气相色谱-质谱法初步鉴定不同品质的麝香     

汪雨  刘聪  陈舜琮  武彦文 《岩矿测试》2011,30(1):59-62

通过气相色谱-质谱法对不同麝香样品乙醇提取物进行初步定性分析,以判断不同麝香样品的品质。结果表明,天然麝香样品中除含有效成分麝香酮外,还含有多种甾类化合物;而几种市售麝香样品中有些仅麝香酮含量较为显著,几乎不含甾类化合物,其他物质为高级脂肪酸(酯)。通过乙醇提取气相色谱-质谱法可简单、快速、有效鉴定不同麝香的品质。  相似文献   

Occurrence and accumulation features of polycyclic aromatic hydrocarbons and synthetic musk compounds in finless porpoises (Neophocaena phocaenoides) from Korean coastal waters     

Moon HB  An YR  Park KJ  Choi SG  Moon DY  Choi M  Choi HG 《Marine pollution bulletin》2011,62(9):1963-1968

Reports of the occurrence and accumulation patterns of polycyclic aromatic hydrocarbons (PAHs) and synthetic musk compounds (SMCs) in marine mammals are scarce. In this study, the concentrations and accumulation profiles of PAHs and SMCs were determined in blubber from finless porpoises in Korean coastal waters. Total concentrations of PAHs and SMCs ranged from 6.0 to 432 (mean: 160) ng/g lipid weight and from 17 to 144 (mean: 52) ng/g lipid weight, respectively. Residue levels of PAHs were lower than those reported from other studies, while residue levels of SMCs were relatively higher than those reported in other studies. Naphthalene was the most abundant PAH and HHCB was the dominant SMC observed in finless porpoises. The concentrations of PAHs and SMCs were not correlated with each other, but were significantly correlated within the same chemical groups. No correlations were found between body size and residue levels of PAHs and SMCs.  相似文献