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火焰原子吸收光谱法测定天青石中锶
引用本文:邢谦,谢海东,董迈青.火焰原子吸收光谱法测定天青石中锶[J].岩矿测试,2008,27(4):313-315.
作者姓名:邢谦  谢海东  董迈青
作者单位:青海省岩矿测试应用研究所,青海,西宁,810008
摘    要:将天青石试样经混合熔剂熔融,使锶转化为碳酸盐,水提取,过滤分离硫酸根离子,沉淀用盐酸溶解,加入聚乙醇,加热煮沸,稀释至一定体积。分取部分溶液于0.4mol/L硝酸介质中,加镧盐为释放剂,原子吸收光谱法(空气-乙炔火焰方式)测定氧化锶。方法适用于天青石中w(SrO)≤50%氧化锶的测定。

关 键 词:原子吸收光谱法  天青石  

Determination of Strontium in Celestite Sample by Flame Atomic Absorption Spectrometry
XING Qian,XIE Hai dong,DONG Mai qing.Determination of Strontium in Celestite Sample by Flame Atomic Absorption Spectrometry[J].Rock and Mineral Analysis,2008,27(4):313-315.
Authors:XING Qian  XIE Hai dong  DONG Mai qing
Institution:(The Rock and Mineral Test Application Research of Qinghai,Xining 810008,China)
Abstract:Celestite sample was decomposed by mixed flux and strontium in the sample was converted into strontium carbonate.The fusion disc was leached using water and the solution was filtered for separating SO2-4.The precipitant was then dissolved with HCl.After adding polyethylene ethanol the sample solution was heated to boiling and then diluted to the volume.A portion of the solution was taken into a 0.4 mol/L HNO3 medium and lanthanum was added as releasing agent and Sr in the sample solution was determined by flame-AAS.The method is suitable for the determination of Sr in celestite samples with SrO content ≤50%.
Keywords:atomic absorption spectrometry  celestite  strontium
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