性是很低的。为了使湿地功能评价的结果对管理和决策具有指导意义,基于湿地功能量计算的、定量的评价湿地功能的方法必须开发出来。针对不同的评价目的,湿地功能评价可采用双重参照标准:一是以自然为参照来评价湿地功能受人类活动影响的程度以及湿地恢复与重建成功与否;二是以人类需要为标准来评价湿地提供的功能量是否满足了我们的期望,以便采取措施改进湿地功能来满足人类的需求。 相似文献
27.
The area of Serravalle, sited in the northern part of the town of Vittorio Veneto (TV), NE Italy, has been the target of a
seismic microzonation campaign. 10 seismic stations have been deployed for a 7 months period to record in continuous mode.
Three stations were installed on bedrock outcrops and seven on sedimentary sites with variable cover thickness. Spectral analyses
have been performed on the collected data-set using the Generalized Inversion Technique (GIT, e.g. Andrews, 1986). In particular,
spectral ratios have been calculated for each station relatively to the average of the three reference, bedrock sites. The
spectral ratios provide quantitative estimates of the seismic motion amplifications which occur in each of the monitored sites.
Two sites show high values of amplification, 5 times larger than signal amplitude at the reference sites, in correspondence
of well discernible peak frequencies of 5 Hz. Results for the other stations show smaller amounts of site amplification spreading
over a broad range of frequencies. Sites where the highest amplifications were recorded all lie on the left bank of the Meschio
River and in areas farther away from its outlet into the plain correlating with the presence of thick layers of Quaternary
deposits. 相似文献
28.
The páramo is a neotropical alpine ecosystem that covers more than 75,000 km2 of the northern Andes of Colombia, Ecuador, Venezuela, and Peru. It provides important environmental services: more than 10 million people in the Andean highlands benefit from the water supply and regulation function, which is attributed to the volcanic soils that underlie the ecosystem. The soils are also major carbon sinks of global significance. Severe land use changes and soil degradation threaten both the hydrology and carbon sink function. Nevertheless, soil genesis and properties in the páramo is rather poorly understood, nor are their ecological functions well documented. The impact of the geomorphology of the páramo on soil genesis was studied in the rio Paute basin, south Ecuador. Two toposequences were described and analysed. In each toposequence, four pedons were selected representing summit, backslope, undrained plain situation, and valley bottom positions in the landscape. The soils are classified as Hydric Andosols in the World Reference Base for Soil Resources and Epiaquands or Hydrudands in Soil Taxonomy. They are very acidic and have a high organic matter content, high P deficiency, and Al toxicity. Their water content ranges from 2.64 g g− 1 at saturation, down to 1.24 g g− 1 at wilting point, resulting in a large water storage capacity. Two major soil forming processes are identified: (1) volcanic ash deposition and (2) accumulation of organic carbon. Volcanic ash deposits may vary in depth as a result of regional geomorphological factors such as parent material, orientation, slope, and altitude. Organic carbon accumulation is an interaction of both waterlogging, which depends on the position in the landscape, and the formation of organometallic complexes with Al and Fe released during volcanic ash breakdown. Despite the high variability in parent material and topography, the soil is characterised by a notable homogeneity in physico-chemical properties. Statistical analysis reveals that only topographic location has a slight but significant influence on soil pH as well as the organic matter content, saturated conductivity and water retention at high pressure. Finally, the exceptional properties of these soils provide useful insights to improve classification of the Andosols reference group of the FAO World reference Base for Soil Resources. 相似文献
29.
河北省永久性GPS参考(网)站建立的研究与探讨 总被引:4,自引:0,他引:4
重点探讨了如何利用VRS技术在河北省区域内建立永久性参考站,如何进行数据的采集与管理,如何为GPS用户提供参考站数据等技术问题。 相似文献
30.
R. Pail 《Journal of Geodesy》2005,79(4-5):231-241
In the recent design of the Gravity field and steady-state Ocean Circulation Explorer (GOCE) satellite mission, the gravity gradients are defined in the gradiometer reference frame (GRF), which deviates from the actual flight direction (local orbit reference frame, LORF) by up to 3–4°. The main objective of this paper is to investigate the effect of uncertainties in the knowledge of the gradiometer orientation due to attitude reconstitution errors on the gravity field solution. In the framework of several numerical simulations, which are based on a realistic mission configuration, different scenarios are investigated, to provide the accuracy requirements of the orientation information. It turns out that orientation errors have to be seriously considered, because they may represent a significant error component of the gravity field solution. While in a realistic mission scenario (colored gradiometer noise) the gravity field solutions are quite insensitive to small orientation biases, random noise applied to the attitude information can have a considerable impact on the accuracy of the resolved gravity field models. 相似文献