Duluth Complex apatites: Age reference material for LA–ICP–MS‐based fission‐track dating     

Hideki Iwano  Tohru Danhara  Takashi Yuguchi  Takafumi Hirata  Masatsugu Ogasawara 《地学学报》2019,31(3):247-256

Anorthositic series apatites of the Duluth Complex, Minnesota, USA, have high spontaneous fission‐track densities of up to ~10⁷ cm^–2 and a homogeneous age of ~900 Ma, allowing high‐precision fission‐track dating based on LA–ICP–MS U analysis. Absolute fission‐track dating, track‐length measurement and chemical composition analysis were performed to evaluate a cooling history, which is essential for age reference materials. Preliminary inverse modelling for a sample with a shortened track‐length distribution yielded a monotonic cooling history from ~100°C at 925 Ma. The apatites incur an over‐etching problem when employing the commonly used etching protocol involving 5.5 M HNO₃.  相似文献   

Northward cooling of the Kuncha nappe and downward heating of the Lesser Himalayan autochthon distributed to the south of Mt. Annapurna,western central Nepal     

Toru Nakajima  Harutaka Sakai  Hideki Iwano  Tohru Danhara  Takafumi Hirata 《Island Arc》2020,29(1)

We investigated the tectonothermal history of the Lesser Himalayan sediments (LHS), which are tectonically overlain by the Higher Himalayan Crystalline. Fission‐track dating and the track length measurement of detrital zircons obtained from the Kuncha nappe and the Lesser Himalayan autochthonous sediments in western central Nepal revealed northward cooling of the nappe and possible downward heating of the autochthon by the overlying hot nappe. Nine zircon fission‐track (ZFT) ages of the nappe showed northward‐younging linear distribution from 11.6 Ma in the front at Tamghas, 6 Ma in the central at Naudanda, and 1.6 Ma in the northernmost point at Tatopani. Thermochronological invert calculation of the ZFT length elucidated that the Kuncha nappe gradually cooled down (30 °C/Myr) at the front and rapidly cooled down (120 °C/Myr) at the root zone. In contrast, the ZFT age of the Chappani Formation, located just beneath the Kuncha nappe in the central part, demonstrated a totally reset age of 6.8 Ma, whereas the Virkot Formation, structurally far from the nappe, yielded a partially reset age of 457.3 Ma. This suggests that the LHS underwent downward heating, resulting in a thermal print on the upper part of the LHS; however, the thermal effect was not sufficient to anneal ZFT totally in the deeper part. Presently, the nappe cover is eroded and denuded from this area. Detrital zircons from the Chappani Formation in Tansen area to the south of the Bari Gad Fault did not show any evidence of annealing, suggesting that nappe never covered the LHS distributed to the south of the fault.  相似文献   

Subduction–accretion–collision history along the Gondwana suture in southern India: A laser ablation ICP-MS study of zircon chronology     

Kei Sato  M. Santosh  Toshiaki Tsunogae  T.R.K. Chetty  Takafumi Hirata 《Journal of Asian Earth Sciences》2011,40(1):162-171

We report the petrological characteristics and preliminary zircon geochronology based on laser ablation ICP mass spectrometry of the various units in an accretionary belt within the Palghat-Cauvery Shear/Suture Zone in southern India, a trace of the Cambrian Gondwana suture. Zircons extracted from a plagiogranite in association with an ophiolite suite within this suture possess internal structure that suggests magmatic crystallization, and yield mid Neoproterozoic ²⁰⁶Pb/²³⁸U age of 817 ± 16 Ma (error: 1σ) constraining the approximate timing of birth of the Mozambique Ocean floor. Compiled age data on zircons separated from a quartzite and metamorphosed banded iron formation within the accretionary belt yields a younger intercept age of 759 ± 41 Ma (error: 1σ) which we relate to a mid Neoproteozoic magmatic arc. Detrital zircons extracted from the quartzite yield ²⁰⁷Pb/²⁰⁶Pb age peaks of about 1.9–2.6 Ga suggesting that they were sourced from multiple protolithis of Neoarchean and Paleoproterozoic. Metamorphic overgrowths on some zircon grains record ca. 500–550 Ma ages which are in good harmony with the known ages for the timing of high-grade metamorphism in this zone during the final stage of continent collision associated with the birth of the Gondwana supercontinent in the latest Neoproterozoic-Cambrian. The preliminary geochronological results documented in our study correlate with the subduction–accretion–collision history associated with the closure of the Mozambique Ocean and the final amalgamation of the Gondwana supercontinent.  相似文献   

Groundwater use in developing cities: policy issues arising from current trends   总被引：1，自引：0，他引：1  

Stephen D. Foster  Ricardo Hirata  Ken W. F. Howard 《Hydrogeology Journal》2011,19(2):271-274

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Progressive changes in lithological association of the Sanbagawa metamorphic complex,Southwest Japan: Relict clinopyroxene and detrital zircon perspectives          下载免费PDF全文

Shunsuke Endo  Kazuhiro Miyazaki  Tohru Danhara  Hideki Iwano  Takafumi Hirata 《Island Arc》2018,27(5)

The main tectono‐stratigraphic unit (Shirataki unit) of the Sanbagawa metamorphic complex in central Shikoku is characterized by abundant mafic schist layers that show the mid‐ocean ridge basalt (MORB) affinity. These MORB‐derived schist layers are absent in a southern (structurally lower) domain within the unit. Instead, sporadic occurrences of small metabasite lenses that contain relict igneous minerals (Ti‐rich augite and kaersutite) indicative of alkali basalt magmatism are newly recognized in the southern domain. Compositions of relict clinopyroxene in metabasalt are useful to identify the tectonic setting and origin of the protolith basalt, and those in each unit of the Sanbagawa metamorphic complex are presented. The metamorphic grade of the Shirataki unit generally increases structurally upwards in the southern side of the highest‐grade zone, and metamorphic zonation is subparallel to lithostratigraphic succession. The protolith assemblage of the Shirataki unit shows a distinct change from the southern low‐grade domain (lower Shirataki subunit) composed of terrigenous sedimentary rocks (mudstone and sandstone) with minor alkali basalt to the northern higher‐grade domain (upper Shirataki subunit) consisting of terrigenous and pelagic sedimentary rocks with abundant MORB. The youngest detrital zircon U–Pb ages (ca 95–90 Ma) suggest that both domains have Late Cretaceous depositional ages at the trench. Progressive peeling of oceanic plate stratigraphy during subduction can account for the observed change of lithological association in the Shirataki unit.  相似文献   

Northward younging zircon fission‐track ages from 13 to 2 Ma in the eastern extension of the Kathmandu nappe and underlying Lesser Himalayan sediments distributed to the south of Mt. Everest     

Toru Nakajima  Harutaka Sakai  Hideki Iwano  Tohru Danhara  Takafumi Hirata 《Island Arc》2020,29(1)

This study is concerned with the tectono‐thermal history of the Kathmandu nappe and the underlying Lesser Himalayan sediments (LHS) that are distributed in eastern Nepal. We carried out zircon fission‐track(ZFT) dating and obtained 16 ZFT ages from the eastern extension of the Kathmandu nappe, the Higher Himalayan Crystalline, Kuncha nappe, and the Main Central Thrust (MCT) zone. The ZFT ages of the frontal part of the Kathmandu nappe range from 13.0 ±0.8 Ma to 10.7 ±0.7 Ma and exhibit a northward‐younging tendency. These Middle Miocene ZFT ages indicate that the frontal part of the Kathmandu nappe remained at a temperature above 240 °C until the termination of its southward emplacement at 12–11 Ma. The ZFT ages of the LHS range from 11.1 ±0.9 Ma in the southern part of the Okhaldhunga Window to 2.4 ±0.3 Ma of the augen gneiss in the northern margin and also exhibit a northward‐younging age distribution. The ZFT ages show the northward‐younging linear distribution pattern (?0.16 Ma/km) along the across‐strikesection from the frontal part of the Kathmandu nappe to the root zone, without a significant age gap. This distribution pattern indicates that the Kathmandu nappe, the underlying MCT zone, and the Kuncha nappe cooled from the frontal zone to the root zone as a thermally united geologic body at a temperature below 240 °C. An older ZFT age (456.3 ±24.3 Ma), which was partially reset at the axial part of the Midland anticlinorium in the central part of the Okhaldhunga Window, was explained by downward heating from the “hot” Kathmandu nappe. The above evidence supported a model that southward emplacement of the hot Kathmandu nappe resulted in a thermal imprint on the upper part of the LHS; however, the lower part did not reach 240 °C.  相似文献   

Spheroidal weathering of granite porphyry with well‐developed columnar joints by oxidation,iron precipitation,and rindlet exfoliation          下载免费PDF全文

Yasuto Hirata  Masahiro Chigira  Youqing Chen 《地球表面变化过程与地形》2017,42(4):657-669

Spheroidal weathering, one of the important rock weathering styles, has been attributed to chemical weathering by the water from joint surfaces, and mechanical aspects of the weathering have not been well addressed. We made an investigation on spheroidal weathering of Miocene granite porphyry with well‐developed columnar joints and found that this spheroidal weathering proceeds through chemical processes and accompanying mechanical processes. The investigation of the textures, physical properties, mineralogy, and chemistry of the porphyry revealed the presence of a brown band on the surface margins of corestones, representing the oxidation of pyrite and chlorite, and the precipitation of iron hydroxides, and the consequent generation of micro‐cracks within the band. During weathering, oxidation progresses inwards from joints that surround the rindlets, including both high‐angle columnar and low‐angle planar joints, and causes rounding of the unweathered interior portion of the rock. Microscopic observations of the brown band embedded with fluorescent resin show that pores are first filled with iron hydroxides, and that micro‐cracks then form parallel to the oxidation front in the outer portion of the brown band. Iron hydroxide precipitation increases the P‐wave velocity in the brown band, while micro‐crack formation decreases the tensile strength of the rock. Where the brown band has thickened to ~6 cm, the micro‐cracks are connected to one another to create continuous cracks, which separate the rindlets from the corestone. Micro‐crack formation parallel to the corestone surface may be attributed to compressive stresses generated by small amounts of volumetric expansion due to the precipitation of iron hydroxides in the brown band. Earth surface is under oxidizing environments so that precipitation of iron hydroxides commonly occurs; the spheroidal weathering in this paper is a typical example of the combination of chemical and mechanical processes under such environments. Copyright © 2016 John Wiley & Sons, Ltd.  相似文献   

Application of laser ablation ICPMS to trace the environmental history of chum salmon Oncorhynchus keta     

Arai T  Hirata T  Takagi Y 《Marine environmental research》2007,63(1):55-66

Trace element levels in otoliths of chum salmon Oncorhynchus keta were examined by means of laser ablation inductively coupled plasma mass spectrometry (LA-ICPMS). A close linear relationship in the Sr:Ca ratios between EPMA (X-ray analysis with an electron microprobe) and LA-ICPMS analyses was found (p<0.0001), suggesting that the latter technique could be used to separate the marine and freshwater life phases. Mg:Ca, Cr:Ca, Zn:Ca and Ba:Ca ratios in either the core region or the oceanic growth zone of the otoliths varied among sites. These differences suggest that elemental compositions may reflect environmental variability among spawning (breeding) or habitat sites. Thus, those element ratios demonstrate the potential to be used to distinguish between fish spawning (breeding) sites and habitats for this species of salmon.  相似文献   

High-reliability zircon separation for hunting the oldest material on Earth: An automatic zircon separator with image-processing/microtweezers-manipulating system and double-step dating     

Yukio Isozaki  Shinji Yamamoto  Shuhei Sakata  Hideyuki Obayashi  Takafumi Hirata  Ken-ichi Obori  Toshinori Maebayashi  Satoshi Takeshima  Toshikazu Ebisuzaki  Shigenori Maruyama 《地学前缘(英文版)》2018,9(4):1073-1083

Despite the recent development in radiometric dating of numerous zircons by LA-ICPMS, mineral separation still remains a major obstacle, particularly in the search for the oldest material on Earth. To improve the efficiency in zircon separation by an order of magnitude, we have designed/developed a new machine-an automatic zircon separator(AZS). This is designed particularly for automatic pick-up of100 μm-sized zircon grains out of a heavy mineral fraction after conventional separation procedures. The AZS operates in three modes:(1) image processing to choose targeted individual zircon grains out of all heavy minerals spread on a tray,(2) automatic capturing of the individual zircon grains with microtweezers, and(3) placing them one-by-one in a coordinated alignment on a receiving tray. The automatic capturing was designed/created for continuous mineral selecting without human presence for many hours. This software also enables the registration of each separated zircon grain for dating, by recording digital photo-image, optical(color) indices, and coordinates on a receiving tray. We developed two new approaches for the dating; i.e.(1) direct dating of zircons selected by LA-ICPMS without conventional resin-mounting/polishing,(2) high speed U-Pb dating, combined with conventional sample preparation procedures using the new equipment with multiple-ion counting detectors(LA-MIC-ICPMS).With the first approach, Pb-Pb ages obtained from the surface of a mineral were crosschecked with the interior of the same grain after resin-mounting/polishing. With the second approach, the amount of time required for dating one zircon grain is ca. 20 s, and a sample throughput of 150 grains per hour can be achieved with sufficient precision(ca. 0.5%).We tested the practical efficiency of the AZS, by analyzing an Archean Jack Hills conglomerate in Western Australia with the known oldest(4.3 Ga) zircon on Earth. Preliminary results are positive; we were able to obtain more than 194 zircons that are over 4.0 Ga out of ca. 3800 checked grains, and 9 grains were over 4300 Ma with the oldest at 4371 ± 7 Ma. This separation system by AZS, combined with the new approaches, guarantees much higher yield in the hunt for old zircons.  相似文献   

Estimation of the <Emphasis Type="Italic">in situ</Emphasis> Ultraviolet-A absorption of seawater by a simple irradiance inversion model     

Takafumi Hirata 《Journal of Oceanography》2008,64(4):561-566

An irradiance inversion model to estimate the in situ absorption coefficient of seawater has been developed for the Ultraviolet-A (UVA) wavelength domain. Input parameters are sun angle and the up-and downward planar irradiances measured for at least two depths. The present method does not require seawater to be sampled, and is a discrete wavelength method which returns the absorption coefficient at a given wavelength from the irradiances measured at that wavelength without assuming a spectral shape of any optical properties a priori. Comparison between the model results and spectrophotometric measurements shows that the model is practically useful when cloud cover in the atmosphere is ≤ 50%. According to the present method, measurements of the irradiances enable simultaneous observation of the in situ underwater UVA radiation level and the absorption capacity of bulk seawater using a radiometer.  相似文献