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1.
The crystallographic preferred orientation (here referred to as texture) developed in extruded ionic polycrystalline aggregates with the NaCl-structure is studied as a function of extrusion temperature and ionicity of the material. In pure alkali halides and silver chloride a 100111 double fibre texture is found for all extrusion temperatures investigated. In extruded natural rock salt the 100 fibre is replaced by 115 at or below room temperature. The temperature dependence of the intensity of preferred orientation together with microstructural investigations suggest the 100 and 115 components to be primarily due to dynamic recrystallization. The 111 deformation texture agrees with model calculations based on simultaneous slip on both the {110}110 and {100}110 slip systems, generally observed as primary and secondary slip systems in NaCl-type ionic crystals, respectively. Possible applications to the study of the diapirism of salt domes are discussed.  相似文献   

2.
The crystallographic preferred orientations of a series of experimentally deformed fine-grained albite aggregates were measured by synchrotron source X-ray diffraction. Most samples were deformed and extensively recrystallized by low-temperature recrystallization-accommodated dislocation creep. In axial compression as well as simple shear these samples developed weak but distinct crystallographic preferred orientations consistent with intracrystalline slip on {001}<100>; the sheared samples have a marked asymmetry of the <100> maxima with respect to the shear zone boundaries. One sample was axially compressed by solution precipitation creep; it developed a somewhat different but equally strong preferred orientation, perhaps reflecting crystallographic anisotropy in rates of dissolution and growth.  相似文献   

3.
4.
K.R. McClay 《Tectonophysics》1977,40(3-4):T1-T8
The results of dislocation etch pit studies of naturally and experimentally deformed galena single and polycrystals are presented. The etch pitting is simple, inexpensive, rapid and reveals dislocation substructures similar to those found in metals and ceramics. Both {110} < 1 0 > and {100} < 110 > type slip systems have been found in naturally and experimentally deformed galena.  相似文献   

5.
Three samples of gem quality plagioclase crystals of An60 were experimentally deformed at 900 °C, 1 GPa confining pressure and strain rates of 7.5–8.7×10−7 s−1. The starting material is effectively dislocation-free so that all observed defects were introduced during the experiments. Two samples were shortened normal to one of the principal slip planes (010), corresponding to a “hard” orientation, and one sample was deformed with a Schmid factor of 0.45 for the principal slip system [001](010), corresponding to a “soft” orientation. Several slip systems were activated in the “soft” sample: dislocations of the [001](010) and 110(001) system are about equally abundant, whereas 110{111} and [101] in ( 31) to ( 42) are less common. In the “soft” sample plastic deformation is pervasive and deformation bands are abundant. In the “hard” samples the plastic deformation is concentrated in rims along the sample boundaries. Deformation bands and shear fractures are common. Twinning occurs in close association with fracturing, and the processes are clearly interrelated. Glissile dislocations of all observed slip systems are associated with fractures and deformation bands indicating that deformation bands and fractures are important sites of dislocation generation. Grain boundaries of tiny, defect-free grains in healed fracture zones have migrated subsequent to fracturing. These grains represent former fragments of the fracture process and may act as nuclei for new grains during dynamic recrystallization. Nucleation via small fragments can explain a non-host-controlled orientation of recrystallized grains in plagioclase and possibly in other silicate materials which have been plastically deformed near the semi-brittle to plastic transition.  相似文献   

6.
The microstructure and texture in cordierites of a moldanubian gneiss from the Bohemian Massif has been analysed by transmission electron microscopy (TEM) and universal stage in order to get information on the deformation mechanisms and textural development of this rock-forming mineral. Deformation may have taken place at temperatures between about 500° C and 630° C and pressures smaller than about 3 kb. The elongated cordierite xenoblasts show a typical dislocation creep microstructure consisting of subgrain boundaries and free dislocations. The dislocations have [001], [010] and 1/2<110> Burgers vectors. [001] dislocations often have pure screw and edge character the latter type being climb-dissociated on (001). Among the dislocations reactions are common. The main subgrain boundaries observed are (010)[001], {110}[001] and (001)[010] tilt boundaries. Burgers vectors and dislocation line directions reveal (100)[001], (010)[001], (100)[010], {110} 1/2<110> and (001)1/2<110> as activated slip systems. The crystallographic preferred orientation (here referred to as texture) consists of a [001] maximum in the foliation parallel to the mineral lineation. [100] and [010] maxima are perpendicular to it within and normal to the foliation, respectively, with a girdle tendency normal to the lineation. The texture may be explained by simple shear deformation on the {hkO}[001] slip systems with preference of (010)[001].  相似文献   

7.
The internal structure of variety III diamonds (Orlov 1977) was examined by X-ray section topography. The crystal space was found to be divided into six cubic sectors of a face-form of rhombododecahedroid variety III (Shafranovsky 1961). The defect lines on the topographs are the traces of {110} defect planes. It is concluded that separate 〈111〉 fibres are grouped into {110} layers (lamellae). The internal structure of the crystals is characterized by continuous warping of crystal planes and is directly connected with {110} defect planes which are tilt boundaries. Examples of variants of filling cubic sectors are given and their connection with misorientation shown on topographs demonstrated. The characteristic internal structure of variety III diamonds can account for their morphological features and structure-dependent properties; for examples, the cleavage on {110} and {100}.  相似文献   

8.
Microfabrics were analysed in calcite mylonites from the rim of the Pelvoux massif (Western Alps, France). WNW-directed emplacement of the internal Penninic units onto the Dauphinois domain produced intense deformation of an Eocene-age nummulitic limestone under lower anchizone metamorphic conditions (slightly below 300 °C). Two types of microfabrics developed primarily by dislocation creep accompanied by dynamic recrystallisation in the absence of twinning. Coaxial kinematics are inferred for samples exhibiting grain shape fabrics and textures with orthorhombic symmetry. Their texture (crystallographic preferred orientation, CPO) is characterised by two c-axis maxima, symmetrically oriented at 15° from the normal to the macroscopic foliation. Non-coaxial deformation is evident in samples with monoclinic shape fabrics and textures characterised by a single oblique c-axis maximum tilted with the sense of shear by about 15°. From the analysis of suitably oriented slip systems for the main texture components under given kinematics it is inferred that the orthorhombic textures, which developed in coaxial kinematics, favour activity of <10–11> and <02–21> slip along the f and r planes, respectively, with minor contributions of basal-<a> slip. In contrast, the monoclinic textures, which developed during simple shear, are most suited for duplex <a> slip along the basal plane. The transition between the dominating slip systems for the orthorhombic and monoclinic microfabrics is interpreted to be due to the effects of dynamic recrystallisation upon texture development. Since oblique c-axis maxima documented in the literature are most often rotated not with but against the shear sense, calcite textures alone should not be used as unequivocal shear sense indicators, but need to be complemented by microstructural criteria such as shape preferred orientations, grain size estimates and amount of twinning.  相似文献   

9.
The Alpi Apuane region of the Northern Apennines appears to have been deformed within a large-scale, low-angle shear zone with an overthrust sense of movement. The presence of mineral stretching lineations, folds progressively rotated into the X strain direction, and schistosities which intersect the nappe boundaries at small angles suggest that a component of shear strain occurred during the deformation. The strain ratios and orientations on two-dimensional sections have been determined from deformed marble breccias, reduction spots, and oncalites. Data from three or more non-perpendicular, non-principal sections have been combined to determine the finite strain ellipsoids at 33 sites within the shear zone.The finite strains have been separated into components of simple shear (γ), longitudinal strain (λ), and volume change (Δ). Algebraic expressions have been derived and graphs constructed which enable components of γ, γ and Δ, and γ and λ to be determined directly from a knowledge of strain ratio (R) within the shear zone and the angle (θ) between the principal strain direction and the shear zone boundary. The Alpi Apuane data indicate that neither simple shear alone, nor simple shear with volume change can satisfactorily explain the observed strains. Consideration of simple shear plus longitudinal strain leads to a general relationship in which the value of shear increases, and the values of longitudinal strain change along a SW-NE profile across the zone. Integration of the resulting shear strain-distance curves gives a minimum displacement of 4 km within the shear zone. Combination of the finite strains with the total time of deformation known from K/Ar studies leads to average strain rates from 1.4 to 9.6 × 10−15 sec−1.A characteristic flat-ramp-flat geometry initially formed the boundaries of what was later to develop into the overthrust shear zone, and deformation of the underlying crystalline basement is believed to have occurred by ductile shearing. Estimates of 21% crustal shortening for the region suggest that the crustal thickness prior to deformation was approximately 20 km in this part of the Northern Apennines.  相似文献   

10.
Mylonitic gneisses from the Münchberg Massif contain single grains (type I) and polycrystalline aggregates (type II) of garnet displaying a distinct elongation parallel to a macroscopic lineation which is interpreted as the result of ductile deformation. Lattice-preferred orientations of quartz (textures) symmetrical to the macroscopic foliation and lineation and the lack of rotational microfabrics indicate that the bulk deformation was pure shear at least during the latest strain increments. Garnet textures measured by EBSD together with microprobe analyses demonstrate that these two structural types of garnet can be related to two different processes of ductile deformation: (1) For the single grains stretching can be attributed to diffusion creep along grain boundary zones (Coble creep). The related mass transfer is indicated by the fact that primary growth zones are cut off at the long faces of the grains while the related strain shadow domains do not show comparable chemical zoning. Pressure solution and precipitation suitable to produce similar structures can be largely ruled out because retrogressive reactions pointing to the presence of free hydrous fluids are missing. (2) For the polycrystalline garnet aggregates consisting of cores grading into fine-grained mantles, dislocation creep and associated rotation recrystallization can be assumed. Continuous lattice rotation from the core to the outer polycrystalline rim allow a determination of the related dominant slip systems which are {100}<010> and equivalent systems according to the cubic lattice symmetry. The same holds for garnets which appear to be completely recrystallized. For this type of fine-grained aggregates an alternative nucleation model is discussed. Due to penetrative dislocation glide in connection with short range diffusion and the resulting lattice rotation, primary growth zones are strongly disturbed.Since for the considered rock unit of the Münchberg Massif peak metamorphic temperatures between 630 and 670 °C can be assumed, this study clearly demonstrates that the inferred processes of ductile garnet deformation can occur not only in HT regimes as often suggested in the literature even if embedded within a matrix of “low-strength” minerals like quartz, feldspars and micas.  相似文献   

11.
We used analogue modelling to investigate the factors controlling tail geometry in porphyroclast systems. Results show that: (1) σ inclusions can develop in both slipping and non-slipping modes, but δ-inclusions only form in the latter. (2) σ inclusions develop when the mantle production rate is constant and the mantle is transected by the separatrix. δ inclusions form when the mantle is initially outside the separatrix and later comes inside this line. (3) In the slipping mode, the wedge-shaped tail of σ-inclusions always has a straight external surface parallel to the shear plane, whereas in the non-slipping mode the external surface is curved inwards (external embayments). (4) Together with earlier theoretical results, σ- and δ inclusions always show stair-stepping of tails when embedded in a viscous matrix under homogeneous simple shear deformation. (5) Maximum stair-stepping occurs in the slipping mode and is at least equal to the inclusion diameter. If our models bear significant similarity to nature, then (i) the straight or curved character of σ-inclusions could mean that they had, respectively, a slipping or non-slipping interface with the surrounding recrystallized matrix, and (ii) δ-inclusions may result from shear deformation under retrogressive metamorphic conditions in thrust systems.  相似文献   

12.
Transmission electron microscopy on natural calcium metatitanate perovskite (dysanalyte) reveals the following twin laws in the orthorhombic (space group Pbnm) phase: reflection twins on the {110} and {112} planes, and 90° rotation twins about the [001] axis (referred to as [001]90° twin). Single crystals that were heattreated and quenched from above 1585 K exhibit a dramatic change in domain structure compared with the starting material and specimens quenched from T < 1470=" k.=" mutually=" perpendicular=" {110}=" and=">90° twins are observed throughout the crystal, forming a cross-hatched domain texture. 1/2[001] antiphase domains, which are very rarely observed in the starting material, also become dominant in the crystal. This change in domain structure is interpreted as due to a structural phase transition in perovskite at a temperature below 1585 K. From the point symmetry elements that describe the twin laws and the translational elements that relate the antiphase domains, the most likely phase near 1585 K is tetragonal with space group P4/mbm. These results are consistent with high-temperature powder X-ray diffraction study. On the other hand, density of the {112} twins is increased significantly in the crystal quenched from 1673 K. Twin domains are either bound by mutually perpendicular {110} and (001) walls, or by {112} walls with {110} twin domains within the polygonal {112} domains. Both twin density variation and domain morphology suggest that the crystal may be cubic at this temperature. Microstructure of a single crystal deformed at 1273 K and 3.5 GPa (within the orthorhombic stability field) is morphologically quite distinct from that of the heat-treated specimens. Dislocations dominate the microstructure and often interact with twin domain boundaries.A National Science Foundation Science and Technology Center  相似文献   

13.
Porphyroclasts of relatively strong minerals in mylonites commonly have an internal monoclinic shape symmetry defined by tails of dynamically recrystallized material. The geometry of a porphyroclast and its tails, called a ‘porhyroclast system’, can serve as a valuable indicator of the sense of vorticity. Porphyroclast systems have been divided into σ- and δ-types on the basis of the geometry of the tails. σ-Types have wedge-shaped recrystallized tails whose median lines lie on opposite sides of a reference plane parallel to the tails and containing the symmetry axis for the system. σ-Types are further subdivided into a σa-types, in which the porphyroclast is isolated in a relatively homogeneous matrix, and σb-types, in which the porphyroclast system is associated with a shear band foliation in the matrix. δ-Types typically have narrow recrystallized tails whose median lines cross the reference plane adjacent to the porphyroclast. Consequently, embayments of matrix material occur adjacent to the porphyroclasts and the tails display characteristic bends.A porphyroclast system in a mylonite develops when the relatively weak dynamically recrystallized grain aggregate in the porphyroclast mantle changes its shape due to non-coaxial flow in the adjacent matrix. This behaviour has been modelled in shear box experiments. Passive marker lines around rigid cylinders embedded in silicone putty were subjected to simple shear. The experiments were modified to simulate a change in recrystallization rate (R) with respect to rate of deformation (γ) by decreasing the diameter of the rigid cylinder during deformation at variable rates. The ratio R/γ appears to be one of the most important factors in determining which porphyroclast system will develop. At high R/γ values, flow of recrystallized material away from the porphyroclast is continuously appended by the production of new grains and wedge-shaped σa-type tails develop. At low R/γ values, relatively few new grains are added to the tails which become thinned and deflected by drag due to the spinning motion of the porphyroclast. In addition, most porphyroclast systems at low shear strains are of σa-type or lack monoclinic symmetry, whereas δ-types are only developed at high shear strain values. Complex porphyroclast systems, characterized by two generations of tails, are observed in many of the natural and model shear zones studied and may form due to fluctuating R/γ. Conditions that allow isolated σa- and δ-type porphyroclast systems to be used as sense of vorticity indicators are: the systems should have a monoclinic shape symmetry; matrix grain size should be small with respect to porphyroclast size; matrix fabric should be homogeneous; deformation history should be simple, and observations should be made on sections normal to the inferred bulk vorticity vector for the mylonite.  相似文献   

14.
A polycrystalline aggregate of anhydrite was deformed in torsion to a maximum shear strain of 8.1 at 700°C and a maximum shear strain rate of 5᎒-3 s-1. The crystallographic preferred orientation (CPO or texture) was investigated as a function of shear strain/shear strain rate in a radial profile from the centre to the edge of the sample. A deformation texture developed at shear strains of 1.5-2 (corresponding to shear strain rates of 1 to 1.3᎒-3 s-1) and reached a stable position relative to the kinematic frame at a shear strain of 3.7 (2.3᎒-3 s-1). Further shear strain only led to a small increase in texture strength but no change in the orientation relative to the kinematic frame. The CPO is very similar to naturally observed textures and can be explained by the activity of the {001}<010> and {012}<121> slip systems. Although independent mechanical data indicate that a change of mechanism from dislocation- to diffusion-controlled creep occurred at a shear strain of approximately 1.5, the texture does not weaken, but rather increases, in strength with higher shear strains.  相似文献   

15.
Transmission electron microscopy (TEM) has been used to investigate deformation microstructures of synthetic stishovite specimens deformed at 14 GPa, 1,300°C. Geometrical characteristics of numerous dislocations have been characterized by dislocation contrast and stereographic analyses in order to identify the easy slip systems of stishovite. TEM data allowed us to characterize the following slip systems: 〈100〉{001}, 〈100〉{010}, 〈100〉{021}, [001]{100}, [001]{110}, [001]{210} and Observation of sub-grain boundaries and scalloped edge dislocations suggest that climb has been activated in the specimens.  相似文献   

16.
我国某细脉浸染型钼矿床内的淡红沸石及其成因   总被引:2,自引:0,他引:2       下载免费PDF全文
杨敏之 《地质科学》1965,6(3):295-302
淡红沸石(Stellerite)是辉沸石族矿物之一种,曾在白令海峡中的苏联铜岛、美国阿拉斯加的朱诺、芬兰和苏联东外贝加尔的一些多金属矿床发现过。前人对淡红沸石着重进行了结晶学和热分析的研究,而对其地质产状和成因以及与有关矿化的关系相对少一些。到目前为止,我国还沒有对淡红沸石进行过报导。  相似文献   

17.
Effect of water and stress on the lattice-preferred orientation of olivine   总被引:6,自引:1,他引:5  
The influence of water and stress on the lattice-preferred orientation (LPO) of olivine aggregates was investigated through large strain, shear deformation experiments at high pressures and temperatures (P = 0.5–2.1 GPa, T = 1470–1570 K) under both water-poor and water-rich conditions. The specimens are hot-pressed synthetic olivine aggregates or single crystals of olivine. Water was supplied to the sample by decomposition of a mixture of talc and brucite. Deformation experiments were conducted up to γ (shear strain)  6 using the Griggs apparatus where water fugacity was up to  13 GPa at the pressure of 2 GPa. The water content in olivine saturated with water increases with increasing pressure and the solubility of water in olivine at P = 0.5–2 GPa was  400–1200 ppm H/Si. Several new types of LPO in olivine are found depending on water content and stress. Samples deformed in water-poor conditions show a conventional LPO of olivine where the olivine [100] axis is subparallel to the shear direction, the (010) plane subparallel to the shear plane (type-A). However, we identified three new types (type-B, C, and E) of LPO of olivine depending on the water content and stress. The type-B LPO of olivine which was found at relatively high stress and/or under moderate to high water content conditions is characterized by the olivine [001] axis subparallel to the shear direction, the (010) plane subparallel to the shear plane. The type-C LPO which was found at low stress and under water-rich conditions is characterized by the olivine [001] axis subparallel to the shear direction, the (100) plane subparallel to the shear plane. The type-E LPO which was found under low stress and moderate water content is characterized by the olivine [100] axis subparallel to the shear direction, the (001) plane subparallel to the shear plane. Observations by transmission electron microscopy (TEM) and scanning electron microscopy (SEM) show that the dislocations in water-poor samples (type-A) are curved and both b =  [100] and b = [001] dislocations have a similar population. Numerous subgrains are seen in water-poor samples in backscattered electron images. In contrast, water-rich samples (both type-B and type-C) contain mostly b = [001] dislocations and dislocations are straight and sub-grain boundaries are rare compared to those in water-poor samples. These observations suggest that (1) dominant slip systems in olivine change with water fugacity (and stress) and (2) grain boundary migration is enhanced in the presence of water. Seismic anisotropy corresponding to the fabrics under water-rich condition is significantly different from that under water-poor condition. Consequently, the relationship between seismic anisotropy and flow geometry in water-rich regions is expected to be different from that in water-poor regions in which type-A fabric dominates (i.e., the lithosphere). A few cases are discussed including anisotropy in the subduction zone and in the deep upper mantle.  相似文献   

18.
直流弧光放电等离子体CVD金刚石薄膜中的晶体类型与特征   总被引:1,自引:0,他引:1  
采用自主研制的直流弧光放电等离子体CVD设备,以甲烷和氢气为气源,在YG6硬质合金基体上制备出主显晶面为(100)、(111)以及纳米晶粒的金刚石薄膜涂层。SEM观测其晶体类型主要为立方体、八面体、立方八面体,其中以立方八面体为主。随着碳源气体浓度的增加,金刚石晶体的形态会呈现从八面体一立方八面体一立方体顺序转变的趋势;而薄膜的表面形貌呈现从主显(111)晶面-(111)与(100)晶面混杂-主显(100)晶面顺序转变的特征。此外,CVD金刚石薄膜中还存在有许多类似接触孪晶、贯穿孪晶、复合孪晶,以及球形或聚晶晶粒形态的晶体,并且多数孪晶属于类似(111)复合孪晶结构。  相似文献   

19.
The structural composition of coal–tar pitch used in the preparation of the special binder-pitch, was determined with special emphasis on the optical properties of the β-resins, as typical components necessary to obtain electrodes of best quality through the pyrogenetic processes of baking and graphitization. In addition to raw toluene- and quinoline-insolubles (TI, QI), the corresponding cokes were analysed to evaluate, by structural composition and microtexture, the behaviour of pitch fractions during carbonization. The results suggest the dependence of the texture development on the type of toluene- and quinoline-insolubles and β-resins during processing conditions, which influence the mesophase formation. An original and important result of the carbopetrographical study is represented by the identification and evaluation of β-resins in the coke texture.  相似文献   

20.
Pyroxenes of pigeonitic and augitic bulk compositions in H3–4 chondritic meteorites commonly exhibit sigmoidal precipitates, rather than the elsewhere common lamellar associations. Most often, submicrometric sigmoids with calcic clinopyroxene composition occur within clinoenstatite; more rarely, clinoenstatite sigmoids occur within calcic clinopyroxene. The sigmoids appear as 001 terminated lamellae, with terminations rotated in opposite directions towards the 100 orientation. Pre-exsolution pigeonite and augite formed at temperatures higher than 980 °C, whereas sigmoidal exsolution occurred between 990 and 830 °C. Local anomalous lattice parameters determined by electron diffraction suggest that lattice parameters are most strained where the exsolution texture is most poorly defined. Shear strain occurs during exsolution due to mismatching lattice parameters and variable angles. In response to shear stress, the lamellae relax and assume sigmoidal strained morphologies. Sigmoidal exsolution is strongly controlled by (100) orthoenstatite stacking faults that possibly trigger exsolution.  相似文献   

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