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用WB和JC标准水合法测定轻烧MgO粉的活性MgO含量,对测定结果进行方差和误差分析,并研究了水化时间对测定结果的影响。结果表明,两种方法存在显著性差异,WB和JC水合法的平均相对误差分别为1.31%和-19.85%,WB水合法精密度远高于JC水合法。以WB水合法为基准,JC水合法的平均相对误差大于-20%,远远超过行业标准中规定的±3%。因此,对于镁水泥原料MgO中活性含量的定量分析,不能采用JC方法,必须采用WB方法。此外,发现水化3 h已经接近活性氧化镁的水化平衡,为修订WB标准方法提供了参考依据。 相似文献
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Carole Cordier Martial Caroff Thierry Juteau Corinne Fleutelot Christophe Hmond Marion Drouin Joseph Cotten Claire Bollinger 《Lithos》2007,99(3-4):289-311
The present study is based on a set of lavas and crosscutting dikes collected by dives along detailed vertical transects on the northern flank of the western part of the Blanco Transform Fault, Northeast Pacific. The studied area consists of a small basin, the Western Blanco Depression (WBD), extending from the southern end of the Juan de Fuca ridge to a pseudofault trace 60 km eastward. The Northern Scarp of the WBD comprises a volcanic unit overlying a sheeted-dike complex. Major and trace element data, coupled with Sr–Nd isotope ratios, reveal a two-component mantle source, composed by an isotopically depleted matrix variably veined by more enriched material. One chemical group (NS2), indistinguishable from the other Northern Scarp samples on the basis of trace element data, has an unusually depleted isotopic composition typical of a nearly pure mantle end-member. Some cogenetic samples of the Northern Scarp have been used to constrain the differentiation modalities. Anorthite and MgO content profiles in plagioclase xenocrysts and phenocrysts reveal (i) the existence of H2O-bearing evolved melts in the mushy zones and (ii) the occurrence of mixing process between these melts and anhydrous mafic liquids. The hydration is supported by other petrographic features such as high magmatic fO2 values, calculated from Fe–Ti oxide pairs, and the presence of pyroxene inclusions in plagioclase phenocrysts. Mixing, consistent with the existence of Ni-rich ferrobasalts, is interpreted to be the consequence of the reservoir refilling by mafic liquids (Mg# = 70). These petrological and geochemical evidences are combined with the evolution of Mg# with depth to suggest a periodic open-system magma chamber evolution beneath the southern end of the Juan de Fuca ridge. 相似文献
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不同浓度的Na2SO4水溶液的拉曼光谱显示了SO42-的四个拉曼活性带:980 cm-1处的SO42-的对称伸缩振动模式v1带,1 106 cm-1处的反对称伸缩振动模式v3带,448 cm-1处的变形振动模式v2带和617 cm-1处的变形振动模式v4带。482 cm-1处的肩膀峰是由于NaSO4-离子对的形成对448 cm-1的v2带的影响而形成的SO42-的一个新的振动峰。浓Na2SO4水溶液中,水共享离子对[Na+.H2O.SO42-]-是主要的离子对物种。随着Na2SO4水溶液浓度的增加,Na+和SO42-的相互作用增强,NaSO4-离子对所占的摩尔分数增加。 相似文献
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Kevin Hall 《地球表面变化过程与地形》1986,11(2):131-142
Rock moisture content is a major control of mechanical weathering, particularly freeze-thaw, and yet almost no data exist from field situations. This study presents moisture content values for rocks, taken from a variety of positions and conditions, in the maritime Antarctic. Additional information regarding the amount of water the rock could take up, as observed from laboratory experiments, is also presented. The results show that the approaches used in simulation experiments, particularly that of soaking a rock for 24 hours, may produce exaggerated results. It was found that the saturation coefficient (S-value) was a good indicator of frost susceptibility (based on water content) but that the derivation of that value may underestimate the potential of some rocks. The distribution of moisture within rocks is seen as an important, but unkown, factor. The results of these field moisture contents suggest that for simulations of freeze-thaw or hydration to be meaningful then they should have rock water contents based on field observations. 相似文献
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The bedrock freeze-thaw and moisture regimes at an actively eroding site on the Niagara Escarpment, Bruce Peninsula, southern Ontario, were monitored between December 1983 and April 1984, and the results compared with amounts of debris collected in an adjacent rock trap. Frost wedging in pre-existing rock fissures is the primary mechanism responsible for the observed rockfall events; hydration effects are negligible. Debris production was more closely related to the duration of the freezing leg of the freeze-thaw cycle than to intensity or to cycle frequency. Release also coincided with periods of high pore saturation (> 60 per cent) and the seepage of water from cracks and fissures. Fewer freeze-thaw cycles were recorded in the air than at 1 and 3.5 cm in the bedrock. The number of cycles that could be declared geomorphologically effective according to established temperature criteria was normally less than half the total number of freeze-thaw cycles recorded in both air and bedrock. Under the current temperature regime at the field site, few effective cycles are capable of penetrating more than 5 cm into the free face. 相似文献
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The characteristics of gas hydrates recovered from the Mount Elbert Gas Hydrate Stratigraphic Test Well, Alaska North Slope 总被引：1，自引：0，他引：1
Hailong Lu Thomas D. LorensonIgor L. Moudrakovski John A. RipmeesterTimothy S. Collett Robert B. HunterChris I. Ratcliffe 《Marine and Petroleum Geology》2011,28(2):411-418
Systematic analyses have been carried out on two gas hydrate-bearing sediment core samples, HYPV4, which was preserved by CH4 gas pressurization, and HYLN7, which was preserved in liquid-nitrogen, recovered from the BPXA-DOE-USGS Mount Elbert Stratigraphic Test Well. Gas hydrate in the studied core samples was found by observation to have developed in sediment pores, and the distribution of hydrate saturation in the cores imply that gas hydrate had experienced stepwise dissociation before it was stabilized by either liquid nitrogen or pressurizing gas. The gas hydrates were determined to be structure Type I hydrate with hydration numbers of approximately 6.1 by instrumentation methods such as powder X-ray diffraction, Raman spectroscopy and solid state 13C NMR. The hydrate gas composition was predominantly methane, and isotopic analysis showed that the methane was of thermogenic origin (mean δ13C = −48.6‰ and δD = −248‰ for sample HYLN7). Isotopic analysis of methane from sample HYPV4 revealed secondary hydrate formation from the pressurizing methane gas during storage. 相似文献
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Shale with high clay content has caused instability from hydration during the hydraulic fracturing process. Macro-level migration phenomenon of water molecules is induced by the chemical potential difference between low-salinity fracturing fluid and high-salinity formation brine. This study aims to establish the equation for the chemical potential difference between fracturing fluid and formation brine by theoretical deduction in order to investigate the effect of the aforementioned phenomenon on fracturing flowback. Accordingly, a mathematical model was established for the gas–water two-phase flow which driven by the chemical potential difference. Viscous force, capillarity and chemiosmosis were considered as the driving forces. A numerical simulation of fracturing fluid flowback with or without considering of the effect of chemiosmosis was performed. A simulation analysis of the water saturation and salinity profiles was also conducted. Results show that capillarity and chemiosmosis hinder fracturing fluid flowback in different degrees. As the condition worsens, they inhibit more than 80% of water to flow back out of the formation, forming a permanent water lock. This study contributes to improvement of the theory on shale gas–water two-phase flow, establishment of a flowback model that suitable for shale gas wells, and accurate evaluation of the fracturing treatment. 相似文献
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应用氯化镁—石灰乳法制备高纯氧化镁,降低氧化镁中钙含量是保证氧化镁产品质量的关键。通过对氧化镁的常温水化及二次煅烧,有效降低了氧化镁中钙含量,并通过正交试验得到了最优的水化工艺参数。氢氧化镁经850℃煅烧120 min,然后水洗,再次在1 050℃煅烧120 min,所得氧化镁纯度为99.1%99.4%,水化后钙含量(以CaO计)降低了约1%。 相似文献