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1.
联用筛析法与激光法进行粒度接序分析的界点选择   总被引:1,自引:0,他引:1  
冷伟  范代读 《沉积学报》2014,32(3):478-484
筛析法、激光法和图像法是三种常用的粒度分析方法,但由于测试原理的不同,三种测试方法有不同的适用性。筛析法和图像法能够精确测量砂质颗粒的粒径,但不适用于泥质细颗粒(<0.063 mm)的粒径测量;相反,激光法无法准确测量中粗砂粒级颗粒(2~0.21 mm),但能高精度测量较细沉积物粒径。分选较差的天然沉积物粒径分布范围较广,需要综合运用筛析法-激光法进行接序粒度测试。通常选用2 mm为界点开展接序粒度分析,但因激光法在测量中粗砂颗粒时误差较大,易导致接序粒度分析结果准确性不高。建议以0.21 mm为分界点开展接序粒度分析,分别避开筛析法和激光法测量精度不高的粒级区间,可使测试结果的准确性得到有效的提高。  相似文献   

2.
Microstructure‐based finite-element analysis with a microcracking algorithm was used to simulate an actual degradation phenomenon of marble structures, i.e., microcracking. Both microcrack initiation and crack propagation were characterized, as were their dependence on lattice preferred orientation (LPO), grain shape preferred orientation (SPO), grain size, marble composition (calcite and dolomite) and grain‐boundary fracture toughness. Two LPOs were analyzed: a random orientation distribution function and an orientation distribution function with strong directional crystalline texture generated from a March–Dollase distribution. Three SPOs were considered: equiaxed grains; elongated grains and a mixture of equiaxed and elongated grains. Three different grain sizes were considered: fine grains of order 200 μm (only calcitic marble); medium size grains of order 1 mm (calcitic and dolomitic marbles); and large grains of order 2 mm (only dolomitic marble). The fracture surface energy for the grain boundaries, γig, was chosen to be 20 and 40 % of the fracture surface energy of a grain, γxtal, so that both intergranular and transgranular fracture were possible. Studies were performed on these idealized marble microstructures to elucidate the range of microcracking responses. Simulations were performed for both heating and cooling by 50 °C in steps of 1 °C. Microcracking results were correlated with the thermoelastic responses, which are indicators related to degradation. The results indicate that certain combinations of LPO, SPO, grain size, grain‐boundary fracture toughness and marble composition have a significant influence on the thermal-elastic response of marble. Microstructure with the smallest grain size and the highest degree of SPO and LPO had less of a tendency to microcrack. Additionally, with increasing SPO and LPO microcracking becomes more spatially anisotropic. A significant observation for all microstructures was an asymmetry in microcracking upon heating and cooling: more microcracking was observed upon cooling than upon heating. Given an identical microstructure and crystallographic texture, calcite showed larger thermal stresses than dolomite, had an earlier onset of microcracking upon heating and cooling, and a greater microcracked area at a given temperature differential. Thermal expansion coefficients with and without microcracking were also determined.  相似文献   

3.
The paper analyses the statistical parameters of the sand grain size distribution of Al-Ubaylah barchan dunes applying the sieving technique and Folk and Ward, and Trask's equation. The results of the sieving analysis divulged that nearly over 90% of the sand particles fall in the size ranging between 1.50ø and 3.ø. Insignificant amount of sand grains also fall in the size ranging from 0.0ø to 1.50ø and from 3.0ø to 4.0ø respectively. The statistical analysis reveals that the sand is characteristically fine grained, moderately to moderately well sorted with an average diameter of 2.4ø and a standard deviation of 0.64ø. The sand distribution is positively fine skewed and mesokurtic to leptokurtic in nature. No significant variation in the statistical parameters (median, mean, sorting, skewness and kurtosis) of the sand grains samples used in this research is detected. The sand grain size distribution of all the samples can also be considered symmetrical and unimodal in nature. Those abovementioned characteristics are found to be nearly similar to that of other Saudi dune deserts. The miscroscopic investigation undertaken by this researcher displays that quartz represents often more than 99% of the samples. Felsic, mafic and calcium carbonates minerals represent less than 1% of the mineralogical constituents. The sand grains are subrounded to subangular and iron and calcium carbonates coated.  相似文献   

4.
A series of detailed small-scale tests have been made to investigate the use of short delays to promote better fragmentation caused by shock wave interactions. The block design had a size of 650/660 × 205 × 300 mm (L × W × H) and two rows with five Ø 10-mm blastholes in each row. The spacing (S) and burden (B) were 110 and 70 mm, respectively, giving an S/B ratio of 1.6. The results showed no distinct differences or high improvements of the fragmentation when the delays were in the time range of interactions compared with no shock wave interactions. The decrease of x 50 (mean size) was around 20 % at a delay time ~1.1 ms/m burden compared with longer delays like 2 ms/m. A statistical analysis of the results has been made to evaluate the minimum at short delays and it is not significant.  相似文献   

5.
Grain size is a fundamental property of sediments and is commonly used to describe sedimentary facies and classify sedimentary environments. Among the various conventional techniques utilized to determine grain‐size frequency distributions, sieving is the most widely applied procedure. The accuracy of such analyses is, among other factors, strongly dependent on the sieving time. However, despite a substantial amount of research in this field, optimal sieving times for different types of sediments have, to date, not been established. In this article, the influence of sieving time on grain‐size analyses of medium‐grained microtidal and mesotidal beach and dune sands has been determined. To assess the precision of important textural parameters, such as median grain size, sorting, skewness and kurtosis, an error analysis was carried out for different sieving times (2, 5, 10, 15 and 20 minutes). After calibrating the analytical and sampling methodologies, significant deviations were registered when sieving time was less than 10 minutes. However, such deviations were very small and grain‐size distributions remained almost identical for sieving times of 10 minutes and longer, relative errors being as low as 0% in some cases.  相似文献   

6.
Behavior of zircon at the schist/migmatite transition is investigated. Syn-metamorphic overgrowth is rare in zircon in schists, whereas zircon in migmatites has rims with low Th/U that give 90.3 ± 2.2 Ma U–Pb concordia age. Between inherited core and the metamorphic rim, a thin, dark-CL annulus containing melt inclusion is commonly developed, suggesting that it formed contemporaneous with the rim in the presence of melt. In diatexites, the annulus is further truncated by the brighter-CL overgrowth, suggesting the resorption and regrowth of the zircon after near-peak metamorphism. Part of the zircon rim crystallized during the solidification of the melt in migmatites. Preservation of angular-shaped inherited core of 5–10 μm in zircon included in garnet suggests that zircon of this size did not experience resorption but developed overgrowths during near-peak metamorphism. The Ostwald ripening process consuming zircon less than 5–10 μm is required to form new overgrowths. Curved crystal size distribution pattern for fine-grained zircons in a diatexite sample may indicate the contribution of this process. Zircon less than 20 μm is confirmed to be an important sink of Zr in metatexites, and ca. 35-μm zircon without detrital core are common in diatexites, supporting new nucleation of zircon in migmatites. In the Ryoke metamorphic belt at the Aoyama area, monazite from migmatites records the prograde growth age of 96.5 ± 1.9 Ma. Using the difference of growth timing of monazite and zircon, the duration of metamorphism higher than the amphibolite facies grade is estimated to be ca. 6 Myr.  相似文献   

7.
The paper proposes a standardized image-processing procedure with the use of sieve analysis results for calibration which is utilized to measure the size distribution of fragmentation at Sungun mine. Through this procedure, a number of 19 bench blasting in various levels have been initially selected as the target of the study for each, multiple photos were taken immediately after blast from suitable perspectives and locations of the muckpiles surfaces. The number of image sampling was chosen adequately high to achieve further reliability of the whole photography procedure. Then fragments of each muckpile were separately mixed by a loader, where another image sampling from these new muckpiles, bucket of loaders, and haulage trucks was performed. For the purpose of sieve analysis, seven sieves with the mesh sizes between 1.27 cm (0.5 in) and 25.4 cm (10 in) were designed, manufactured, and then installed at Sungun semi-industrial laboratory. Additionally, three mass samples of the mixed fragments were randomly chosen among the 19 muckpiles for sieving. During image analysis stage, “sieve shift” and “mass power” factors, required to obtain standardized size distribution, were precisely assigned when the results obtained by the image analysis software was in accordance with the sieving results. In order to validate the reliability of the image processing, a comparative analysis of the achieved results was made with the results of the original Kuz–Ram model [Cunningham (1983) The Kuz–Ram model for prediction of fragmentation from blasting. In: Proceedings of the first international symposium on rock fragmentation by blasting, Lulea, Sweden, pp 439–454]. Finally, the image-processing procedure was found to be more efficient, with results close-matched to the real results of the sieve analysis.  相似文献   

8.
Factors Affecting Crack Initiation in Low Porosity Crystalline Rocks   总被引:1,自引:1,他引:0  
Crack initiation in uniaxial compressive loading of rocks occurs well before the peak strength is reached. The factors that may influence the onset of cracking and possible initiating mechanisms were explored using a discrete element numerical approach. The numerical approach was based on grain-based model that utilized the Voronoi tessellation scheme to represent low porosity crystalline rocks such as granite. The effect of grain size distribution (sorting coefficient ranging from 1.5 to 1.03), grain size (average grain size ranging from 0.75 to 2.25 mm), and the heterogeneities of different mineral grains (quartz, K-feldspar, plagioclase) on the onset of cracking were examined. The modelling revealed that crack initiation appears to be a tensile mechanism in low porosity rocks, and that shear cracking along grain boundaries is only a prominent mechanism near the peak strength. It was also shown that the heterogeneity introduced by the grain size distribution had the most significant effect on peak strength and crack initiation stress. The peak strength ranges from 140 to 208 MPa as the grain size distribution varies from heterogeneous to uniform, respectively. However, the ratio of crack initiation to peak stress showed only minor variation, as the heterogeneity decreases. The other factors investigated had only minor effects on crack initiation and peak strength, and crack initiation ratio.  相似文献   

9.
Liquefaction of soils is a natural phenomenon associated with a dramatic loss of the soil shear strength in undrained conditions due to a development of excess pore water pressure. It usually causes extensive damages to buildings and infrastructures during earthquakes. Thus, it is important to evaluate extent of influential parameters on the liquefaction phenomenon of soils in order to clearly understand the different mechanisms leading to its triggering. The soil gradation is one of the most important parameters affecting the liquefaction phenomenon. In this context, a series of undrained compression triaxial tests were carried out on eighteen natural loose (Dr = 25%) sandy samples containing low plastic fines content of 2% (Ip = 5%) considering different extreme sizes (1.6 mm ≤ Dmax ≤ 4 mm and 0.001 mm ≤ Dmin ≤ 0.63 mm) and two mean grain size ranges (0.25 mm ≤ D50 ≤ 1.0 mm) and (1.0 mm ≤ D50 ≤ 2.5 mm). The initial confining pressure for all tests was kept constant (P′c = 100 kPa). The obtained test results indicate that the mean grain size (D50) and extreme grain sizes (Dmax and Dmin) have a significant influence on the undrained shear strength (known as liquefaction resistance) and appear as pertinent factors for the prediction of the undrained shear strength for the soil gradation under study. The undrained shear strength and the excess pore water pressure can be correlated to the extreme grain sizes (Dmax and Dmin) and the mean grain size (D50) of tested wet deposited samples.  相似文献   

10.
We examined relationships between freshwater inflow and population abundance and distribution of two size classes (15–50 mm Standard Length and 51–100 mm SL) of spotted seatrout (Cynoscion nebulosus) and red drum (Sciaenops ocellatus) over our 13-year study covering shallow waters of Tampa Bay and several adjacent rivers. Juveniles of seatrout were relatively abundant most years and broadly distributed primarily in the bay. Freshwater inflow was positively related to spatial distribution and abundance of smaller juveniles of seatrout, yet it was unrelated to the larger size class. Red drum juveniles were less abundant and narrowly distributed primarily within the rivers. Lower portions of the Alafia, Little Manatee, and Manatee Rivers—a combined area comprising only 2 % of the study area—contained 40–96 % of the annual population. Freshwater inflow was positively related to population distribution and abundance of larger red drum suggesting that reductions in inflow can reduce both habitat area and populations. Inflow was related to abundance but not distribution of the smaller red drum suggesting that inflow may increase habitat quality but perhaps not quantity at this earlier growth stage. Comparing spatial and population dynamics of multiple species can help prioritize them for conservation and management issues, such as freshwater inflow regulation. Reductions in inflow reduce populations and spatial distribution of at least one juvenile life stage of these two fishery species. Due to their narrow spatial distribution in the rivers, juveniles of red drum appear to be particularly vulnerable to modification of the riverine environment.  相似文献   

11.
THE CARBONATE FRACTION OF BEACH AND DUNE SANDS   总被引:1,自引:0,他引:1  
The sand size carbonate fractions of beach and dune sands from the southeastern U.S. Atlantic coast were investigated from the standpoint of mineralogy, roundness and size distribution. The carbonate fractions of beach-dune sands used in this study range in abundance from less than 1% to over 40% and average about 10%. Calcium carbonate is least abundant in Georgia beaches and increases slightly to the north and greatly to the south. The size distribution of the carbonate fraction is similar to that of the non-carbonate fraction since both have been distributed by the same processes. The variable flat shape of calcareous fragments causes the carbonate fraction to be usually coarser and more poorly sorted than the acid insoluble residues of the samples. No regional relationship between roundness and wave energies was found in sand size materials although field observations indicate high energies strikingly round gravel sized calcareous fragments. There is some tendency for angularity to increase with decreasing grain size in the sand sizes as with quartz grains. The mineralogy of beach sand carbonate fractions is characterized by the almost total absence of high My calcite. Aragonite is the dominant mineral.  相似文献   

12.
Understanding the mechanisms of parent-daughter isotopic mobility at the nanoscale is key to rigorous interpretation of Ue The Pb data and associated dating. Until now, all nanoscale geochronological studies on geological samples have relied on either Transmission Electron Microscope(TEM) or Atom Probe Microscopy(APM) characterizations alone, thus suffering from the respective weaknesses of each technique. Here we focus on monazite crystals from a ~1 Ga, ultrahigh temperature granulite from Rogaland(Norway). This sample has recorded concordant UeP b dates(measured by LA-ICP-MS) that range over 100 My, with the three domains yielding distinct isotopic Ue Pb ages of 1034 ± 6 Ma(D1; Srich core), 1005 ± 7 Ma(D2), and 935 ± 7 Ma(D3), respectively. Combined APM and TEM characterization of these monazite crystals reveal phase separation that led to the isolation of two different radiogenic Pb(Pb*) reservoirs at the nanoscale. The S-rich core of these monazite crystals contains Cae Srich clusters, 5 -10 nm in size, homogenously distributed within the monazite matrix with a mean interparticle distance of 40 -60 nm. The clusters acted as a sink for radiogenic Pb(Pb*) produced in the monazite matrix, which was reset at the nanoscale via Pb diffusion while the grain remained closed at the micro-scale. Compared to the concordant ages given by conventional micro-scale dating of the grain,the apparent nano-scale age of the monazite matrix in between clusters is about 100 Myr younger, which compares remarkably well to the duration of the metamorphic event. This study highlights the capabilities of combined APM-TEM nano-structural and nano-isotopic characterizations in dating and timing of geological events, allowing the detection of processes untraceable with conventional dating methods.  相似文献   

13.
砂土颗粒级配是影响砂土工程性质的重要参数之一,传统的颗分试验方法由于试验原理不同而具有不同的适用范 围。为更加方便、准确地获取砂土颗粒级配,提出了一种基于数字图像处理技术来获取SEM照片中的砂颗粒粒径参数及级 配特征的新方法。将准备好的砂土样品打磨成薄片放在扫描电镜下拍照,然后利用Photoshop软件对照片进行拼接,并采用 自主研发的SMAS数字图像分析系统对拼接好的照片进行定量分析处理,获取样品的微观结构参数,将获得的“土颗粒等 效直径”和“土颗粒面积”分别等效为实际土颗粒粒径和土颗粒质量,进而换算得到砂土的颗粒级配曲线;然后将通过数 字图像技术获得的砂土颗粒级配曲线与通过传统筛分法和激光粒度分析法得到的颗粒级配曲线进行对比,验证了提出的数 字图像处理方法的有效性和可靠性,同时分析了两种方法之间存在的差异及其原因,并对数字图像处理方法和传统颗分方 法各自的优缺点进行了讨论。  相似文献   

14.
砂土颗粒级配是影响砂土工程性质的重要参数之一,传统的颗分试验方法由于试验原理不同而具有不同的适用范 围。为更加方便、准确地获取砂土颗粒级配,提出了一种基于数字图像处理技术来获取SEM照片中的砂颗粒粒径参数及级 配特征的新方法。将准备好的砂土样品打磨成薄片放在扫描电镜下拍照,然后利用Photoshop软件对照片进行拼接,并采用 自主研发的SMAS数字图像分析系统对拼接好的照片进行定量分析处理,获取样品的微观结构参数,将获得的“土颗粒等 效直径”和“土颗粒面积”分别等效为实际土颗粒粒径和土颗粒质量,进而换算得到砂土的颗粒级配曲线;然后将通过数 字图像技术获得的砂土颗粒级配曲线与通过传统筛分法和激光粒度分析法得到的颗粒级配曲线进行对比,验证了提出的数 字图像处理方法的有效性和可靠性,同时分析了两种方法之间存在的差异及其原因,并对数字图像处理方法和传统颗分方 法各自的优缺点进行了讨论。  相似文献   

15.
Grain size effect on the electrical conductivity of clinopyroxene   总被引:3,自引:0,他引:3  
Complex impedance spectra of polycrystalline samples (with grain size fractions ~5–63, 63–160 and 160–250 μm) and a single crystal sample (with orientation parallel to b), prepared from a natural megacryst augite, were measured in a piston cylinder apparatus at 10 kbar and 500–1,000°C and with a Solartron 1260 Impedance/Gain Phase analyzer over a frequency range of 0.1–106 Hz. The main charge carriers are attributed to small polarons, and the activation enthalpy is 83 ± 3 to 90 ± 3 kJ/mol. The measured electrical conductivity shows no difference between the polycrystalline and single crystal samples, suggesting independence of electrical conductivity on grain size given a change above ~5 μm. The electrical conductivity of augite is much higher than that of olivine, indicating that, if regionally enriched, augites may lead to zones of high electrical conductivity and electrical anisotropy in the deep lithosphere.  相似文献   

16.
Sixteen penecontemporaneously deposited mudrock-sandstone pairs ranging in age from Devonian to Cretaceous were treated chemically to isolate the quartz and chert fraction from the other constituents of the rocks. The amount of crystalline silica was determined from the chemical treatments; its size distribution was determined using a combination of normal and Micro Mesh sieving and settling tube analysis; the crystalline silica coarser than 10 μu was examined petrographically to determine the amount of chert. Percentages of crystalline silica in the mudrocks range from 6·7 to 46·7 % and average 27·6 (σ= 10·7). Mean grain size ranges from 4·4 φ to 7·3 φ and averages 6·1 φ. The crystalline silica fraction is a poorly sorted medium to fine silt consisting of one-eighth sand, six-eighths silt, and one-eighth clay size sediment. Percentage of crystalline silica and mean size of crystalline silica in the thirty-two mudrocks and sandstones are positively correlated; r= 0·685, which is significant at the 99 % level. The best fit linear regression line is: Y= 102·7–11·3X. Extrapolation of the regression line indicates that, on the average, crystalline silica is lacking in mudrocks in grain sizes finer than 9·1 φ (1·μm), a result consistent with observations by clay mineralogists. The crystalline silica fraction of both the mudrocks and associated sandstones averages 4% chert in the >10 μm portion. There is no correlation between the mean grain size of the crystalline silica and the percentage of chert in it.  相似文献   

17.
山东黄河流域下游土壤粒度和深度试验成果   总被引:1,自引:0,他引:1  
以黄河流域下游野外获得的土壤粒度和深度纵剖面试验资料为基础,分析了黄河流域下游不同土壤类型区、不同地貌单元的土壤粒级组成、元素在各粒级组中的分配特征和元素在土壤纵剖面中的含量、纵向变化规律,探讨了其在生态地球化学调查中的意义。确定了能代表区域内土壤主要物质组成的粒级范围,提出了本区生态地球化学调查的最佳样品筛分加工方案和表层、深层土壤样品采集的有效深度和层位。  相似文献   

18.
Relative density is an important state parameter that influences the soil behavior. Preparation of sand specimens with uniform density is critical during large-scale laboratory testing in geotechnical engineering. In this study, the details of a stationary air pluviation device used to prepare uniform sand specimens in a large-size test chamber with dimensions equal to 900 mm × 900 mm × 1000 mm (in length, width, and depth) are provided. The proposed device is found to be simple to construct due to presence of only two diffuser sieves with an ability to produce uniform sand beds in a reasonably quick time. Prior to construction of full-scale pluviation device, a scaled-down model of the device with plan dimensions equal to 300 mm × 300 mm is fabricated to perform calibration studies. The range of densities of two gradations of Indian Standard sand (IS Grade II and IS Grade III) obtained using this device for various heights of fall of sand particles and passing through different opening sizes are provided. Relative density in the range of 53–99 % and 74–99 % is achieved for IS Grade II and III sands, respectively. The spatial uniformity in densities is also assessed, and the coefficient of variation (COV) in the density is found to be less than about 7 %. In addition to pluviation method, uniform sand beds are also prepared using pneumatically-operated vibratory method. The target relative density of sand bed is achieved by adjusting the pressure of compressed air inside the vibrator, and the maximum relative density of IS Grade II and Grade III sands from vibratory method is found to be higher than that from pluviation method for the range of pressures chosen in the study.  相似文献   

19.
Evaluation of fractures and their parameters, such as aperture and density, is necessary in the optimization of oil production and field development. The purpose of this study is the calculation of fracture parameters in the Asmari reservoir using two electrical image logs (FMI, EMI), and the determination of fracture parameters’ effect on the porosity and permeability using thin sections and velocity deviation log (VDL). The results indicate that production in the Asmari reservoir is a combination of fractures and rock matrix. Fracture aperture (VAH) and fracture porosity (VPA) are only measurable with core and image logs directly. However, regarding core limitations, the image log has been recognized as the best method for fracture parameter determination due to their high resolution (2.5 mm). In this study, VDL log and thin sections have been used as auxiliary methods which may be available in all wells. The VDL log provides a tool to obtain downhole information about the predominant pore type in carbonates. Results indicate that between fracture parameters, VAH is considered as the most important parameter for determining permeability. For well No. 3, VAH ranges from minimum 51 × 10?5 mm to maximum 0. 047 mm and VPA changes from min 10?5% to maximum 0.02056%. For well No. 6, VAH varies from 5 × 10?4 to 0.0695 mm and VPA varies from 10?5 to 0.015%. Therefore, due to high fracture density and fracture aperture, it seems that most of effective porosity originates from fractures especially in well No. 3. However, VDL for well No. 6 indicates that intercrystalline and vuggy porosity are the dominant porosity. This result may be an indication for fracture set diversity in the two studied wells. While in well No. 3, they related to the folding and active faults, in well No. 6 they are only of folding type. Furthermore, results indicate the high capability for both of EMI and FMI image logs for calculation of fracture and vug parameters in the carbonate reservoirs.  相似文献   

20.
With the intensification of oil and gas exploration, tight sandstone reservoirs have received an increasing amount of attention, particularly with regard to the genesis of tight reservoir rock. The Upper Triassic Yanchang Formation in the Longdong area of the Ordos Basin has developed a typical tight, oil-bearing, clastic reservoir (lithic arkose and feldspathic litharenite, grain size is mainly 0.1~0.3 mm in diameter). During the depositional period of the Chang 4 and 5 members, the two provenance systems of the southwest and northeast developed in the study area. In the southwest, sandstones in the lower part of distributary channels are coarser with fewer quartz overgrowth and ankerite and better reservoir quality (porosity about 12%, permeability about 1 mD). In the northeast, chlorite coating is thicker (>?4 vol%) in the underwater channel sandstones (porosity is about 14%, permeability is about 2 mD) than in the mouth bar sandstones. Sandstones in the upper part of distributary channels are finer with lower permeability (about 0.1 mD). Authigenic ankerite mainly appears around detrital dolomite as an overgrowth. The SiO2 in the quartz overgrowth most likely came from the transformation of smectite to illite and the dissolution of feldspar. In the northeast, only 2 vol% of chlorite rims significantly inhibited quartz overgrowth, but they probably blocked and delayed the dissolution of feldspars by acids. We present results here that show the diagenetic differences in sand bodies in delta fronts are influenced by sediment size, maturity, and the composition of framework grain; the materials that compose authigenic minerals mainly come from the alteration of sandstones. As a whole, the formation of tight reservoir rocks in the study area is closely related to sedimentary facies, composition of framework grain, cement type and content, and development of dissolution.  相似文献   

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