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橡胶砂作为一种廉价环保的土工材料，应用前景十分广阔，关于其力学特性的研究具有重要意义。采用弯曲–伸缩元法对橡胶砂进行了剪切波和压缩波联合测试，分别采用离散频率扫描法和初达波法确定了剪切波和压缩波的传播时间，进而得到其弹性动力学参数：初始剪切模量、侧限模量和泊松比，分析了橡胶含量和围压对橡胶砂弹性动力学参数的影响。结果表明：在同样围压下，随着橡胶含量的增加，橡胶砂初始剪切模量和侧限模量逐渐减小，初始泊松比逐渐增大；在同样橡胶含量下，随着围压的增大，橡胶砂初始剪切模量和侧限模量逐渐增大，初始泊松比逐渐减小。最后，在此基础上进行了两种因素耦合效应的分析以及相关力学机制的探讨。 相似文献
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经典凯氏定氮法是通过观察消解反应现象来控制温度和时间,对于数量较多的样品同时消解会耗费大量的人力及时间,因此需要采用合理的试验设计方法确定最佳消解温度和时间,以实现批量消解样品,提高分析效率。本文利用响应曲面法对凯氏定氮法中的消解条件进行了优化分析,选择料液比、消解温度和消解时间作为优化因素,研究三因素的不同水平对氮含量测定的影响。通过响应曲面分析得到最优的消解条件为:料液比(g/mL)=0.3∶5,消解温度260℃,消解时间60 min。重复实验结果表明,样品在优化的条件下能够很好地消解,重现性较好;标准物质的氮含量的实验测定值(1310×10-6)与标准值(1300×10-6)基本一致,两者的对数误差绝对值为0.003,方法的准确性高。应用响应曲面试验设计方法,对于评价凯氏定氮法中三个消解条件对氮含量的非线性影响起到了很好的优选作用,能更好地预测实验因素对分析结果的影响趋势,可以准确控制消解温度和消解时间,对于提高分析效率具有实用意义。 相似文献
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Maedeh Galehdar Habibollah Younesi Mojtaba Hadavifar Ali Akbar Zinatizadeh 《洁净——土壤、空气、水》2009,37(8):629-637
In the present study, the effects of initial COD (chemical oxygen demand), initial pH, Fe2+/H2O2 molar ratio and UV contact time on COD removal from medium density fiberboard (MDF) wastewater using photo‐assisted Fenton oxidation treatment were investigated. In order to optimize the removal efficiency, batch operations were carried out. The influence of the aforementioned parameters on COD removal efficiency was studied using response surface methodology (RSM). The optimal conditions for maximum COD removal efficiency from MDF wastewater under experimental conditions were obtained at initial COD of 4000 mg/L, Fe2+/H2O2 molar ratio of 0.11, initial solution pH of 6.5 and UV contact time of 70 min. The obtained results for maximum COD removal efficiency of 96% revealed that photo‐assisted Fenton oxidation is very effective for treating MDF wastewater. 相似文献
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橡胶砂作为轻质、耗能填料在土木工程中有广泛的应用前景,但其强度往往会随橡胶含量的增大而降低。土工格栅常用于对散体材料的加筋补强,研究土工格栅对橡胶砂强度特性的加筋效应具有重要意义。基于三轴压缩试验,对3种不同格栅布置方式（1、2、3层）下的干燥橡胶砂强度特性展开研究,重点考察加筋层数对不同围压（50、100、200 kPa）下、不同配比（0%、10%、20%、30%、40%）橡胶砂的强度参数,如峰值强度、似黏聚力、内摩擦角的影响规律。结果表明：土工格栅加筋橡胶砂的强度参数,包括峰值强度、似黏聚力、内摩擦角,相对于未加筋橡胶砂均有明显提高,提高幅度随土工格栅加筋层数的增加而增大,随着围压的降低而增大;土工格栅对配比为20%橡胶砂的强度加筋效应最为明显;土工格栅加筋橡胶砂的强度参数恢复系数与加筋密度之间呈良好的线性关系;土工格栅加筋橡胶砂的强度特性可由试验所得的经验恢复函数较好地估计。 相似文献
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Palanivel Sathishkumar Kannan Balan Thayumanavan Palvannan Seralathan Kamala‐Kannan Byung‐Taek Oh Susana Rodríguez‐Couto 《洁净——土壤、空气、水》2013,41(7):665-672
Laccase from the white‐rot fungus Pleurotus florida, produced under solid‐state fermentation conditions, was used for the decolorization of reactive dye Remazol Brilliant Blue R (RBBR). RBBR was decolorized up to 46% by P. florida laccase alone in 10 min. In the presence of N‐hydroxybenzotriazole (HBT), the rate of decolorization was enhanced 1.56‐fold. Central composite design of response surface methodology with four variables namely, dye, enzyme, redox mediator concentrations, and time at five levels was applied to optimize the RBBR decolorization. The predicted optimum level of variables for maximum RBBR decolorization (87%) was found to be 52.90 mg L?1 (RBBR), 1.87 U mL?1 (laccase), 0.85 mM (HBT), and 7.17 min (time), respectively. The validation results showed that the experimental value of RBBR decolorization (82%) was close to the predicted one. The disappearance of C–N and C–X groups, and a small shift in N–H groups in Fourier‐transform infra red (FTIR) spectroscopy confirms the degradation of RBBR chromophore by laccase enzyme. The phytotoxicity of RBBR was considerably reduced after the treatment with laccase. RBBR decolorization kinetics; Km and Vmax were calculated to be 145.82 mg L?1 and 24.86 mg L?1 min, respectively. 相似文献
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对7种不同配比的橡胶颗粒-砂混合物（简称橡胶砂）进行了循环单剪试验,得出了4种不同竖向固结压力p下不同配比橡胶砂的动剪模量和阻尼比的变化规律。研究表明：同一固结压力下,橡胶颗粒的增多使得应力-应变曲线明显降低,动剪模量衰减,阻尼比和隔震消能能力提高;同一配比下,橡胶砂的应力-应变曲线和动剪模量随固结压力的增大而增大,而阻尼比则随着固结压力的增大略有降低;橡胶颗粒含量的增加,会使得动剪模量归一化 曲线衰减更早,更有利于橡胶砂的隔震应用;与已有研究的对比分析表明,该试验结果与已有文献的试验结果吻合良好,橡胶砂混合物的动剪模量和阻尼比受试验方法的影响不大。 相似文献
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RSM仪与场地剪切波波速测试技术 总被引：2，自引：1，他引：2
介绍了采用检层法进行场地剪切波波速测试的技术和应用以及这种方法的原理、发展历史、测试技术和计算方法。本文还简要介绍了ＲＳＭ的设备和软件以及作者的现场实测经验 相似文献
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Interval complete quadratic combination rule for the response spectrum analysis of buildings with accidental eccentricity 
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下载免费PDF全文 The accidental torsion, caused by several sources of structural uncertainties, gets the elastic response of a building different from that computed. To take into account of these uncertainties, building codes impose the introducing in every storey of the buildings an artificial eccentricity, called accidental, as a fraction of the plan dimension. Because, according to building codes, the accidental eccentricity can mathematically be expressed as a modification of the mass matrix, it follows that each mass modifications require new dynamic analyses that could be cumbersome from a numerical point of view. This paper proposes a new combination rule to obtain in closed form the maximum responses of structures with mass modification by the response spectrum analysis (RSA) without solving any further eigenproblem. In particular, the proposed procedure, based on the application to the RSA of the interval perturbation method, leads to an extension of the classical complete quadratic combination rule to the analysis of structural systems with uncertain‐but‐bounded parameter. In particular, for structural systems with accidental eccentricity, the proposed approach allows to directly evaluate the worst condition for the structural elements with a single RSA. This very remarkable result is obtained by adopting a new modal combination rule, here called interval complete quadratic combination. Numerical results evidence a very good accuracy of the interval complete quadratic combination for single‐storey buildings as well as for the analyzed multistorey buildings. Copyright © 2014 John Wiley & Sons, Ltd. 相似文献