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1.
近年来激光剥蚀电感耦合等离子体质谱(LA-ICP-MS)应用于单个流体包裹体成分定量分析已成为研究流体包裹体的最佳手段之一。该实验过程和数据处理比较复杂,目前国内外采用的数据分析软件为一款基于MATLAB的SILLS软件,该软件主要是对矿物(锆石)、流体包裹体以及熔体包裹体LA-ICP-MS分析结果进行处理。本文以萤石流体包裹体LA-ICP-MS分析为例,阐述了样品制备与流体包裹体的优选方法,对流体包裹体片厚度以及单个流体包裹体的选取要求作了详细描述,对仪器参数设置、内外标样选取和剥蚀方法等进行了说明。基于SILLS软件采用尖峰消除的方法对待处理数据进行校正,对不同种类型的波峰进行峰宽的选取。在元素比值校正和等效盐度计算过程中,由于被测样品是萤石,Ca元素具有较高的背景值,选择以Na作为流体包裹体的内标元素,以Ca作为寄主矿物的内标元素对寄主矿物浓度进行计算,同时提出以电价平衡代替质量平衡进行等效盐度计算。以上方案提高了LA-ICP-MS分析单个萤石流体包裹体的准确性,有助于解释成矿流体来源和矿床成因等问题。 相似文献
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三峡库区龙门寨危岩体崩塌产生涌浪研究 总被引:1,自引:1,他引:0
长江两岸高耸的危岩体对航道、沿岸居民带来巨大安全隐患。大宁河属于长江一级支流,龙门寨危岩体位于大宁河上,距离巫山县城仅1 km。利用FLOW-3D软件,模拟了145 m、175 m两种水位工况下龙门寨危岩体崩塌产生涌浪过程和涌浪传播过程。模拟结果表明,涌浪在145 m水位工况下最大浪高约为17.9 m,175 m水位工况下最大浪高约为11.6 m;在巫山县的五个码头处,两种水位工况最大涌浪爬高分别约为10.9 m、3.8 m;根据涌浪高度,对大宁河进行危险分区,145 m水位工况下极高危险区长度约4.4 km,很高危险区长度约1.9 km;175 m水位工况下极高危险区长度约3.0 km,很高危险区长度约1.0 km。研究结果有助于防控龙门寨危岩体潜在涌浪灾害危害,保障大宁河航道和巫山县码头安全,同时也为三峡库区滑坡涌浪灾害提供了预警依据。 相似文献
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Attribution analysis for water yield service based on the geographical detector method: A case study of the Hengduan Mountain region 总被引:1,自引:0,他引:1
Ecosystem services, which include water yield services, have been incorporated into decision processes of regional land use planning and sustainable development. Spatial pattern characteristics and identification of factors that influence water yield are the basis for decision making. However, there are limited studies on the driving mechanisms that affect the spatial heterogeneity of ecosystem services. In this study, we used the Hengduan Mountain region in southwest China, with obvious spatial heterogeneity, as the research site. The water yield module in the In VEST software was used to simulate the spatial distribution of water yield. Also, quantitative attribution analysis was conducted for various geomorphological and climatic zones in the Hengduan Mountain region by using the geographical detector method. Influencing factors, such as climate, topography, soil, vegetation type, and land use type and pattern, were taken into consideration for this analysis. Four key findings were obtained. First, water yield spatial heterogeneity is influenced most by climate-related factors, where precipitation and evapotranspiration are the dominant factors. Second, the relative importance of each impact factor to the water yield heterogeneity differs significantly by geomorphological and climatic zones. In flat areas, the influence of evapotranspiration is higher than that of precipitation. As relief increases, the importance of precipitation increases and eventually, it becomes the most influential factor. Evapotranspiration is the most influential factor in a plateau climate zone, while in the mid-subtropical zone, precipitation is the main controlling factor. Third, land use type is also an important driving force in flat areas. Thus, more attention should be paid to urbanization and land use planning, which involves land use changes, to mitigate the impact on water yield spatial pattern. The fourth finding was that a risk detector showed that Primarosol and Anthropogenic soil areas, shrub areas, and areas with slope 5° and 25°–35° should be recognized as water yield important zones, while the corresponding elevation values are different among different geomorphological and climatic zones. Therefore, the spatial heterogeneity and influencing factors in different zones should be fully con-sidered while planning the maintenance and protection of water yield services in the Hengduan Mountain region. 相似文献
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Automated Extraction of a Five‐Year LA‐ICP‐MS Trace Element Data Set of Ten Common Glass and Carbonate Reference Materials: Long‐Term Data Quality,Optimisation and Laser Cell Homogeneity 下载免费PDF全文
LA‐ICP‐MS is increasingly applied to obtain quantitative multi‐element data with minimal sample preparation, usually achieved by calibration using reference materials (RMs). However, some ubiquitous RMs, for example the NIST SRM 61× series glasses, suffer from reported value uncertainties for certain elements. Moreover, no long‐term data set of analyses conducted over a range of ablation and tuning conditions exists. Thus, there has been little rigorous examination of the extent to which offsets between measured and reported values are the result of error in these values rather than analytically induced fractionation. We present new software (‘LA‐MINE’), capable of extracting LA‐ICP‐MS data with no user input, and apply this to our system, yielding over 5 years of data (~ 5700 analyses of ten glass and carbonate RMs). We examine the relative importance of systematic analytical bias and possible error in reported values through a mass‐specific breakdown of fourteen of the most commonly determined elements. Furthermore, these data, obtained under a wide range of different ablation conditions, enable specific recommendations of how data quality may be improved, for example the role of diatomic gas, the effect of differential inter‐glass fractionation factors and choice of transport tubing material. Finally, these data demonstrate that the two‐volume Laurin ablation cell is characterised by no discernible spatial heterogeneity in measured trace element ratios. 相似文献
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利用赤峰台井下和山洞观测、二连浩特台井下和地表观测测震数据,通过计算其加速度PSD值和相应的PDF值及1~20 Hz频段RMS值,研究井下观测压制测震台站背景噪声的特征。结果表明,在大于2 Hz频段,井下观测相比于山洞和地表观测有显著的压制背景噪声特征,尤其在大于9 Hz频段压制背景噪声特征突出;在16 s~2 Hz频段,井下、山洞、地表观测测震台站背景噪声水平一致性较高,井下观测在该频段不能压制背景噪声;在低于16 s频段,井下观测相比于山洞和地表观测有一定的压制背景噪声特征。通过井下观测可有效降低测震台站背景噪声水平,从而提高观测数据质量。 相似文献
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