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以灰树花发酵菌丝体为原料，经过提取分离纯化得到1种水溶性多糖GF4F1，经高碘酸氧化、Smith降解、甲基化、红外光谱（IR）以及核磁共振波谱（NMR）等分析表明，该多糖是1种β-1, 3／1，6-葡聚糖，且小鼠体内实验结果表明其具有良好的抗肿瘤活性。在1mg／kg时，对小鼠抑制率为67.3％。 相似文献
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Gui-Ping Wu Guang-Li Huang Yu-Hua Tang Yu Dai Department of Physics Southeast University Nanjing Purple Mountain Observatory Chinese Academy of Sciences Nanjing Department of Astronomy Nanjing University Nanjing 《中国天文和天体物理学报》2007,7(1):141-147
1INTRODUCTIONEnrichment of3He and heavy ions(i.e.,Ne,Mg,Si and Fe),characteristic of impulsive?ares,have beenstudied for more than three decades.It is found that they are generally associated with nonthermal energeticelectron-rich events(Reames et al.1988;Reames1999and references therein;Ho et al.2001;Wang et al.2006)and are related to the peculiar ratio of charge to mass(Mazur et al.1996;Reames1999).Althoughthe abundance of3He ions is not correlated with the abundance of heavy ions,s… 相似文献
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1 INTRODUCTIONSolar microwave bursts are usually produced by dtherellt radiation mechanisxns: gyroresonance absorption, Coulomb brernsstrahlung of the thermal baCkground plasma, as well asgyrosynchrotron radiation of the nonihermal electrons (Hildebrandt et al. 1998). Meanwhile,cyclotron or synchrotron maser instabilities may be responsible for microwave spaaes, blips, andtype ill bursts (Wu 1985; Huang 1987; Huang et al. 1996; Huang 1998), which are usuajly superposed on the ambient mi… 相似文献
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本文以厚叶切氏海带(Kjellmaniella crassi folia)为原料,经提取分离获得4种多糖(KW1,KW2,KA1和KA2).运用电泳、高效液相色谱(HPLC)、高效凝胶渗透色谱(HPGPC)及核磁共振氢谱(1H-NMR)法分别对其单糖组成、相对分子量(Mr)以及结构进行分析.结果表明,KW1与KA1是Mr为520 kD和430 kD且M/G(6.14和1.90)显著不同的褐藻胶;KW2是以岩藻糖(82％)为主的岩藻糖硫酸酯;KA2是以半乳糖(34％)、岩藻糖(27％)和甘露糖(21％)为主的杂聚硫酸多糖.KW2和KA2的Mr和硫酸基含量分别为536 kD和427 kD及30％和21％.经1 H-NMR分析表明,KW2的硫酸酯基主要存在于岩藻糖残基的C2和C4位. 相似文献
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1979-1999全球天测与测地VLBI观测资料处理结果与讨论 总被引：1，自引：0，他引：1
采用国际地民服务（ＩＥＲＳ）１９９６年规范和上海天文台甚长基线干涉测量（ＶＬＢＩ）资料分析软件,对自１９７９年８月以来全球约２９００次天测与测地ＶＩＢＬ实验进行了综合归算,得到６０１颗河外射电源在Ｊ２０００．０的坐标、１０１台站在Ｊ１９９７．０的坐标和运动速度、以及约２０年地地球定向参数序列。与国际相关结果的比较表明,归算结果不存在显著系统差。通过对归算结果的分析,指出目前国际上评估天球参考架局部 相似文献
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以灰树花发酵菌丝体水不溶性多糖GF4A为原料,以三氧化硫三甲胺盐(SO3·Me3N)为酯化试剂,探讨了GF4A的硫酸酯化工艺.实验结果表明,当三氧化硫与GF4A中单糖摩尔比为5.8∶1、反应温度为80 ℃、反应时间6 h时,所得酯化产物(SGF4A)水溶性好、产率高.该产物硫酸酯取代度为1.6, 相对分子质量为88 kD.通过红外光谱及核磁共振碳谱分析表明,糖残基中所有C-6羟基以及部分C-4和C-2位羟基被酯化.体外实验表明,SGF4A具有较好的抗凝活性. 相似文献
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The surface accuracy of a large parabolic antenna is an important indicator to evaluate the quality of the antenna.It not only directly affects the antenna’s aperture efficiency,thereby determining the shortest wavelength that the antenna can work,but also affects the main lobe width and side lobe structure of the antenna pattern.Microwave holography is an important method for parabolic antenna profile detection.In this article we adopt a new algorithm to adjust the panels for the large radio telescope with an active main reflector through the TM65 m antenna’s aperture phase profile.The panels of the TM65 m radio telescope is in a radial pattern with 14 rings.Each corner of the panel is fixed on the screw of the actuator to move up and down,and the adjacent corners of the four panels share an actuator.We use the method of plane fitting to calculate the adjustment value of every panel’s corner.But one actuator,which simultaneously controls the common corner of the adjacent panels,will have different adjustment values according to the different plane fitting equation based on adjacent panels.In this paper,the adjustment value of the adjacent panels’crosspoints are constrained to be equal to the constraint condition to calculate each actuator’s adjustment value of the TM65 m radio telescope.Through multiple adjustments and application of the new algorithms,the accuracy of the TM65 m antenna reflector profile has been improved from the original 0.28 mm to the current 0.19 mm. 相似文献
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In this paper, the observed solar radio pulsations during the bursts at 9.375 GHz are considered to be excited by some plasma instability. Under the condition of the conservation of energy in the wave-particle interaction, the saturation time of plasma instabilities is inversely proportional to the initial radiation intensity, which may explain why the repetition rate of the pulsations is directly proportional to the radio burst flux at 9.375 GHz as well as 15 GHz and 22 GHz. It is also predicted that the energy released in an individual pulse increases with increasing the flux of radio bursts, the modularity of the pulsations decreases with increasing the flux of radio bursts, these predictions are consistent with the statistical results at 9.375 GHz in different events. The energy density of the non-thermal particles in these events is estimated from the properties of pulsation. For the typical values of the ambient plasma density (109 cm–3) and the ratio between the nonthermal and ambient electrons (10–4), the order of magnitude of the energy density and the average energy of the nonthermal electrons is 10–4 erg/cm3 and 10 kev, respectively. It is interesting that there are two branches in a statistical relation between the repetition rate and the radio burst flux in a special event on March 11–17, 1989, which just corresponds to two different orders of magnitude for the quasi-quantized energy released in these five bursts. This result may be explained by the different ratios between the thermal and the nonthermal radiations. 相似文献
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制备5种氯霉素糖基化衍生物,并对这些衍生物的抑菌活性和安全性进行初步测试。实验结果表明:1)氯霉素被糖基化后水溶性得到了明显提高;2)氯霉素糖基化衍生物时未产生抗菌活性,但经相关糖苷酶水解后,可重新表现出抗菌活性;3)小鼠急毒试验证明,氯霉素糖基化衍生物的毒副作用与原药相比显著降低。该项研究对于设计和合成类氯霉素前药开辟了新领域。 相似文献
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