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Wu Shitou Yang Yueheng Roberts Nick M. W. Yang Ming Wang Hao Lan Zhongwu Xie Bohang Li Tianyi Xu Lei Huang Chao Xie Liewen Yang Jinhui Wu Fuyuan 《中国科学:地球科学(英文版)》2022,65(6):1146-1160
Science China Earth Sciences - U?Pb geochronology of calcite using laser ablation-inductively coupled plasma-mass spectrometry (LA-ICP-MS) is an emerging method, with potential applications... 相似文献
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大陆岩石圈地幔定年 总被引：4，自引：0，他引：4
大陆岩石圈地幔是伴随地壳熔体抽取而形成的低密度地幔残留,是联系软流圈与地壳的重要纽带。虽然大陆岩石圈地幔一直是固体地球科学研究的重要内容,但对其形成时代的准确厘定则是当前研究的难点。传统方法是采用岩石圈地幔中橄榄岩主要元素的贫瘠程度来对岩石圈进行定年,即古老的岩石圈地幔Al2O3和CaO含量低,而MgO含量高(同时导致橄榄石高Fo值),而年轻岩石圈地幔的特征正好相反。显然,这种间接的方法不能给出确切的年龄信息。尽管Sr-Nd和锆石U-Pb等同位素方法也被用来进行地幔橄榄岩定年,但岩石圈地幔通常具有的较高温度使上述同位素体系不能保持封闭,因而给出的年龄大多与岩石圈地幔的形成时代无关。近几年发展起来的Re-Os同位素技术是目前进行岩石圈地幔定年的最理想工具,但也存在一系列需要研究的问题。文中对这一方法的基本原理、发展现状和存在的问题进行了全面的介绍。同时,根据目前获得的Os同位素资料,对中国东部岩石圈地幔的时代进行了讨论,并简要论述所获得的资料对岩石圈减薄研究的启示。 相似文献
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基于国外大量硼同位素示踪的地热研究实例,在先期建立的MC-ICP-MS测定水中硼同位素分析方法基础上,以羊八井地热田为研究对象,进行了热田地热流体的硼同位素地球化学初步研究。研究表明,羊八井地热田区热储流体的硼同位素值为 -10.5‰～-9.1‰,为非海相来源; 结合区域地质特征,研究认为热储内的硼组分来源于蚀变花岗岩围岩,并且蚀变花岗岩的硼同位素特征可能与深层地热流体相似。研究表明羊八井浅层热储内硼元素的地球化学行为并非完全是保守元素,存在着一定的硼同位素分馏。在端元硼同位素特征差异较小的羊八井热田,为硼同位素二元混合模型示踪水体混合过程带来了相当的复杂性。本文从热田开采过程与采样时间、水-岩相互作用、气-液相分离以及结垢过程等方面分析了浅层热储内引起硼同位素分馏的可能因素,其中从整体来看,气-液相分离过程的影响相对较大;而在个别井位水-岩相互作用与结垢的影响可能相对较为显著。 相似文献
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Yangting Lin Sen Hu Bingkui Miao Lin Xu Yu Liu Liewen Xie Lu Feng Jing Yang 《Meteoritics & planetary science》2013,48(9):1572-1589
Grove Mountains (GRV) 020090 is an enriched lherzolitic shergottite, distinct from other lherzolitic shergottites, except RBT 04262/1. Its characteristics include high abundance of plagioclase (24.2 vol% in the nonpoikilitic area), presence of K‐feldspar, common occurrence of baddeleyite, high FeO contents of olivine (bimodal peaks at Fa 33 mol% and Fa 41 mol%) and low‐Ca pyroxenes (bimodal peaks at Fs 23.8–31.7 mol% and Fs 25.7–33.9 mol%), and significant LREE enrichment of phosphates (500–610 × CI). The bulk composition of GRV 020090 suggests derivation from partial melting of an enriched reservoir. However, the REE patterns of the cores of pigeonite oikocrysts and the olivine chadacrysts are indistinguishable from those of GRV 99027 and other moderately depleted lherzolitic shergottites, and reveal a LREE‐depleted pattern of the primordial parent magma. We propose that the primordial parent magma of GRV 020090 was derived from a moderately depleted Martian upper mantle reservoir, and later the residual melt was contaminated by oxidized and enriched Martian crustal materials as it ascended up to the subsurface. GRV 020090 and RBT 04262/1 may have sampled an igneous unit different from other lherzolitic shergottites. 相似文献
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Wei Qindi Wang Hao Yang Yueheng Yang Jinhui Huang Chao Wu Shitou Xie Liewen 《中国科学:地球科学(英文版)》2020,63(11):1780-1790
Science China Earth Sciences - To meet the rapid development of zircon U-Pb geochronology and Hf-O isotope geochemistry, it is imperative to develop well-characterized zircon reference materials... 相似文献
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Xiaoping Long Chao Yuan Min Sun Wenjiao Xiao Guochun Zhao Yujing Wang Keda Cai Xiaoping Xia Liewen Xie 《Tectonophysics》2010,480(1-4):213-231
Subduction–accretion complexes occur widely in the Central Asian Orogenic Belt (CAOB). Due to the scarcity of fossils, the depositional timing of the Habahe flysch sequence of the subduction–accretion complex in the Chinese Altai is poorly constrained, which gave rise to much controversy in understanding the time of the basement and the tectonic evolution of the Chinese Altai. U–Pb dating of detrital zircons from the Habahe sequence in the northwestern Chinese Altai reveals a young zircon population with a mean 206Pb/238U age around 438 Ma which, together with a mean 206Pb/238U age of 411 ± 5 Ma for the overlying rhyolite of the Dongxileke Formation, brackets the time of deposition of the sequence between early Silurian and early Devonian. The age of the Dongxileke rhyolite also indicates that the overlying Baihaba Formation possibly began to be deposited in the early Devonian, though U–Pb dating of detrital zircons from this formation gave a maximum depositional age of ～ 438 Ma. The youngest detrital zircons and metamorphic grains of the Habahe sequence reveal different provenance to the sequence in the east. The youngest and metamorphic zircon grains, with early Paleozoic, Neoproterozoic and pre-Neoproterozoic populations, suggest a multi-source for the Habahe sequence. The predominantly early Paleozoic zircons, characterized by concentric zoning, high Th/U ratios and euhedral shapes, imply that the sediments of the sequence were mostly derived from a proximal magmatic source. Based on the age patterns of the Neoproterozoic and pre-Neoproterozoic populations, the Tuva–Mongol Massif, along with adjacent island arcs and metamorphic belts, may be an alternative source region for the Habahe sequence. In view of new geochemical and chronological data for granitoids and advancement in the study of regional metamorphism in the Chinese Altai, we suggest a tectonic model of subduction beneath a huge subduction–accretion complex for the evolution of the Chinese Altai in the early Paleozoic. 相似文献
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Simultaneous in-situ analyses of trace elements, U–Th–Pb and Lu–Hf isotopes were carried out on distinct domains of zircons in ultrahigh-pressure (UHP) eclogite-facies metamorphic rocks from the main hole of the Chinese Continental Scientific Drilling (CCSD) in the Sulu orogen. For the first time, trace elements are directly linked to Lu–Hf isotopes in metamorphic zircons with reference to their U–Pb dates. This enables methodological integration to distinguish four types of metamorphic zircon: solid-state, replacement and dissolution recrystallizations of protolith zircons, and new growth from the aqueous fluid. Metamorphically grown zircons are characterized by concordant U–Pb ages for the metamorphism, flat HREE patterns typical of the garnet effect, low contents of REE (especially HREE), Y, Nb + Ta and Th + U, high contents of Hf, low (Lu/Gd)N, Lu/Hf and Th/U (< 0.1) ratios, and elevated 176Hf/177Hf ratios relative to solid-state recrystallized zircons. This suggests the effects of both garnet and fluid on the growth of metamorphic zircons. In contrast, metamorphic recrystallization has reset the U–Th–Pb isotope system of protolith zircons to different extents, depending on the extents of fluid action during metamorphism. Solid-state recrystallized zircons exhibit the lowest degrees of resetting and thus almost inherit all geochemical features from the protolith zircons, which are characterized by discordant U–Pb ages close to or below the protolith age, steep MREE–HREE patterns typical of magmatic origin, high contents of trace elements and their ratios, and low 176Hf/177Hf ratios. On the other hand, dissolution recrystallized zircons show the highest degrees of reworking and thus have concordant or nearly concordant U–Pb ages for the metamorphism, steep MREE–HREE patterns, lowered contents of trace elements such as REE, Th, U, Y, Nb, Ta and Ti relative to the protolith zircons, and almost unchanged Hf isotope ratios. Replacement recrystallized zircons display intermediate degrees of reworking and thus have their many features of elements and isotopes in between. While the metamorphic growth in the presence of both garnet and fluid is characterized by both depletion of HREE with flat pattern and the low contents of trace elements, the metamorphic recrystallization in the presence of aqueous fluid is indicated by gradual decreases of MREE to HREE without the flat HREE pattern. Therefore, the simultaneous in-situ analyses of metamorphic zircons have the advantage over single-term analyses in making distinction between the new growth and the different types of recrystallization. 相似文献
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An Improved Procedure for the Determination of Ferrous Iron Mass Fraction in Silicate Rocks Using a Schlenk Line‐Based Digestion Apparatus to Exclude Oxygen 
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下载免费PDF全文 Dingshuai Xue Hongyue Wang Yanhong Liu Liewen Xie Ping Shen 《Geostandards and Geoanalytical Research》2017,41(3):411-425
Precise and accurate determination of ferrous iron mass fraction in silicate rocks and geological reference materials is still a significant challenge due to the labile nature of the analyte. Here, we report a modified and improved procedure for the determination of ferrous iron mass fraction, capable of yielding moderately accurate and highly precise results in a relatively shorter time than before. This modified technique requires a more convenient operational procedure than the classical method. A sample digestion apparatus was designed that included a Schlenk line to expel air in order to prevent oxidation. The advantages of this procedure over the classical procedure are shorter process flow, higher efficiency and absence of an additional redox indicator. The composition of the acid matrix used to dissolve the samples as well as the incubation temperature and time was investigated. Comparative data for twenty‐one reference materials are reported, with five of them reported for the first time by the Schlenk line procedure. A series of experiments were carried out to identify and minimise the main source of error. In addition, the possibility of eliminating the reducing substances before digestion, by pretreatment of the sample by cold 10% methanolic bromine, was also studied. 相似文献
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