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Experimental results are presented from the extensive program of drained plane strain compression tests on sand carried out in Grenoble over the last two decades. Systematic analysis of photographs of the deforming specimen allowed for measuring deformations and determining strain fields throughout the test, that is: prior to, at, and after the onset of strain localization. The principles, details and accuracy of the procedure are described, as well as its suitability to properly depict the patterns of deformation. Findings concerning the occurrence and progression of strain localization are discussed. The issues of shear band orientation and thickness are addressed, as well as temporary and persistent complex localization patterns, and the volumetric behaviour inside a band after its formation. The influence of such variables as initial state of the sand (effective stress and relative density), specimen size and slenderness, as well as grain size, is discussed. Copyright © 2004 John Wiley & Sons, Ltd 相似文献
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Milatz Marius Hüsener Nicole Andò Edward Viggiani Gioacchino Grabe Jürgen 《Acta Geotechnica》2021,16(11):3573-3600
Acta Geotechnica - Gauging the mechanical effect of partial saturation in granular materials is experimentally challenging due to the very low suctions resulting from large pores. To this end, a... 相似文献
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This paper deals with the effects of thermal stresses on selected carbonate rocks used as dimension stones. They are Mesozoic calcareous and dolomitic rocks cropping out in Apulia (southern Italy) that, for their physico-mechanical and aesthetic properties, have always been finding a large application both as ornamental stones and as simple construction materials; their use is attested not only in Italy, in works of archaeological, historical and artistic interest too. The cause–effect relationships of thermal degradation were studied by means of an artificial accelerated ageing test, in order to provide a perspective about the decay of carbonate stones due to diurnal and seasonal temperature fluctuations, as well as thermal shocks during events of fire development. The stone samples were subjected to thermal cycles in a muffle furnace, ranging from 100 to 700 °C; after each cycle, several non-destructive and semi-destructive tests were carried out: mass and volume measurements, mercury intrusion porosimetry, sclerometer tests, ultrasonic tests, thin-section observations and determination of chromatic alterations through image analysis and Munsell charts method. In this way, the qualitative and quantitative modifications induced in fabric, physical and mechanical properties were discussed. The results highlight the fundamental role of depositional and diagenetic fabric that, together with mineralogical composition, represents the most significant discriminating factor in the response of the stone to thermal stresses. 相似文献
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Giorgio S. Senesi Gioacchino Tempesta Paola Manzari Giovanna Agrosì 《Geostandards and Geoanalytical Research》2016,40(4):533-541
An innovative approach of double pulse laser‐induced breakdown spectroscopy (DP‐LIBS) coupled with optical microscopy was applied to the characterisation and quantitative analysis of the Agoudal iron meteorite in bulk sample and in petrographic thin section. Qualitative analysis identified the elements Ca, Co, Fe, Ga, Li and Ni in the thin section and the whole meteorite. Two different methods, calibration‐free LIBS and one‐point calibration LIBS, were used as complementary methodologies for quantitative LIBS analysis. The elemental composition data obtained by LIBS were in good agreement with the compositional analyses obtained by traditional methods generally applied for the analysis of meteorites, such as ICP‐MS and EDS‐SEM. Besides the recognised advantages of LIBS over traditional techniques, including versatility, minimal destructivity, lack of waste production, low operating costs, rapidity of analysis, availability of transportable or portable systems, etc., additional advantages of this technique in the analysis of meteorites are precision and accuracy, sensitivity to low atomic number elements such as Li and the capacity to detect and quantify Co contents that cannot be obtained by EDS‐SEM. 相似文献
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P. Manzari S. De Angelis M. C. De Sanctis G. Agrosì G. Tempesta 《Meteoritics & planetary science》2019,54(3):475-494
Microimaging spectroscopy is going to be the new frontier for validating reflectance remote sensed data from missions to solar system bodies. In this field, microimaging spectroscopy of Martian meteorites can provide important and new contributions to interpret data that will be collected by next instruments onboard rover missions to Mars, such as for example Exomars‐2020/Ma_MISS spectrometer. In this paper, a slab from the Northwest Africa (NWA) 8657 shergottite was studied using the SPectral IMager (SPIM) microimaging spectrometer, in the visible‐infrared (VIS‐IR) range, with the aim to subsequently validate the spectral data by means of different independent techniques. The validation was thus carried out, for the first time, comparing SPIM spectral images, characterized by high spatial and spectral resolution, with mineralogical–petrological analyses, obtained by scanning electron microscopy (SEM). The suitability of the SPIM resolution to detect and map augite, pigeonite, maskelynite, and other minor phases as calcite, Ca‐phosphates, and troilite/pyrrhotite with no loss of information about mineral distribution on the slab surface, was ascertained. The good agreement found between spectral and mineralogical data suggests that spectral‐petrography of meteorites may be useful to support in situ investigations on Martian rocks carried out by MaMiss spectrometer during Exomars2020 mission. Moreover, micro spectral images could be also useful to characterize, in a nondestructive way, Martian meteorites and other rare minerals occurring in meteorites. The results obtained in this work represent not only a methodological contribution to the study of meteorites but furnish also elements to reconstruct the history of this sample. The finding of zoned pyroxene, symplectitic texture, amorphous phases as maskelynite, and Fe‐merrillite permits us to hypothesize four stages, i.e., (1) igneous formation of rimmed pyroxenes and other minerals, (2) retrograde metamorphism, (3) shock by impact, and (4) secondary minerals by terrestrial contamination. 相似文献
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This paper discusses the results of a large experimental program designed to investigate in a systematic manner the main features of the incremental response of fine‐grained soils. The results are obtained from triaxial stress probing experiments carried out on a French silty clay (Beaucaire Marl). All the tests have been performed on reconstituted specimens, normally consolidated to an initial state which is either isotropic or anisotropic. In the interpretation of the experimental results, extensive use is made of the concept of strain response envelope. The response envelopes obtained for different stress increment magnitudes are remarkably consistent with each other and indicate an inelastic and irreversible material response, i.e. a strong dependence on the stress increment direction, also at relatively small strain levels. A companion paper (Int. J. Numer. Anal. Meth. Geomech., this issue, 2006) assesses the performance of some advanced constitutive models in reproducing the behaviour of reconstituted Beaucaire Marl as observed in this experimental program. Copyright © 2006 John Wiley & Sons, Ltd. 相似文献
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Pierre Bésuelle Gioacchino Viggiani Jacques Desrues Cécile Coll Pascal Charrier 《Rock Mechanics and Rock Engineering》2014,47(1):143-155
This paper reports some results of a large experimental program on Boom Clay conducted in Grenoble in the framework of the European project SELFRAC. The program included isotropic compression up to relatively high stress, drained triaxial compression tests at different cell pressures, as well as permeability measurements under isotropic and deviatoric stress. Local measurement of axial and radial displacements allowed the detection of strain localization during deviatoric loading. The permeability of Boom Clay is found to depend on the mean effective stress. The response of Boom Clay during deviatoric loading appears to be strongly affected by the swelling experienced during the isotropic stage preceding triaxial compression. The rate of swelling decreases with isotropic stress. The longer the swelling before shear, more the response under shear becomes ductile and the lower the initial stiffness. Permeability depends on the mean effective stress and it is found to decrease of about two orders of magnitude when the mean stress increases from 1 to 32 MPa. Permeability during shear loading is essentially constant and does not seem to be affected by strain localization. These results are complemented by a few observations obtained using X-ray microtomography in the framework of the more recent European project TIMODAZ. These findings illustrate the impact of pre-existing inclusions and fissures on specimen deformation upon deviatoric loading in the laboratory. 相似文献
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G. Agrosì G. C. Capitani E. Scandale G. Tempesta 《Physics and Chemistry of Minerals》2011,38(2):101-109
Transmission Electron Microscopy (TEM) and High Resolution TEM (HRTEM) investigations were used to study a complex micro-structure
of twin-related lamellae of 15R SiC polytype, in syntactic coalescence with 6H-SiC. The analysis of the local stacking microstructure by means of HRTEM revealed that the perfect structure of 15R polytype, (23)3 was locally interrupted by numerous adjoining stacking faults parallel to (0001) with stacking of the coupled (22) and (33)
bilayers superimposed on the twin boundaries. HR images taken exactly across both the twin boundaries showed a zig-zag pattern
(23) that switched to (32) by a twin coherent interfaces or, alternatively, a zig-zag pattern (32) which passed to (23) through
an isolated (33), 6H like sequence. The selected area electron diffraction (SAED) patterns taken exactly above both the twin interfaces indicate
classifying of the twin found in this study as a “Friedelian” reticular merohedric twinning. However, two indistinguishable
twin operations matched the observed features: a reflection through rational plane (0001), and 180°-rotation around [0001].
Since individual Si and C atoms and even the SiC bilayer polarity could not be established from these HR images, the real
twin law was deduced by taking into account that the coherent structural match at the interface could be guaranteed only by
a 180°-rotation around [0001]. In order to explain the origin of the planar defects found in this sample, the growth mechanism
and the influence of the low-energy stacking faults were considered. 相似文献
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