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1.
A method was developed for the determination of organic halogens in water samples with the aim of minimizing matrix effects and simplifying the sample preparation technique commonly used. The method is based on the adsorption of organic halogens in modified hydrophilic divinylbenzene polymer columns and their elution with methanol. The adsorbent used enables rapid adsorption and desorption due to comparatively high operating flow rates and minimized solvent amounts. Furthermore, no additional reconcentration steps are needed. The methanol extract obtained is combusted with a standard EOX (extractable organic halogen) analyzer and the concentration of organically bound halogens is determined by microcoulometric analysis. The matrix effects are considerably reduced compared to the standard procedure (EN 1485) commonly used. A detection limit of 13 μg/L was established. 相似文献
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Immediately after the flood event in summer 1997 at the Odra river, samples of flood sediments were taken for a complex phase analysis. The realized investigations show that the sampled flood sediments are very inhomogeneous. The main reasons for this substantial condition are surely different states of flow during the flood event. It is possible to characterize the investigated material as middle to fine sands with variable phase compositions. The mineral content of the fraction <2 μm shows a complex composition of amorphous matter, quartz, feldspars, and a different composed clay mineral matter. A high distribution of several mixed layers in the clay mineral phase is detectable. Within the scope of the taken analyses the following minerals were detected: kaolinite (disordered), kaolinite/smectite-mixed layer, chlorite/smectite-mixed layer, montmorillonite, illite/smectite-mixed layer, celadonite. The investigation of the heavy fraction shows heavy minerals and heavy particles of different geneses. Mainly these are geogenic, transparent heavy minerals like zircon, amphibole, garnet, pyroxene, apatite, rutile, and epidote. Furthermore there were analysed geogenic, opaque heavy minerals (magnetite and ilmenite), anthropogenic, opaque heavy particles (fly ashes and slags), and biogenic components (pyrite framboids). The substantial character of the investigated flood sediments (e.g. content of organic matter, content of clay minerals) shows that this material is able to act as a fixation medium of contaminants. 相似文献
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Driss Khattach Hamid Mraoui Driss Sbibih Touria Chennouf 《Comptes Rendus Geoscience》2006,338(8):521-526
The multiscale wavelet analysis has been applied to the gravity data from northeastern Morocco to map the major geological contacts, such us faults. Hence, the faults affecting the survey area were outlined with their importance level and dip direction. Seismic data confirm these results and testify the efficiency of this method, particularly in studying structure of plains. The structural map established is a very useful document in the planning of natural resources investigations (i.e. water, mines) to be undertaken in the area of study. To cite this article: D. Khattach et al., C. R. Geoscience 338 (2006). 相似文献
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福建省仙游2013年ML5.0级地震是福建该省年度内发生的最大地震事件。在地震监测以及精定位的基础上,从地震序列、震源深度和震源机制解等方面做了统计分析,并依据震区地质构造图,分析了地面流动重力反映的不同构造部位深部物质的变化及其与断裂构造和地应力的关系,最后从断面凸破模型分析了地震发生的机理,并与地球物理及震源机制解进行相互验证。 相似文献
5.
本文通过武育粳3号的播期试验研究,利用生育期的试验资料,结合本地的温光资源,建立其温光模式,从中分析该品种有感温性强,感光性弱的特性,在本地区应采用稀播长秧龄等配套措施,确保在安全齐穗期内齐穗,达到高产的目的。 相似文献
6.
Syn-orogenic extension in the Peloritani Alpine Thrust Belt (NE Sicily,Italy): Evidence from the Alì Unit 总被引：1，自引：0，他引：1
Structural and petrological analyses on the Alì Unit, in the Peloritani Thrust Belt, document the first evidence for Alpine exhumation associated with syn-orogenic extension in this part of the Calabria-Peloritani Arc. The Alì Unit displays ductile structures occurred during three Alpine deformation phases (Da1, Da2, Da3). Da1 and Da3 developed in a contractional context, whereas Da2 was generated in an extensional regime. The present-day tectonic contact between the Alì Unit and the overlying Mandanici Unit is interpreted as a low-angle extensional detachment responsible for the metamorphic break between the two units. Structural overprinting relationships indicate that the development of Da2 structures and related tectonic exhumation occurred during syn-convergence extension, and were followed by further nappe stacking in the Peloritani Belt. To cite this article: R. Somma et al., C. R. Geoscience 337 (2005). 相似文献
7.
Nearshore crescentic bars play a key role in nearshore morphodynamics. These bars are observed all along the Aquitanian Coast, with a mean wavelength of about 700 m. A non-linear stability analysis is undertaken to simulate the development of crescentic patterns. Results show that self-organization mechanism can lead alone to the development of these alongshore rhythmic features. Simulated wavelengths are in agreement with observations on the Aquitanian Coast. To cite this article: B. Castelle et al., C. R. Geoscience 338 (2006). 相似文献
8.
The contents of Ni and Cr in sewage sludge with high and low amounts of heavy metals were investigated by polarography. The DIN-digestion (aqua regia) was used, and the resulting solution was treated with H2O2/UV (90 °C, 60 min) for further destroying of the organic material. Besides, the solution of the DIN-digestion was examined with AAS (flame) and ICP-OES. With the determination of Ni it was shown that after digestion with aqua regia no further treatment with H2O2/UV is necessary. Contrariwise it was found that for the determination of Cr a H2O2/UV photolysis is necessary followed by further steps to get good agreement with AAS and ICP results as well as with the certified values of a sludge of the Community Bureau of Standards. 相似文献
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10.
Fatiha Laoufi Ahmed-Hafid Belbachir Noureddine Benabadji Abdelouahab Zanoun 《Comptes Rendus Geoscience》2011,343(10):653-663
We have mapped the region of Oran, Algeria, using multispectral remote sensing with different resolutions. For the identification of objects on the ground using their spectral signatures, two methods were applied to images from SPOT, LANDSAT, IRS-1 C and ASTER. The first one is called Base Rule method (BR method) and is based on a set of rules that must be met at each pixel in the different bands reflectance calibrated and henceforth it is assigned to a given class. The construction of these rules is based on the spectral profiles of popular classes in the scene studied. The second one is called Spectral Angle Mapper method (SAM method) and is based on the direct calculation of the spectral angle between the target vector representing the spectral profile of the desired class and the pixel vector whose components are numbered accounts in the different bands of the calibrated image reflectance. This new method was performed using PCSATWIN software developed by our own laboratory LAAR. After collecting a library of spectral signatures with multiple libraries, a detailed study of the principles and physical processes that can influence the spectral signature has been conducted. The final goal is to establish the range of variation of a spectral profile of a well-defined class and therefore to get precise bases for spectral rules. From the results we have obtained, we find that the supervised classification of these pixels by BR method derived from spectral signatures reduces the uncertainty associated with identifying objects by enhancing significantly the percentage of correct classification with very distinct classes. 相似文献