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1.
The bowing potential of granitic rocks: rock fabrics, thermal properties and residual strain 总被引：1，自引：0，他引：1
The bowing of natural stone panels is especially known for marble slabs. The bowing of granite is mainly known from tombstones
in subtropical humid climate. Field inspections in combination with laboratory investigations with respect to the thermal
expansion and the bowing potential was performed on two different granitoids (Cezlak granodiorite and Flossenbürg granite)
which differ in the composition and rock fabrics. In addition, to describe and explain the effect of bowing of granitoid facade
panels, neutron time-of-flight diffraction was applied to determine residual macro- and microstrain. The measurements were
combined with investigations of the crystallographic preferred orientation of quartz and biotite. Both samples show a significant
bowing as a function of panel thickness and destination temperature. In comparison to marbles the effect of bowing is more
pronounced in granitoids at temperatures of 120°C. The bowing as well as the thermal expansion of the Cezlak sample is also
anisotropic with respect to the rock fabrics. A quantitative estimate was performed based on the observed textures. The effect
of the locked-in stresses may also have a control on the bowing together with the thermal stresses related to the different
volume expansion of the rock-forming minerals. 相似文献
2.
We have studied the evolution of the texture in two granites and two limestones subjected to slow and uniform temperature change. Each granite has a different grain size and each limestone a different texture: Carrare crystalline limestone and Crepey oolitic limestone. Temperature was varied from 200°C to 700°C. Scanning Electron Microscope observations of different rock samples show that during thermal cycling intercrystalline boundaries in granites widen out progressively and porosity increases. New microcracks appear in crystals between 500°C and 600°C. In Carrare crystalline limestone, intercrystalline cracks appear at temperatures as low as 200°C. Due to its heterogeneous cracks appear at temperatures as low as 200°C. Due to its heterogeneous increasing temperature. Longitudinal wave velocity and intrinsic permeability show good correlation with the Scanning Electron Microscope observations. 相似文献
3.
Enrico Sassoni Serena Andreotti George W. Scherer Elisa Franzoni Siegfried Siegesmund 《Environmental Earth Sciences》2018,77(10):387
Bowing of thin marble slabs is a phenomenon affecting both historic monuments and modern buildings. In spite of the ubiquity and destructiveness of this phenomenon, no fully satisfactory treatment is currently available to arrest and/or prevent bowing. In this study, a treatment based on formation of hydroxyapatite (HAP) was investigated as a possible route to arrest and possibly prevent bowing of Carrara marble slabs. Four different formulations of the HAP treatment were tested and compared to ammonium oxalate and ethyl silicate (widely used in the practice of marble conservation). The treatments were applied onto pre-weathered and unweathered specimens to investigate their ability to arrest and prevent bowing, respectively. Marble behavior was studied in terms of residual strain and bowing after thermal cycles up to 90 °C in dry and wet conditions. Marble cohesion was assessed before and after the thermal cycles by ultrasound. The HAP treatments exhibited promising results, as the residual strain and the bowing after the cycles were always lower or equal to the untreated references, while marble cohesion was always higher. Surprisingly, ammonium oxalate caused marked worsening of marble thermal behavior. In the case of ethyl silicate, most of the initial benefit after consolidation was lost after the thermal cycles. In general, the results of the study point out the importance of evaluating marble thermal behavior to assess the suitability of any conservation treatment and suggest that treatments able to strengthen marble without causing excessive pore occlusion and stiffening are preferable to enhance durability to thermal cycles. 相似文献
4.
The veneer cladding of the Oeconomicum (OEC, Göttingen), the State Theatre of Darmstadt (STD, Darmstadt) and of the State and University Library (SUB, Göttingen) is characterised by pronounced bowing after a short time of exposure. Direct comparison of bowing data related to measurements from 2000 to 2003 at the SUB clearly show that the amplitude in bowing had significantly increased. The bowing is different in intensity and orientation (concave, convex). The cladding material (Peccia marble, Rosa Estremoz marble and Carrara marble) are different in lattice preferred orientation, grain size distribution and grain interlocking. Depending on the bowing, panels may show cracks mostly initiated at the dowels. The percentage of visible cracks and breakouts increases with the amplitude of bowing except for the STD. Repetitive heating–cooling under dry conditions leads to considerable inelastic residual strain only after the first or second thermal cycle. The residual strain continuously increases again if water is present, whereby the moisture content after a thermal cycle has a certain impact on the decay rate. The water-enhanced thermal dilatation strongly correlates with the deterioration rate obtained from the laboratory bow test. Detailed petrophysical investigations provide evidence that with increasing bowing a decrease of mechanical properties (flexural strength or breaking load at dowel hole) occur. Marble degradation is also connected with the increase in porosity and a general shift of the maximum pore radii to larger pore sizes. On-site damage analyses were combined with laboratory tests of the bowing potential to constrain factors that may influence the risk failure. The experimental bowing data clearly demonstrate that after 40 heating cycles combined with the effect of moisture a certain impact on the decay rate is observed. In the case of demounted panels the bowing tests show that already strongly deformed panels from the building exhibit a lower bowing potential than those with lower amplitudes of bowing. This is not the general case for all marble types. Finally, the artificial bowing causes a significant reduction of the flexural strength and the breaking load at the dowel hole. The strength loss of the experimentally aged claddings combined with on-site damage analyses led to conclusions concerning risk assessment and the predicted lifetime of the investigated marble claddings. 相似文献
5.
Three calcitic marble types often used as cladding material and different in lattice preferred orientation (texture), grain shape preferred orientation, grain size distribution and grain interlocking are investigated to study the combined effect of thermal cycles (day-night) and moisture on the decay of marble, particularly on the bowing phenomenon. Repetitive heating-cooling under dry conditions leads to considerable inelastic residual strain only in the first thermal cycle. The residual strain continuously increases again if water is present, whereby the moisture content after a thermal cycle has a certain impact on the decay rate. The water-enhanced thermal dilatation strongly correlates with the deterioration rate obtained from the laboratory bow test. All applied approaches reveal that the texture in combination with the grain shape preferred orientation control the intensity and anisotropy of marble deterioration, thus, the cutting direction of facade panels has to be considered in terms of durability. On-site analysis from building facades confirm the laboratory results such as the bowing tendency of different marbles, directional dependence, relevance of moisture content during cyclical heating and the loss of strength due to environmental impact.Special Issue: Stone decay hazards 相似文献
6.
7.
A new cylinder-piston high hydrostatic testing equipment was briefly introduced. Testing procedure and measuring technique during the hydrostatic experiment were described. The properties of a marble、a silicarenite ,and a granite under hydrostatic tests were rhoroughly studied, A phase-transform in the marble under 1780 MPa was found. The effect of porosity, mineral composition ,and grain size on compressibility and residual deformation of rocks under hydrostatic pressure were examined. 相似文献
8.
Victoria Shushakova Edwin R. Fuller Jr. Siegfried Siegesmund 《Environmental Earth Sciences》2013,69(4):1263-1279
Microstructure‐based finite-element analysis with a microcracking algorithm was used to simulate an actual degradation phenomenon of marble structures, i.e., microcracking. Both microcrack initiation and crack propagation were characterized, as were their dependence on lattice preferred orientation (LPO), grain shape preferred orientation (SPO), grain size, marble composition (calcite and dolomite) and grain‐boundary fracture toughness. Two LPOs were analyzed: a random orientation distribution function and an orientation distribution function with strong directional crystalline texture generated from a March–Dollase distribution. Three SPOs were considered: equiaxed grains; elongated grains and a mixture of equiaxed and elongated grains. Three different grain sizes were considered: fine grains of order 200 μm (only calcitic marble); medium size grains of order 1 mm (calcitic and dolomitic marbles); and large grains of order 2 mm (only dolomitic marble). The fracture surface energy for the grain boundaries, γig, was chosen to be 20 and 40 % of the fracture surface energy of a grain, γxtal, so that both intergranular and transgranular fracture were possible. Studies were performed on these idealized marble microstructures to elucidate the range of microcracking responses. Simulations were performed for both heating and cooling by 50 °C in steps of 1 °C. Microcracking results were correlated with the thermoelastic responses, which are indicators related to degradation. The results indicate that certain combinations of LPO, SPO, grain size, grain‐boundary fracture toughness and marble composition have a significant influence on the thermal-elastic response of marble. Microstructure with the smallest grain size and the highest degree of SPO and LPO had less of a tendency to microcrack. Additionally, with increasing SPO and LPO microcracking becomes more spatially anisotropic. A significant observation for all microstructures was an asymmetry in microcracking upon heating and cooling: more microcracking was observed upon cooling than upon heating. Given an identical microstructure and crystallographic texture, calcite showed larger thermal stresses than dolomite, had an earlier onset of microcracking upon heating and cooling, and a greater microcracked area at a given temperature differential. Thermal expansion coefficients with and without microcracking were also determined. 相似文献
9.
Post-deformational annealing of calcite rocks 总被引：3，自引：3，他引：3
The evolution of microstructure and crystallographic preferred orientation (CPO) during post-deformational annealing was studied on three calcite rock types differing in purity and grain size: Carrara marble (98% calcite, mean grain size of 115 μm), Solnhofen limestone (96%, 5 μm) and synthetic calcite aggregates (99%, 7 μm). Samples were first deformed in torsion at 727 °C at a shear strain rate of 3 × 10− 4 s− 1 to a shear strain of 5 and subsequently heat-treated at 727 °C for various durations between 0 and 24 h. Microstructures and CPOs were analysed by optical microscopy, image analysis and electron backscatter diffraction (EBSD).All rock types deformed in the dislocation creep field at the same applied conditions, but their microstructures and CPOs after deformation and after annealing differed depending on starting grain size and material composition. In Carrara marble and in the synthetic calcite aggregate, a strong CPO developed during deformation accompanied by dynamic recrystallisation with significant changes in grain size. During annealing, widespread grain growth and subtle changes of CPO occurred, and equilibrated foam microstructures were approached after long annealing times. The CPO is the only feature in annealed samples indicating an earlier deformation phase, although it is not always identical to the CPO formed during deformation. In the more impure Solnhofen limestone, secondary phases on grain boundaries suppressed grain boundary mobility and prevented both the formation of a recrystallisation CPO during deformation and grain size modification during deformation and annealing. 相似文献
10.
A. M. Aksyuk A. A. Konyshev V. S. Korzhinskaya Yu. B. Shapovalov 《Doklady Earth Sciences》2016,470(1):921-923
The melting of two basic granite varieties in the Voznesenka Complex such as Yaroslavka biotite granite and Voznesenka Li–F granite was subject to experimental studies to analyze and to compare the conditions of their physicochemical formation. The experiments were conducted at 550–700°C and 50–500 MPa in pure water and in 0.1 and 1 m HF aqueous fluorine-bearing solutions. The melting temperature of Voznesenka Li–F granites was 60–70°C lower than that of Yaroslavka biotite granites. The temperature decreased by almost 100°C from the completion of biotite granite crystallization to the completion of Li–F granite crystallization. 相似文献
11.
PL9-1潜山油藏是渤海湾盆地储量最大的古潜山油气藏之一,探明储量过亿吨.该油藏发育于庙西北凸起鞍部的中生界花岗岩侵入体顶部.凸起端部变质岩中没有油气发现.油气的分布受岩性控制明显.综合岩心观察、薄片鉴定、X粉晶衍射以及常量元素分析等技术手段,通过对比不同岩石类型的矿物组成、储集空间类型及发育程度,探讨了岩性组成对储层发育的控制作用.研究表明,变质岩中裂缝和孔隙均不发育,不能形成有效储层.花岗岩主要储集空间类型为孔隙-裂缝型,总体具有从砂质风化带→砾质风化带→裂缝带→基岩带,储集空间组合类型从孔隙→孔隙+裂缝→裂缝→不太发育的微裂缝的变化特征.储层厚度大,成层性强,可形成有效的规模性储层.花岗岩与变质岩的矿物组成差异控制了研究区优质储层的发育.变质岩中长石含量极低,不能形成溶蚀孔隙,较高含量(30%~50%)的片状矿物使其在应力作用下易发生塑性变形,不易产生裂缝.花岗岩具有很高的长石含量和含量很低的片状矿物,不仅容易被风化并产生溶蚀孔隙,而且易于发生脆性变形形成裂缝. 相似文献
12.
Jan H. Behrmann 《International Journal of Earth Sciences》1983,72(2):605-618
A suite of marble specimens from the Sierra Alhamilla (Spain), deformed to large strains under natural conditions at about 300° C shows distinct variations in microstructure and fabrics. It can be demonstrated that the development of crystallographic preferred orientations and grain shape fabrics are strongly dependent on recrystallized grain size. This is interpreted to reflect the relative importance of various deformational mechanisms. Superplasticity seems to have a sharp upper grain size limit at 10–15 /smm. Within the power law creep regime, deformation in fine grained aggregates is probably dominated by diffusional, in coarser ones by dislocation mechanisms. The transition is a gradual one, and may span a grain size range of 30 /sm. 相似文献
13.
The Xuebaoding crystal deposit, located in northern Longmenshan, Sichuan Province, China, is well known for producing coarse‐grained crystals of scheelite, beryl, cassiterite, fluorite and other minerals. The orebody occurs between the Pankou and Pukouling granites, and a typical ore vein is divided into three parts: muscovite and beryl within granite (Part I); beryl, cassiterite and muscovite in the host transition from granite to marble (Part II); and the main mineralization part, an assemblage of beryl, cassiterite, scheelite, fluorite, apatite and needle‐like tourmaline within marble (Part III). No evidence of crosscutting or overlapping of these ore veins by others suggests that the orebody was formed by single fluid activity. The contents of Be, W, Sn, Li, Cs, Rb, B, and F in the Pankou and Pukouling granites are similar to those of the granites that host Nanling W–Sn deposits. The calculated isotopic compositions of beryl, scheelite and cassiterite (δD, ?69.3‰ to ?107.2‰ and δ18OH2O, 8.2‰ to 15.0‰) indicate that the ore‐forming fluids were mainly composed of magmatic water with minor meteoric water and CO2 derived from decarbonation of marble. Primary fluid inclusions are CO2? CH4+ H2O ± CO2 (vapor), with or without clathrates and halites. We estimate the fluid trapping condition at T = 220 to 360°C and P > 0.9 kbar. Fluid inclusions are rich in H2O, F‐ and Cl‐. Evidence for fluid‐phase immiscibility during mineralization includes variable L/V ratios in the inclusions and inclusions containing different phase proportions. Fluid immiscibility may have been induced by the pressure released by extension joints, thereby facilitating the mineralization found in Part III. Based on the geochemical data, geological occurrence, and fluid inclusion studies, we hypothesize that the coarse‐grained crystals were formed by: (i) the high content of ore elements and volatile elements such as F in ore‐forming fluids; (ii) occurrence of fluid immiscibility and Ca‐bearing minerals after wall rock transition from granite to marble making the ore elements deposit completely; (iii) pure host marble as host rock without impure elements such as Fe; and (iv) sufficient space in ore veins to allow growth. 相似文献
14.
Dolomitic marble on the island of Naxos was deformed at variable temperatures ranging from 390 °C to >700 °C. Microstructural investigations indicate two end-member of deformation mechanisms: (1) Diffusion creep processes associated with small grain sizes and weak or no CPO (crystallographic preferred orientation), whereas (2) dislocation creep processes are related with larger grain sizes and strong CPO. The change between these mechanisms depends on grain size and temperature. Therefore, sample with dislocation and diffusion creep microstructures and CPO occur at intermediate temperatures in relative pure dolomite samples. The measured dolomite grain size ranges from 3 to 940 μm. Grain sizes at Tmax >450 °C show an Arrhenius type evolution reflecting the stabilized grain size in deformed and relative pure dolomite. The stabilized grain size is five times smaller than that of calcite at the same temperature and shows the same Arrhenius-type evolution. In addition, the effect of second phase particle influences the grain size evolution, comparable with calcite. Calcite/dolomite mixtures are also characterized by the same difference in grain size, but recrystallization mechanism including chemical recrystallization induced by deformation may contribute to apparent non-temperature equilibrated Mg-content in calcite. 相似文献
15.
In the Dora Maira Massif, western Alps, essentially undeformed ultrahigh-pressure (UHP) metamorphic granites (Brossasco granite) are embedded in, and locally grade into, granite gneisses or augengneisses and mylonites. In this study, the quartz microfabrics of the undeformed granites are compared against the augengneisses and mylonites in a representative number of samples from several locations. In the undeformed granites, the fine-grained quartz aggregates that formed from coesite upon decompression are characterized by a foam structure and random crystallographic orientation. In the deformed granites, the quartz microstructures and the crystallographic preferred orientation (CPO) indicate deformation by dislocation creep. Most of the deformation of the granites (if not all) must have happened at a late stage during exhumation, after transformation of coesite to quartz, at greenschist facies conditions in the middle crust. The deformed granites provide no evidence of deformation during subduction, at (U)HP metamorphic conditions, and in the earlier stages of exhumation. The diameter of internally undeformed slices of continental crust subducted to and exhumed from about 100 km can exceed that of the presently exposed Brossasco granite, i.e. it can be on the kilometre scale. 相似文献
16.
Influence of Marble’s Texture on its Mechanical Behavior 总被引：1，自引：1，他引：0
This research work studied the influence of texture on the mechanical properties of crystalline rocks at the scale of the laboratory sample. The experiments were performed on a marble varying in texture, so that the study was conducted on homogeneous (entirely xenoblastic or totally granoblastic) and heterogeneous (mix of the two textures) specimens. The mechanical behavior of the homogeneous and heterogeneous samples was investigated with static and dynamic, destructive and nondestructive tests, in natural conditions, at the laboratory temperature, and at higher temperatures. The specimens were heated to 100, 200, and 300 °C, in order to examine the effect of heating temperature on the elastic modulus and P-waves velocity. As a result, the pure granoblastic marble exhibits values of the elastic modulus, P-waves velocity, and strengths, both in natural conditions and on heated specimens, lower than xenoblastic samples. Such different behavior can be explained by a higher grain boundaries porosity of the granoblastic marble. On heterogeneous samples, only the Rock Impact Hardness Number (RIHN) appears able to highlight the dependence of the mechanical properties on the rock texture. In particular, the impact strength improves with increasing the percentage of xenoblastic texture inside the specimen. 相似文献
17.
高放废物深部地质处置目前受到世界各国的高度重视。花岗岩是我国高放废物地质处置工程的候选围岩,深入了解处置库花岗岩的强度及破坏特性对于处置系统的设计及性能评价具有十分重要的意义。作为矿物颗粒的集合体,花岗岩是一种由石英、长石和黑云母等矿物组成的非均质岩石,矿物粒径对其宏观力学特性影响明显。以我国高放地质处置库预选区阿拉善花岗岩为例,选取矿物粒径差异明显的似斑状花岗岩和中粒花岗岩两类岩石,采用单轴压缩试验与数值模拟相结合的方式研究了矿物粒径对岩石力学特性的影响。单轴压缩试验在MTS815岩石力学试验系统进行,数值模拟采用基于离散元的颗粒流程序PFC2D完成。数值模拟过程中,以试件表面图像为基础,采用数字图像处理技术获取岩石内部矿物组分的实际空间分布,从而建立了精确反映花岗岩内部矿物种类及其空间位置的数值模型。利用该模型对花岗岩的单轴压缩试验进行了数值模拟,并与试验结果对比,论证了模型的可靠性。试验及模拟结果表明,阿拉善花岗岩破坏形式为脆性张拉破坏,裂纹大多平行于轴压方向,数字图像数值分析方法可真实地反映材料细观结构。矿物粒径对材料力学特性的影响主要表现为:细粒、等粒结构的岩石强度高,粗粒、不等粒结构的岩石强度低。研究成果可为掌握矿物粒径对岩石强度及变形特性的影响提供依据。 相似文献
18.
脆性对岩石破裂机制及声发射特性具有重要影响。采用花岗岩及大理岩两种不同岩性的岩石,开展了单轴压缩及声发射测试试验,获取了两种岩石的强度及变形特性,并对其脆性大小进行定量评价,分析了单轴压缩过程中两种岩石声发射能量演化特性,结合声发射b值计算结果及其物理意义,对比了两种岩石破裂机制的差异性。结果表明:(1)试验所采用的两种岩石,花岗岩的σcd/σp之比介于0.676~0.745之间,平均为0.706,而大理岩的σcd/σp之比介于0.439~0.615,平均为0.52;(2)基于脆性评价指标,结合试样宏观破坏现象及形态,本次试验采用的花岗岩其脆性大于大理岩;(3)岩石脆性程度越大,在裂纹不稳定扩展阶段,在产生相同的轴向压缩变形的情况下,环向变形量越大;(4)强脆性的花岗岩在裂纹不稳定扩展阶段持续出现高能级的声发射信号,而弱脆性的大理岩则表现出能量持续降低的变化趋势,峰值强度后,弱脆性的大理岩其高能级能量的声发射信号更活跃;(5)单轴压缩下,与大理岩相比,花岗岩破坏过程中大尺度的破裂事件所占比例较大。 相似文献
19.
Weqiang Zhang Qiang Sun Yuliang Zhang Lei Xue Fanfan Kong 《Environmental Earth Sciences》2018,77(9):350
The evolution of porosity and changes in wave velocity in granite after high-temperature treatment has been experimentally investigated in different studies. Statistical analysis of the test results shows that there is a temperature threshold value that leads to variations in porosity and wave velocity. At a temperature that is less than 200 °C, the porosity of granite slowly increases with increases in temperature, while the wave velocity decreases. When the temperature is greater than 200 °C (especially between 400 and 600 °C), the porosity quickly increases, while the wave velocity substantially decreases. The temperature ranges of room temperature to 200 and 200–400 °C correspond to the undamaged state and the micro-damage state, respectively. The results confirm that there is an important link between the variations of physical and mechanical properties in response to thermal treatment. By studying the relationships among rock porosity, wave velocity and temperature, this provides the basis for solving multi-variable coupling problems under high temperatures for the thermal exploitation of petroleum and safe disposal of nuclear waste. 相似文献
20.
In order to describe and explain the effect of bowing of marble facade panels, neutron time-of-flight diffraction was applied to determine residual macro- and microstrain on the calcite mineral phase. The measurements were combined with investigations of the crystallographic preferred orientation (texture) measurements by neutron diffraction, macroscopic measuring of the bowing on marble building stones, as well as microfabric analyses. Three samples were investigated to explain the bowing effect: a fresh broken sample, a good conditioned facade panel and a strongly deformed facade panel. Residual intracrystalline strain was detected in all investigated samples, which differed in the degree of bowing. For the first time, the preferred orientation and the residual strain were found to be related. The results show that different strain magnitudes are reflected by residual strains, which differ significantly in magnitude and direction. Furthermore, different Bragg peak widths have been detected as an indication of microscopic strain. The observed residual strain values in the samples are related with the grain shape and texture properties. 相似文献