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The more sensitive an analysis method the more care must be given to sample preparation. Solid phase extraction (SPE) onto RP 18 phases has established itself as a general purification and enrichment technique for trace components in aqueous samples. Various factors may thereby influence the recovery rate. For example, the ratio amount of sorbent and sample volume should be taken into account to avoid breakthrough of the investigated substance. Extracting phenylurea herbicides from drinking water, the ratio should be 1 g RP 18 sorbent per 1 L water sample. Concerning the flow rate for the fungicides procymidone, vinclozolin, and iprodione, the recovery rate decreases using higher flow rates than 3 or 6 mL/min. In the case of phenylurea herbicides, a flow rate of 10 or 14 mL/min showed best results. Even the coefficient of variation is below ± 5% at these flow rates. Furthermore, the company dependence should be considered because the recovery rate might differ by up to 40% using the nominally identical material. The same applies to the batch dependence of quality from the same company. The concentration of the eluate must also be monitored and carried out with great care to avoid decreasing the recovery rate. Considering these factors of influence, SPE is a very useful tool in sample preparation, particularly if an automated system is used. 相似文献
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介绍了美国API规范的内容，并将南加利福尼亚和中国渤海海域地震活动特征与地震危险性进行对比. 对比结果表明，无论在地震活动的频度与强度还是地震危险性分析结果上，渤海都比南加州弱. API规范指出，对于南加利福尼亚地区的永久性建筑， 强度设计水准取重现期200 a，变形设计水准取几百至几千年. 我国相关规范规定的海洋平台强度设计和变形设计水准分别取500 a和10 000 a，过于保守. 同时，与其它建构筑物的抗震水平相比较，甲类建筑变形设计水准取设计基准期100 a内超越概率2%~3%，乙、丙类取50 a内2%~3%，考虑海洋平台易于引起严重的次生灾害，变形设计水准取设计基准期30 a内1%（相当于重现期3 000 a）应是安全的. 基于上述对比分析， 同时考虑到经济承受能力以及与现行标准的连贯性， 建议我国海洋石油平台的强度设计水准和变形设计水准分别取200 a和3 000 a. 相似文献
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Introduction Offshore platform is the main facility for exploitation of ocean resources, e.g. oil and gas. Nearly 6 000 platforms have been built in the world, 100 among them in China, another 100 will be erected in China in the coming 5 years. The current aseismic design code commonly used in the world is RP2A-WSD based on the seismic hazard zone in the coastal waters of the United States, which is compiled by American Petroleum Institute (American Petroleum Institute, 2002). No specif… 相似文献
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Ecosystem-based marine spatial management: Review of concepts, policies, tools, and critical issues 总被引：1，自引：0，他引：1
Stelios Katsanevakis Vanessa Stelzenmüller Andy South Thomas Kirk Sørensen Peter J.S. Jones Sandy Kerr Fabio Badalamenti Christos Anagnostou Patricia Breen Guillem Chust Giovanni D’Anna Mike Duijn Tatiana Filatova Fabio Fiorentino Helena Hulsman Kate Johnson Aristomenis P. Karageorgis Ingrid Kröncke Simone Mirto Carlo Pipitone Susan Portelli Wanfei Qiu Henning Reiss Dimitris Sakellariou Maria Salomidi Luc van Hoof Vassiliki Vassilopoulou Tomás Vega Fernández Sandra Vöge Anke Weber Argyro Zenetos Remment ter Hofstede 《Ocean & Coastal Management》2011,54(11):807-820
Conventional sectoral management and piecemeal governance are considered less and less appropriate in pursuit of sustainable development. Ecosystem based marine spatial management (EB-MSM) is an approach that recognizes the full array of interactions within an ecosystem, including human uses, rather than considering single issues, species, or ecosystem services in isolation. Marine spatial planning and ocean zoning are emerging concepts that can support EB-MSM. EB-MSM is driven by high-level goals that managers aim to achieve through the implementation of measures. High-level goals and objectives need to be translated into more operational objectives before specific targets, limits and measures can be elaborated.Monitoring, evaluation and adaptation are necessary to ensure that marine management measures are both effective and efficient. Solid monitoring frameworks are the foundation of adaptive management, as they provide the necessary information to evaluate performance and the effectiveness of management actions. Marine protected areas (MPAs) - possibly set up in networks - constitute a key component in EB-MSM policies and practises and have been applied as a cornerstone in conservation of marine biodiversity, management of fish populations, development of coastal tourism, etc. Moreover, MPA experiences have provided methods and concepts (such as zoning) to a wider EB-MSM context. The assignment of values to biophysical features of the marine environment allows the direct assessment of related management choices and may assist EB-MSM.A range of monetary valuation techniques have been proposed to reduce attributes of goods and services to a single metric. However, in the marine environment such an approach is often over simplistic, and thus less reductive techniques may be necessary. Rather than producing a single metric, the results of non-monetary assessments guide policy allowing weight to be given as necessary to potential areas of conflict and consensus.Strategies to take into account climate change effects and geohazard risks in EB-MSM have been applied or proposed worldwide. EB-MSM regimes must be alert to such risks and flexible to account for changes. 相似文献
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The primary degradation of a technical nonylphenol ethoxylate surfactant with an average chain length of 10 ethoxylate units (NPEO‐10) was studied in a flow‐through system by means of miniaturized biofilm reactors (mBFR) with bacteria from an activated sludge plant. 5 mg/L of the test compound (total EO concentration) were spiked in synthetic wastewater (SWW) and fed to the reactors continuously for 64 days. Compound removal and the formation of degradation products (DP) were monitored under both oxic and anoxic conditions. Solid‐phase extraction and RP‐HPLC with fluorescence detection were employed for sample preparation and analysis. Better removal of the parent compound was seen with the oxic reactors (50 to 70%) than with the anoxic reactors (30 to 50%). Compared to SWW organic matter, the test compound proved to be of refractory nature. The appearance of degradation products in the effluent was earlier with anoxic reactors despite their lower elimination efficiency. After extraction of biomass only minor amounts of NPEO‐10 and metabolites were found, indicating that small amounts were present in adsorbed or intracellular form. Ultimate biodegradation of NPEO‐10 and of octylphenol ethoxylates (OPEO‐9.5; average chain length of 9.5 EO units) was tested by means of manometric respirometry at a theoretical oxygen demand (ThOD) of 100 mg/L. Whereas NPEO‐10 was biodegraded by only 26%, at best, in 28 days, OPEO‐9.5 degradation amounted to (40 ± 5)%. 相似文献
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Use of remote sensing and GIS to determine recharge potential zones: the case of Occidental Lebanon 总被引：3，自引：1，他引：3
Water recharge from land surfaces into subsurface media is an essential element in the hydrologic cycle. For a small-scale assessment, experimental approaches are usually followed, however, on a regional scale, this assessment needs to be made into a comprehensive picture where spatial data of the different contributing factors are treated. The case of Occidental Lebanon, with an area of around 5,000 km2, was studied by the integration of all factors influencing this hydrologic process. Contributing factors are: lineaments and drainage frequency density, lithologic character, karstic domains and land cover/land use. The determination of these factors was carried out mainly by the application of remote sensing. Satellite images (Landsat 7 ETM &; SPOT) and aerial photos were subjected to several treatment processes using a miscellany of software, mainly ERDAS Imagine and ESRI’s Arc View software. Furthermore, exogenetic data, such as topographic and geologic maps, were utilized. The extracted information for these factors was plotted on maps. The integration of the maps in a GIS allowed deciding their interactive effects. However, each factor had its own degree of effect, i.e., weight, which was also determined in this study. This study is an approach to better estimate and provide qualitative assessments of recharge potential (RP). The resultant map shows the highest recharge potentials towards the elevated regions where karstification is well development. It was found that around 57% of the study area is terrain with very high to high recharge rate values, which a considerable amount of precipitated water is allowed to percolate into subsurface rocks. 相似文献
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The reductive amination of low‐molecular‐weight saccharides, uronic acids, and amino sugars, followed by a separation of the derivates by means of ion‐pair chromatography or RP‐HPLC, offers an interesting alternative to HPAEC‐PAD for the environmental analysis of these compounds. Under this aspect various potential amination reagents, i.e., p‐amino‐benzoic acid (p‐AMBA), p‐AMBA propyl ester, 1‐aminopyrene, 2‐(2‐aminophenyl)indole, and 4‐aminoazobenzene, were tested with regard to the formation of derivates and to the chromatographic properties of the formed derivates. p‐AMBA, p‐AMBA propyl ester and 4‐aminoazobenzene proved to be especially suited, because they facilitate the amination of all carbohydrate reference components together with a complete separation and sensible detection (detection limits < 0.5 mg/L) of the derivates. Mainly the following elution sequence was ascertained: amino sugars (hexosamines) / disaccharide(s) / monosaccharides (hexoses) / hexuronic acid(s) / N‐acetyl‐D‐glucosamine. Detection limits down to 0.1 μmol/L were realized using p‐AMBA as reagent, facilitating the determination of the target compounds in landfill leachates and lysimeter percolates. Applying the p‐AMBA propyl ester for derivatization, chromatographic interferences with weakly retained derivates and the coelution of the reagent with its galactosamine derivate can be avoided, since the ester elutes after its derivates unlike p‐AMBA itself. 相似文献
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ABSTRACT Karst aquifers and springs are important with respect to their potential for supplying drinking water in regions suffering from water scarcity in Iran. Accordingly, it is essential to determine the recharge potential of the catchment and the regions with higher obtainability potential. This study provides a road map for the Sheshpeer catchment in southern Iran. A recharge potential (RP) map was produced from which a recharge index (RI) was computed for several selected springs in the catchment. Furthermore, the unit discharge (q) – defined as the average annual discharge for a given catchment area and unit rainfall depth for each spring – was calculated. The plot of q versus RI for the springs showed a linear positive relationship between the two variables (R 2 = 0.9). Applying the trend equation of this plot to the whole Sheshpeer karstic catchment reveals that its long-term recharge coefficient is 0.74. 相似文献