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1.
Very fine samples from the mineralized zones of the Jacupiranga complex at the Cajati mine were selected for crystallographic identification of Ti-magnesioferrite (TMf) nanostructures embedded in titanomagnetite (TM) using high-resolution transmission electron microscopy (TEM). A magnetic concentrate obtained of pyroxenite samples (sites 4 to 7) was reduced and divided into fractions of distinct range sizes: 26±2 μm, 19±1 μm, 13±1 μm, 9±1 μm, 6±1 μm and 6-0.1 μm. The mineralized samples of carbonatite and pyroxenite were characterized by X-ray diffraction, transmitted and reflected light microscope, and scanning electron microscope with multielemental analysis. The finest magnetic concentrate sample (MC6) was analyzed under high-resolution transmitted electron microscopy (TEM) and high angle annular dark field and Raman spectroscopy. Magnetic properties were measured for the distinct granulometric fractions, showing drastic changes when grain sizes go beyond the frontier from micro to nanometer sizes. Frequency-dependent magnetic susceptibility percentage (÷fd%) report higher values (10.2%) for the finer fractions (6±1 μm and 6-0.1 μm) attributed to dominant fractions of superparamagnetic particles. Nanometer and < 6 μm grain size TMf in TM particles require a magnetic field up to 249 mT to reach saturation during the isothermal remanent magnetization experiment. Coercivity and remanent magnetization of these samples increase when the particle size decreases, probably due to parallel coupling effects. Magnetic susceptibility versus temperature experiments were conducted two times on the same (< 35 nm) sample, showing that the repetition during the second heating is probably due to the formation of new TMf nanoparticles and growth of those already present during the first heating process.  相似文献   
2.
The Early Cretaceous may be considered a key period for understanding the evolution of the Earth’s magnetic field. Some still unsolved problems are related to the mode of paleosecular variation (PSV) of the Earth’s magnetic field before and during the Cretaceous Normal Superchron. We report here a detailed rock-magnetic, paleomagnetic and paleointensity investigation from 28 lava flows (331 standard paleomagnetic cores) collected in the Argentinean part of the Parana Flood Basalts (Formation Posadas) in order to contribute to the study of PSV during the early Cretaceous and to obtain precise Cretaceous paleomagnetic pole positions for stable South America. The average paleofield direction is precisely determined from 26 sites, which show small within-site dispersion and high directional stability. Five sites show evidences for the self-reversal of thermoremanent magnetization. 23 sites yielded normal polarity magnetization and only 3 are reversely magnetized. Moving windows averages were used to analyze the sequential variation of virtual geomagnetic pole’s (VGP) axial positions. Interestingly, the axial average VGP path traces an almost complete cycle around the geographical pole and passes near the location of all previously published Paraná Magmatic Province poles. Both paleomagnetic poles and average VGP paths are significantly different from the pole position suggested by fixed hotspot reconstructions, which may be due to true polar wander or the hotspot motion itself. Only 15 samples from 5 individual basaltic lava flows, yielded acceptable paleointensity estimates. The site mean paleointensities range from 25.2 ± 2.2 to 44.0 ± 2.2 μT. The virtual dipole moments (VDMs) range from 4.8 to 9.9 × 1022 Am2. This correspond to a mean value of 7.7 ± 2.1 × 1022 Am2 which is 96% of the present day geomagnetic field strength. These intensities agree with the relatively high values already reported for Early Cretaceous, which are consistent with some inferences from computer simulations previously published.  相似文献   
3.
Twenty years after Tanaka and Kono's pioneering contribution (Tanaka and Kono, 1984), we give some new details on the effect of applied field strength during Thellier paleointensity experiments. Special attention is paid to the relation of magnitude of laboratory field and Coe's quality factors (Coe et al., 1978). Full thermoremanent magnetizations were imparted on natural samples containing low-Ti titanomagnetites of pseudo-single domain structure in a 40-μT magnetic field from 600?°C to room temperature. The samples were subjected to the routine Thellier procedure using a wide range of applied laboratory fields. Results indicate that values of laboratory fields may be accurately reproduced within 2% of standard error. The quality factors, however, decrease when the magnitude of ‘ancient’ field does not match to applied laboratory fields. To cite this article: J. Morales et al., C. R. Geoscience 338 (2006).  相似文献   
4.
In this work, we investigate the correlation between some magnetic parameters and the level of contamination by heavy metals in urban soils from Morelia city, western Mexico. The magnetic study was carried out on 98 urban soils samples belonging to distinct land uses. Most of analyzed samples contain ferrimagnetic minerals as the responsible for magnetization, most probably corresponding to the titanomagnetites/ titanomaghemites solid solutions. This is inferred from the susceptibility vs. temperature measurements and the isothermal remanent magnetization (IRM) experiments. These measurements also indicate that most of samples are almost completely saturated before 300 mT. Additionally, the S-200 values (S-200 = IRM-200/ SIRM, where IRM-200= Back-field of 200 mT after magnetic saturation) are between 0.7 and 1.0, characteristic of low coercivity magnetic minerals. The averaged saturation isothermal remanent magnetization (SIRM) curves can be used as an indicator of pollution level, as these curves show different saturation values according to the level of contamination by heavy metals: Cu, Ni, Cr and Sr. These associations of (titano)magnetite with heavy metals were observed by Scanning Electron Microscope revealing some complex aggregates rather than commonly detected spherules.  相似文献   
5.
We report the results of a rock magnetic and archeointensity study on pottery fragments recovered at the archaeological site of Puertas de Rolón, Capacha culture (Colima), that is considered one of the most important pre-Classic cultural developments of western Mesoamerica, Mexico. Standard rock magnetic experiments were carried out in order to investigate the reliability of the ancient field strength recovered from studied materials. Six out of the seven analyzed fragments gave reliable intensity determinations. The mean archeointensity value obtained in this study is 35.3 ± 3.4 μT. It is in good agreement with another contemporaneous Mesoamerican mean archeointensity of 34.3 ± 1.1 μT obtained for El Opeño. Statistically similar rock-magnetic parameters between ceramics from El Opeño and Puertas de Rolón potsherds appear to be related to clay-sources with similar geological settings and weathering processes. Alternatively, ancient trade or interexchange between western (Capacha Culture) and eastern Mesoamerica locations, as it has been proposed earlier, seem to be supported by results obtained in this study.  相似文献   
6.
Laguna Melincué is a shallow lake located in Santa Fe Province, Argentina (33°41′27.8″S, 61°31′36.5″W). The catchment area is around 1495 km2 and it is located in the Pampean Plains. It was reduced to 678 km2 by the construction of the San Urbano channel in 1941 and reconditioned in 1977, which was built to avoid floods. The floods are related to some El Niño episodes, with high precipitation events. The lake has been previously studied from different approaches, mainly to understand hydrological and climatic variations, but more multidisciplinary studies are needed to understand its complex hydrological situation. Here we present the first paleomagnetic and rock magnetic studies made on a short sediment core collected from the lake in order to contribute to identifying paleoclimatic proxies and to present the first paleomagnetic results for the site. Rock magnetic analyses suggest that the well-preserved magnetic mineralogy is dominated by pseudo single-domain (titano)magnetite and/or maghemite. The results also indicate that a stable characteristic remanent magnetisation can be isolated and thus the directions of the geomagnetic field may be obtained, providing evidence for the use of this lake for paleomagnetic and paleoenvironmental studies. Changes in magnetic grain size and concentration of magnetic minerals suggest environmental variations and changes in the lake level, which are consistent with historical reports. The paleomagnetic results agree well with Cals3k.3 model for inclination and declination of the geomagnetic field except for the dry period probably due to the fact that the core was extracted near the shore.  相似文献   
7.
The paleosecular variation (PSV) and polarity transitions are two major features of the Earth’s magnetic field. Both PSV and reversal studies are limited when age of studied units is poorly constrained. This is a case of Central and western Mexico volcanics. Although many studies have been devoted to these crucial problems and more than 200 paleomagnetic directions are available for the last 5 Ma, only few sites were dated directly. This paper presents new paleomagnetic results from seventeen independent cooling units in the Michoacán-Guanajuato Volcanic Field (MGVF) in western Mexico. Twelve sites are directly dated by 40Ar/39Ar or K-Ar methods and span from 2.78 to 0.56 Ma. The characteristic paleodirections are successfully isolated for 15 lava flows. The mean paleodirection (inclination I and declination D) obtained in this study is I = 28.8°, D = 354.9°, and Fisherian statistical parameters are k = 28, α95 = 7.3°, N=15, which corresponds to the mean paleomagnetic pole position Plat = 83.9°, Plong = 321.6°, K = 34, A95 = 6.6°. The paleodirections obtained in present study compiled with those, previously reported from the MGVF, are practically undistinguishable from the expected Plio-Quaternary paleodirections. The paleosecular variation is estimated through the study of the scatter of the virtual geomagnetic poles giving SF = 15.9 with SU =21.0 and SL = 12.7 (upper and lower limits respectively). These values agree reasonably well with the recent statistical Models. The oldest sites analyzed (the Santa Teresa and Cerro Alto) yield normal polarity magnetizations as expected for the cooling units belonging to the Gauss geomagnetic Chron. The interesting feature of the record comes from lava flows dated at about 2.35 Ma with clearly defined normal directions. This may point out the possible existence of a normal polarity magnetization in the Matuyama reversed Chron older than the Reunion and may be correlated to Halawa event interpreted as the Cryptochron C2r.2r-1. Another important feature of the geomagnetic record obtained from the MGVF is the evidence of fully reversed geomagnetic field within Bruhnes Chron, at about 0.56 Ma corresponding to the relative paleointensity minimum of global extent found in marine sediments at about 590 ka.  相似文献   
8.
Many archaeological artifacts contain magnetic minerals that may record the direction and strength of the Earth’s magnetic field. The geomagnetic field parameters (declination, inclination and intensity) change through time and then may be used as a dating tool. Over the last three decades, the archeomagnetic method was successfully applied in Europe. Still, no systematic studies are devoted to the American sites. We report here, a detailed rock-magnetic and archeomagnetic investigation of some pre-Columbian settlements at Chapultepec archeological site (western Mesoamerica). Continuous low-field susceptibility vs. temperature curves performed in air point to Ti-poor titanomagnetites as remanence carriers. Hysteresis ratios fall essentially in the pseudo-single-domain region. The twelve oriented samples taken from the furnace located in the habitation area were demagnetized applying pick alternative fields. In most cases, a stable uni-vectorial remanent magnetization was found yielding a reasonably well defined mean characteristic direction: inclination I = 32.8°, declination D = 353.4°, and parameters of Fisherian statistics α95 = 10.4° and k = 14. Still poorly defined directional master curves for Mesoamerica, together with relatively dispersed mean directions obtained in this study, make dating targets difficult. Archaeomagnetic dating was carried out on the basis of Bayessian statistics. This established a most probable time interval from 512 to 634 A.D. with an average of 573 ± 61 A.D.  相似文献   
9.
Rock-magnetic investigations of environmental samples, such as soils, dust and leaves, can provide useful information on environmental stress. Aim of this paper is to report on the first magnetic survey carried out on environmental samples from Bogotá, Colombia, which is the fifth most populated city of Latin America. We studied three kinds of samples in order to evaluate their potential as pollution markers: soils, urban dust and leaves of the Sauco (Sambucus nigra) tree. Standard magnetic methods were used to analyze the three groups of samples, with special emphasis on leaves investigated here for the first time for environmental purposes. Samples were collected along two perpendicular transects in an area of the city presumably unpolluted, with two different systems of public transportation. Thermomagnetic curves obtained from soils and atmospheric dust show clearly defined ferrimagnetic phase (probably magnetite) as the main magnetic carrier. Curves of acquisition of isothermal remanent magnetization confirm the ferrimagnetic character of magnetic particles. Frequency-dependent magnetic susceptibility was found between 0 and 10%, suggesting less-important contribution of ultrafine super-paramagnetic magnetite. The apparent contradictory results between soils and the rest of samples may reflect different accumulation period for magnetic particles, being shorter for leaves and urban dust than for soils.  相似文献   
10.
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