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1.
Sang-kon Kim Maeng-eon Park Seung-gyun Baek Kyu-youl Sung Sun-ok Kim Hee-yul Park 《世界地质(英文版)》2004,7(2)
Chemical composition, Raman microspectrometry, and Fourier transform infrared (FT-IR) and SEM-CL (Cathodluminescence) analyses are carried out for Tanzania and Madagascar garnets for locality identification. Inclusion study was sustained after electron probe microanalysis (EPMA). Needle-like illmenites, apatites and zircons were the most common solid inclusions in Tanzania garnets. Madagascar garnets revealed rutile needles and apatites were also observed, but differences in size, shape and distribution patterns were noticed compared to Tanzania garnets. Tanzania garnets exhibited all types of observable fluid inclusions such as "fingerprint" pattern, called Type Ⅰ-A, liquid-only (L) single phase fluid inclusion, called Type Ⅰ-B and Type Ⅱ-A (L + S), Type Ⅱ-B (L + V) and Type Ⅲ-A (L + Sylvite +S), Type Ⅲ-B (L+S+V), while no more than two phase fluid inclusions found in both Madagascar and Korea garnets even if all examined garnets from three localities retained "fingerprint" features, so called, partially healed fractures, in common. Chemical composition, Raman microspectrometry and Fourier transform infrared (FT-IR) analysis taken turned out to be useful methods for the purpose of this study. Using consequences of SEM-CL and inclusion study, accordingly,the locality identification of gem-quality garnets is capable of being available in further application for other kinds of gemstones. 相似文献
2.
In this study,the water-based ferromagnetic fluid and magnetic resin made from chitosan and cerium complex(MRCCC) were successfully prepared by using the chemical co-precipitation technique and by the reversed-phase suspension cross-linking polymerization.MRCCC presented uniform and narrow particle size distribution as determined by the Laser Particles Sizer.The Inductively Coupled Plasma-Atomic Emission Spectrometry(ICP-AES),Fourier transform infrared spectroscopy(FT-IR),differential scanning calorimetry(DSC)and X-ray powder diffraction(XRD)study demonstrated that there were iron and cerium existing in MRCCC.The movement of MRCCC under magnetic field proved its magnetic property.The swelling kinetics in water or solutions with different pH indicated that MRCCC could be applied in solutions with pH greater than 1.0.The ferromagnetic fluid particles were stable in MRCCC soaked in solutions with pH >2.0.In view of these results,MRCCC can be used as material for separation,clarification,adsorption,sustained release and hydrolysis activity. 相似文献
3.
Geology and fluid inclusion of Wadi Sharis Neoproterozoic orogenic gold deposits in northwestern Yemen 
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下载免费PDF全文 Moteea A． Al-Shameery 《世界地质(英文版)》2011,14(1):21-28
The Wadi Sharis orogenic gold deposit in northwestern Yemen is related to the fault and shear zones vein at medium depth in the crust in the Neoproterozoic meta-sedimentary and meta-volcanosedimentary succession of greenschist to amphibolite facies metamorphism.Three distinct fluid inclusion types have been identified in the gold-bearing quartz sulphide veins of the deposit:(1) type I:vapour-liquid two-phase(VH2O-LH2O),(2) type II:three-phase CO2(VCO2-LH2O-LCO2) and(3) type III:vapour-rich(LCO2-VCO2) inclusions.Six analysis of individual fluid inclusion indicate the fluid inclusions comprise mainly of H2O and CO2.Formation P-T conditions recorded by fluid inclusions in quartz crystals correspond to 180℃-380℃ and up to 130 MPa,as indicated by high-density CO2 bubbles(up to 0.98 g/cm3) observed in some inclusions.The estimated crystallization pressures correspond to approximately 4-10 km of overburden,assuming a lithostatic load.The salinity ranges from 0 to 22 wt%.The deposit holds at 0.2-5 g/t Au and contains low-moderate salinity. 相似文献
4.
用流延法成功制备壳聚糖/PVA共混膜,并进行湿热处理,用FT-IR、XRD对经过湿热处理共混膜进行了表征,测试了膜的力学性能和吸水性;结果表明,随着湿热处理时间的增长共混膜的无水结晶峰出现并不断增强。共混膜的吸水性实验表明,壳聚糖/PVA共混膜的pH敏感性可通过控制湿热处理的时间来改变,由于湿热处理不需要引入诸如戊二醛等对生物有毒副作用的化学交联剂,所以该法可望在壳聚糖/PVA共混膜控释体系的后处理方面得到应用。 相似文献
5.
通过对储层成岩作用、流体包裹体岩相学和孔隙沥青特征的分析,在烃包裹体期次划分的基础上,结合流体包裹体均一温度特征、烃源岩热演化史、地层埋藏史和储层成岩史,确定了鄂尔多斯盆地中部延长组下组合油气充注期次。结果表明:鄂尔多斯盆地中部延长组长8段和长9段致密储层主要发育压实、胶结、交代和溶解4种成岩作用,自生矿物主要为绿泥石、石英胶结物、长石胶结物和方解石胶结物。根据包裹体宿主矿物形成序列,识别出3期烃包裹体。第一期烃包裹体分布在石英愈合缝、石英次生加大边和充填孔隙的石英胶结物中,少数低成熟的黄色荧光烃包裹体及黑色荧光沥青包裹体代表了烃源岩进入生烃门限后排出的少量烃类充注,多数成熟度较高的蓝色、蓝白色荧光烃包裹体代表了生烃高峰期大量烃类充注;第二期烃包裹体分布在长石胶结物中,数量较少,显示蓝色和蓝白色荧光,在溶蚀孔隙周围或沿解理分布,呈短柱状,边界平直;第三期烃包裹体分布在方解石胶结物中,呈孤立或零星分布,形状近六边形;后两期烃包裹体均是在烃类充注结束后捕获孔隙中烃类形成的。研究区延长组长8段和长9段经历了晚侏罗世末期至早白垩世末期的一期烃类持续充注。 相似文献
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LANG Xuqian LI Yang SUN Guohui ZHOU Zhongzheng LI Jing FENG Chao KONG Ming LIU Ya CHENG Xiaojie CHEN Xiguang 《中国海洋大学学报(英文版)》2020,19(2):459-465
Uniform molecular weight(Mw)chitosan(CS)is highly demanded in medical biomaterial industry.This present article described heterogeneous degradation of CS in aqueous HCl/ethanol solution,in which progress uniform Mw CS was successfully prepared.The Mw distribution of CS was measured by gel permeation chromatography(GPC)analysis.Moreover,the structure and properties of degraded CS were characterized by Fourier transform infrared spectroscopy(FT-IR),nuclear magnetic resonance spectroscopy(^1H NMR),X-ray diffraction(XRD)and thermogravimetric(TG)analysis.In addition,the biocompatibility of degraded CS was also assessed by hemolysis rate(HR)measurement.The Mw of CS dramatically decreased from 246 KDa to 76 k Da at the initial 30 min,and stabilized at 18 kDa after 24 h.GPC analysis results showed that the degraded CS molecular become homogenization.FT-IR and 1 H NMR analysis confirmed the basic structure of CS molecular backbone was not destroyed during this progress.Besides,the water solubility of CS was not significantly influenced by this reaction.Moreover,the XRD analysis revealed that crystallinity of degraded CS increased from 70.32% to 99.25%with time.The TG analysis showed improved thermal stability of degraded CS.HR measurement demonstrated the degraded CS possessed excellent biocompatibility.This simple and efficient heterogeneous degradation would open up a new route to produce uniform Mw CS. 相似文献
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为了深入了解油气分布规律，利用流体包裹体显微荧光光谱和显微测温以及一维盆地模拟的埋藏热历史，结合地震构造属性和沉积相分析，对泌阳凹陷北部缓坡带核桃园组油气运聚成藏过程进行了研究。结果显示北部缓坡带核桃园组第三段储层检测到橙黄色、黄绿色和蓝绿色3种颜色荧光油包裹体，反映了3幕不同成熟度的原油捕获。油包裹体的丰度和伴生盐水包裹体均一温度和埋藏史曲线表明，北部储层共存在两期三幕充注事件:第一期规模小，发生于断陷末期的相对低成熟度发橙黄色荧光油，第二期发生在中新世构造抬升期的相对高成熟度的黄绿色和蓝绿色荧光油。流体包裹体古压力模拟显示第二期油气充注时储层是超压状态，推测与当时的构造挤压有关。超压持续作用以及北部地层抬升造成与深凹带源岩增加的流体势差为第二期油气提供了强有力的动力；频繁的断层活动，特别是走滑断裂使得单一的砂体顺层输导转变为砂体顺层输导+断裂垂直输导的复合立体运移输导体系，使得原油以高效率运移到凹陷北部缓坡带。这对精细理解构造抬升控制油气大规模运聚具有重要的意义。 相似文献
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Four kinds of polysaccharides (FA, FB, FC and FD) were extracted and purified from a red alga Furcellaria lumbricalis. Their monosaccharide composition, average molecular mass
and structural feature were determined by gas chromatography (GC), high performance gel permeation chromatography (HPGPC)
and Fourier transform infrared spectroscopy (FTIR), respectively. The results showed that FA and FB were composed of galactose
(Gal), 3,6-anhydro-galactose (AnG) and 4-sulfated-galactose (G4S), which were structurally similar to β-carrageenan and κ-carrageenan.
FC was composed of sulfated galactose and small amount of AnG, indicating that it was a hybrid-sulfated galactan. FD was composed
of α-1,4-glucose and belonged to floridean starch. The respective yields of FA, FB, FC and FD were 4.84%, 33.74%, 8.76% and
13.5%, and the corresponding
were 537 kD, 432 kD, 513 kD and 51 kD respectively. Owning to its high content (>60%) of polysaccharide, F. lumbricalis will be a good source of marine sulfated polysaccharide and shows its potential utilization in food and medicine. 相似文献
10.
SUN Qu WANG Li ZHANG Yongsheng FAN Xingzhu ZHANG Guofeng SHENG Jianhua CHEN Xiaohang LIU Xiang 《世界地质(英文版)》2021,24(3):144-153
The South Narimalahei area is located on the north side of the Middle Kunlun fault in the eastern section of the East Kunlun composite orogenic belt. The ore body is veined and controlled by structures and se-condary fissures, which occurs in the structural alteration fracture zone in the Late Triassic granodiorite. In this deposit, copper mineralization is closely related to silicification and sericification. The formation process of the deposit includes hydrothermal mineralization and supergene oxidation. In this paper, the fluid inclusion minera-logy, microscopic temperature measurement and stable isotope studies have been carried out for ore of the main mineralization stage. The results show that the primary gas-liquid two-phase inclusions and a small amount of single-liquid inclusions are mainly developed in the quartz in the main mineralization stage. The results of microscopic temperature measurement show that the ore-forming fluid which has low temperature(151.7℃--205.8℃), low salinity(2.06 wt%--4.94 wt%NaCl), low density(0.86--0.92 g/cm~3) and shallow formation(1.5--3.0 km) is a hydrothermal solution of NaCl-H_2O system. Hydrogen and oxygen isotope results show that the ore-forming fluids mainly come from atmospheric precipitation, with a small amount of magmatic fluids participating. It is preliminarily determined that the South Narimalahei copper polymetallic deposit is a low-temperature hydrothermal vein deposit. 相似文献
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A Comparative Analysis of Four Kinds of Polysaccharides Purified from Furcellaria lumbricalis 总被引：4，自引：0，他引：4
BARROW Colin 《中国海洋大学学报(英文版)》2007,6(1):16-20
1 Introduction Carrageenan, a water-soluble sulfated polymer, usually extracted from red algae, has been widely used in food industry due to its unique properties, such as gelation, emulsification, protein stabilizer, and so on. There are at least 13 types of carrageenans defined structurally based on the content of sulfate, galactose (Gal) and 3,6-anhydro-galactose (AnG), but only three types of them are commercially available, i.e., κ-, ι- and λ-type carrageenan. Different red algae prod… 相似文献
13.
Shock effects of 93 Grove Mountains (GRV) ordinary chondrites were studied in this work, including fracture, various types of extinction, and recrystallization of silicates observed under optical microscopy. Shock-induced veins and pockets show various microtextures, decomposition and phase transformation of minerals. The confirmed high-pressure polymorphs of silicates are ringwoodite, majorite, pyroxene glass and maskelynite. Based on the shock effects and assemblages of high-pressure minerals, shock stages of all of 93 GRV chondrites were classified. In comparison with literature, the Grove Mountains meteorites have a higher fraction (23 out of 93) of heavily shocked samples (S4-S5). Most of the heavily shocked meteorites are L group (22 out of 23), except for one H chondrite. The distinct shock metamorphism between H and L groups may indicate different surface properties of their parent bodies. In addition, there is relationship between petrologic types and shock stages, with most heavily shocked samples observed in equilibrated ordinary chondrites (especially Type 5 and 6). 相似文献
14.
A novel sensor for ocean electric field testing has been fabricated by polyacrylonitrile-based on carbon fibers with electro-chemical oxidation.The surface profile characteristics of the carbon fibers were characterized by scanning electron microscope,Fourier transform infrared spectra and contact angle.Cyclic voltammetry and Tafel curves have been used to study its electro-chemical performances.Two identical electrodes in sea water as the electric field sensor will swiftly respond to applied electric field which causes positive and negative ions to move in opposite direction,resulting in a electric potential difference(ΔE).Test result indicates that the offset potential is typically below 1 m V with a drift of 60-170μVd^-1.Typical self noise level is 1.07 nV√Hz1/2@1 Hz.The electric field response indicates that the modified electrode pair shows better response to AC sine signal of amplitude and frequency(5 mV and 1 mHz)respectively than its blank.The electric field response model of the modified electrodes is creatively presented according to its electric double layer capacitance and Faraday pseudo-capacitance.Many advantages of the carbon fiber electric field electrode will make it have potential application prospect. 相似文献
15.
为揭示陕西石泉井不同频带水位对气压和固体潮的响应特征，采用频谱分析、相干函数和时移分析方法，对石泉井2015-11-01~2016-02-29的井水位、气压和理论重力固体潮等进行深入分析。结果表明，低频带（f＜0.5 cpd）井水位对气压响应较为一般且波动较大，对固体潮响应很差；中频带（0.5~8 cpd）井水位对固体潮响应很好，同时，对气压成分中的K1、S2和S3频点有较好的响应；高频带（f＞8 cpd）井水位与气压和固体潮的相干性均较差，这可能由于该频带井水位的信噪比较低和气压能量较弱等因素所致。此外，在全频带内，随着气压周期的增大，井水位的滞后时间也相应从1 min增至720 min；在中低频带的某些频点或频段，井水位对气压响应的时移存在超前和异常波动现象。
关键词： 相似文献
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Black shales of the Paleocene Patala Formation are proven source rocks for conventional hydrocarbons in southern Potwar Basin of Pakistan and are assumed to be effective source rocks towards north in the Margalla Hill Range of Pakistan. In this regard, the current study focuses on source rock geochemistry of the Paleocene Patala Formation to assess its source rock potential, organic matter types and thermal maturity levels in the Mar-galla Hill Range of North Pakistan. Source rock generative potential, kerogen types and thermal maturation of the analysed rock samples were unraveled by using Rock-Eval pyrolysis Tmax, TOC (total organic carbon) and vitrinite reflectance ( R0 ) analyses. TOC analysis coupled with S2 yield revealed poor to fair source rock quality encountered within the formation. The pyrolysis Tmax vs Hydrogen Index ( HI) , showed mostly Type Ⅲ kerogen dominated by thermally immature to mature organic matter. The HI and genetic potential is low and revealed poor hydrocarbon generation potential of the formation. The S1 vs TOC plots confirm the indigenous nature of the hydrocarbons hosted by Patala Formation. The vitrinite reflectance outcomes indicated immature to mature source rock beds lying in dry gas zone. The HI and OI signatures and abundance of Type Ⅲ kerogen are indica-ting dominance of terrestrial organic matter within the formation. Overall, the investigated Patala Formation ex-posed at the studied section of Margalla Hill Range, Pakistan acts as a poor source rock unit for liquid hydrocar-bon generation but holds prospects for dry gas generation in the study area. 相似文献
17.
新疆阿尔泰铁矿成矿流体及成矿过程 总被引：2，自引：0，他引：2
以新疆阿尔泰铁矿为研究对象,综述铁矿成矿背景,划分成因类型和成矿时期,对典型矿床地质特征进行描述,研究成矿流体的温度和盐度以及成矿流体来源,最后探讨构造演化与铁矿成矿作用。结果表明:铁矿成因类型可划分为火山岩型、矽卡岩型、伟晶岩型、与花岗岩有关的热液型、与基性岩体有关的钒钛磁铁矿型和砂矿型;矽卡岩矿床流体包裹体从矽卡岩阶段到退化蚀变阶段再到石英-硫化物-碳酸盐阶段的均一温度(从200℃～500℃到200℃～350℃,再到160℃～300℃)以及流体盐度(NaCleq)峰值(从4.5%～21.5%到3.5%～20.5%,再到1.5%～17.5%)逐渐降低;托莫尔特铁(锰)矿沉积期成矿流体以中低温(集中在160℃～300℃)、低盐度(主要集中在4%～9%和14%～20%)为特征;两棵树伟晶岩型铁矿成矿流体为中温(173℃～290℃)、低盐度(0.35%～16.05%);氢和氧同位素特征表明,火山沉积型铁矿沉积期成矿流体是海水与岩浆水的混合,矽卡岩阶段成矿流体主要为岩浆水,石英-硫化物-碳酸盐阶段成矿流体主要为大气降水,混合少量岩浆水,同时两棵树伟晶岩型铁矿成矿流体主要来源于岩浆水和大气降水的混合;碳和氧同位素表明,矽卡岩型铁矿成矿流体中碳主要来自深部岩浆,少量来自海相碳酸盐岩。 相似文献
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The Xiaohongshilazi mineral deposit in Jilin Province,China,is located in the accretion zone in the northern margin of the North China Block. The deposit contains two types of ore bodies: layered Pb-Zn ore bodies in volcanic rock and vein-hosted Pb-Zn ore bodies controlled by fractures. The vein Pb-Zn ore bodies are strictly controlled by tectonic fracture zones trending in S-N direction,which comprise sulfide veins or sulfidebearing quartz veins distributed along faults or structural fissures. The ores mainly appear mesh-vein and vein structures,and also show solid-solution separation and metasomatic textures. The metal minerals are mainly sphalerite,galena,and pyrite,etc. Wall-rock alteration includes mainly sericitization,chloritization,silicification and carbonatization,etc. Microscope observations and Raman spectroscopy analyses indicate that the oreforming fluid of the vein Pb-Zn ore bodies was mainly magmatic water with low temperature,low salinity,and a shallow depth of metallogenesis( ~ 1.5 km). Sulfur and lead isotope analyses indicate that the sulfide source is mainly formation sulfur or biogenic sulfur,which is similar to the sulfur source of hydrothermal deposit( negative( δ~(34) S values),while the main Pb source was the upper crust with some mantle input. This article argues that the vein Pb-Zn ore body of the Xiaohongshilazi deposit is a low-to medium-temperature hydrothermal vein type related to the formation of a shallow magma chamber. 相似文献
19.
近年来,城市发展快速,大量人口奔向城市工作生活,城市建筑物的数量有如雨后春笋般扩张,需要合理地规划城市土地资源,遏制违规乱建现象,因此基于高分辨率遥感影像,对建筑物进行准确提取,对城市规划和管理有着重要辅助作用。本文基于U-Net网络模型,使用美国马萨诸塞州建筑物数据集,对网络模型结构进行探究,提出了一种激活函数为ELU、“编码器-特征增强-解码器”结构的网络模型FE-Net。实验首先通过比较不同网络层数的U-Net5、U-Net6、U-Net7的建筑物提取效果,找到最佳的基础网络模型U-Net6;其次,基于该模型,加入特征增强结构得到“U-Net6+ReLU+特征增强”的网络模型;最后,考虑到ReLU容易产生神经元死亡,为优化激活函数,将激活函数替换为ELU,从而得到网络模型FE-Net（U-Net6+ELU+特征增强）。比较3个网络模型（U-Net6+ReLU、U-Net6+ReLU+特征增强、FE-Net（U-Net6+ELU+特征增强））的建筑物提取结果,表明FE-Net网络模型的建筑物提取效果最好,精度放松F1值达到97.23%,比“U-Net6+ReLU”和“U-Net6+ReLU+特征增强”2个网络模型分别高出0.36%和0.12%,且与其他具有相同数据集的研究成果比较,具有最高的提取精度,它能较好地提取出多尺度的建筑物,不仅对小尺度建筑物有较好的提取效果,而且能大致、较完整地提取出形状不规则的建筑物,有相对更少的漏检和错检,较准确地实现了端到端的建筑物提取。 相似文献
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Bacteria-infected turbots Scophthalmus maximus with septicaemia were examined between 2001 and 2004 in aspects of the conditions of disease occurrence, clinical syndromes and pathological changes. The phenotypic information of pathogenic bacteria was studied, including morphology, physiological and biochemical characteristics, and the mol% G C of the DNA. In addition, representative strains (S010623-1, LH031120-1) were selected for molecular identification by partial 16S rRNA gene sequencing. The results show that the isolates (LH031120-1 to LH031120-6, HT040308-1 to HT040308-6, HT040620-1 to HT040620-6) from three farms were identified as Edwardsiella tarda. The isolates (S010610-1 to S010610-10, S010623-1 to S010623-20) from one farm were identified as Listonella anguillarum. We conducted studies on the pathogenicity of isolates by artificial infection, and revealed all infected groups in morbidity and mortality. The septicaemia infected turbot showed a syndrome similar to that of the naturally infected fish. Antibiotic sensitivity showed that of 37 antimicrobial agents, E. tarda was sensitive to 27 agents, and L. anguillarum was sensitive to 21 agents. 相似文献