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1.
废水中二苯胺的分析方法有气相色谱和液相色谱法。气相色谱法不能直接测定水中二苯胺的含量，需经过提取、浓缩等过程；液相色谱法则操作费用较高。因此，这2种方法作为选择工艺条件的监测手段都有缺陷。本文利用二苯胺易被氧化的性质建立了水溶液中二苯胺的间接吸光光度法。该法的原理是以铁（Ⅲ）—邻菲罗啉混合液为显色剂在一定的条件下使二苯胺将Fe^3＋还原为Fe^2＋，产生的Fe^2＋再与邻菲罗啉显色并测定，从而间接测定出废水中二苯胺的含量。 相似文献
2.
Fe^2＋ acted as an accessorial factor for many cellular enzymatic reactions is very important for seaweed growth and development, but the Fe^2＋ requirement in nori had not been seen. Porphyra yezoensis cells were separated enzymatically and cultured in a series of sterilized seawater media containing various concentrations of Fe^2＋. The growth development and cell were investigated in this work. Through this experiment, two biologically-meant concentration scales were found, one is low concentrations, 12.1-102.1μg/L, 10-100 times than that in seawater, favoring the development of isolated cells of Porphyra and the other was high concentrations, more than 10mg/L inhibiting the cell growth, leading to the deformity and shrinkage of the cells. At the concentration of 50 mg/L, the cells stopped growing and died eventually. 相似文献
3.
一、岩石的颜色特征
沉积岩的颜色是沉积环境的良好指示剂，岩石中最主要的色素为有机质和铁质。通常有机质含量增加，岩石颜色变深变暗，说明岩石形成于还原环境或强还原环境下。一般碳质反映浅水沼泽弱还原环境，沥青质和分散状铁的硫化物则反映深水或较深的停滞水环境。岩石中含有Fe^2＋的矿物，反映弱氧化或弱还原环境。岩石中含有Fe^3＋矿物，如赤铁矿、褐铁矿则呈红色或褐黄色，反映氧化或强氧化环境，如河流、冲积扇等。 相似文献
4.
Preparation by enzymolysis and bioactivity of iron complex of fish protein hydrolysate （Fe-FPH）from low value fish 总被引：6，自引：0，他引：6
Preparation of Fe^2＋ chelate of fish protein hydrolysate （Fe-FPH） obtained from low value fish proteins was introduced and its bioactivity was studied by compound enzymolysis. The optimum conditions for hydrolysate chelating Fe^2＋ are DH （degree of hydrolysis） at 5%, pH 7.0, 20℃ and 15 min chelating time for FM （material not being defatted）. Four types of Fe-FPH including CA （deposit after chelating）, CB （deposit in 50% of absolute ethanol solution）, CC （suspended deposit in 80% of absolute ethanol solution）, and CD （bottom deposit in 80% of absolute ethanol solution） were fractionated with absolute ethanol from FM. Structural analysis through infra-red spectrum revealed that Fe^2＋ was combined strongly with amino-group and carboxyl-group in each chelate and each Fe^2＋ could form two five-member ring structures. All of the four chelates were shown more significant antioxidative activity and can be used as natural hydrophobic and hydrophilic antioxidant. Among all the chelates, the CB possesses the most effective antioxidative activity at 92% as high as that of a-tocopherol. Among all Fe-FPHs, only CD showed the most effective antibacterial activity against Escherichia coli, Staphylococcus aureus, Salmonella typhi, and Bacillus subtilis and can be used as natural antibacterial. It provides a more effective way for utilization of low value fish proteins and key information of Fe-FPH as additive in food industry. 相似文献
5.
用4种药剂对甘蔗植株进行点心防治甘蔗螟虫,结果表明;各处理都可减少螟害节率,对甘蔗条螟的防治效果显著,其中以（90％敌百虫晶体30g＋18％杀虫双水剂40g）／133m2效果最好,校正防效达83．3％,降低螟害节率33％。 相似文献
6.
周丽湘 《国土资源导刊(湖南)》2002,21(3):225-227
用HNO3和HCl消解烟草样本,在pH为4.2的乙酸-乙酸钠介质中,微量硼与铍试剂Ⅲ形成紫红色络合物,方法灵敏度高,简便易掌握,方法检出限为0.04μg/ml,线性范围为0～0.4μg/ml完全能满足烟草中微量硼的测定要求. 相似文献
7.
升降式深水网箱控制平台的尺寸设计 总被引：1，自引：0，他引：1
控制平台的宽度l与网箱主构架半径r正相关，设计时必须满足网箱框架外侧与平台的距离七大于零，其中：k=1-2＋√2/2r-√h4^2＋1/4l^2＋1/2r^2-√2/2rl,h4为控制平台高度，其受放置区水深h的制约，高度与水深的关系：h=h1＋h2＋h3＋2h4＋1/2H,h1为网衣缩结高度，h2为网衣底部重力装置高度，h3为重力装置到水底的距离，H为网箱放置区台风期预计最大波高。以“HDPE升降式圆形双浮管深水网箱”为应用实例，h=24m，H=7m，r=7.15m，h1=7．0m，h2=1．0m，l=25m，h4=5．0m，在浪高5m，风力10级的情况下，网箱系统工作正常。 相似文献
8.
研究了3种无机盐对隐甲藻（Crypthecodinium cohnii ATCC30556）生长及DHA产量的影响。结果表明：隐甲藻可在NaCl为唯一无机盐的培养基中生长；培养基中NaCl质量浓度为6g/L,Mg^2＋浓度为13．23mmol/L,PO4^3-浓度为7．19mmol/L可满足藻细胞生长和DHA积累的需求，此时隐甲藻有着最大的生物量和DHA产量，分别为3．31g/L和499．93mg/L。 相似文献
9.
岚山头含柯石英榴辉岩呈透镜状构造块体产于晚元古代含霓石碱长花岗质片麻岩中，其原岩为玄武岩浆分离结晶晚期堆积的辉长岩。该榴辉岩典型的共生矿物组合可划分为4个世代：①Cpx1＋Mu1（OrPhen1）＋Qz＋Pl1；②Cpx2（Om1）＋Gr1＋Ky＋Cs；③Cpx3（Om2）＋Gr2＋Phen2＋Ky＋Zo＋Qz；④Pl2＋Tl＋Mrg＋Phen3＋Czo＋Qz。它们分别反映4个变质演化阶段：前榴辉岩相阶段（M1）、柯石英榴辉岩相阶段（M2）、后榴辉岩相第一退变质阶段（M3）及后榴辉岩相第二退变质阶段（M4）。各阶段的变质条件；M1为P≤1．56Gpa，T＝700℃；M2为P＝2．74～2．95GPa，T＝722℃～981℃；M3为P＝1．34～1．54GPa，T＝568℃～589℃；M4为P＝0.61～1．04GPa，T469℃。柯石英榴辉岩相阶段（M2）末期的年龄为613．3±30．4Ma，榴辉岩相第二退变质阶段（M4）的多硅白云母40Ar－39Ar坪年龄为313．49Ma。据上述资料再塑了一个较完整的顺时针PTt轨迹。 相似文献
10.
符史良 《广东海洋大学学报》2002,22(1):64-66
制备固体超强酸SO4 2 - /Fe2 O3,并测定其红外光谱。以乙酸和正丁醇为反应物、固体超强酸SO4 2 - /Fe2 O3为催化剂 ,进行合成乙酸丁酯的研究。实验结果表明 ,固体超强酸SO4 2 - /Fe2 O3在合成乙酸丁酯反应中的催化活性与浓硫酸相当 ,用 0 1mol正丁醇与 0 2mol乙酸反应 ,催化剂用量 0 3g ,回流时间 90min ,乙酸丁酯收率为 63 8%。 相似文献
11.
低值鱼蛋白多肽-铁(Ⅱ)螯合物的酶解制备及其抗氧化、抗菌活性 总被引：1，自引：0，他引：1
以南海低值鱼蛋白为原料,采用木瓜蛋白酶和风味酶的复合酶水解得到多肽水解物(HP),并制备多肽-铁(Ⅱ)螯合物,对螯合工艺及螯合产物的结果及抗氧化和抗菌功能特性进行了初步研究。结果表明:1)水解度为5%的多肽与铁(Ⅱ)螯合效果最佳,螯合率为94.15%;2)化学分析及红外光谱表明活性肽与亚铁离子螯合并形成稳定结构的螯合物;(3)经过50%乙醇(体积分数)沉淀的螯合铁具有明显的抗氧化活性,其抗氧化作用相当于维生素E的90%,经过80%乙醇(体积分数)沉淀的螯合物具有显著的抗枯草牙孢杆菌和金黄色葡萄球菌活性,其抑菌圈均直径为13mm。 相似文献
12.
本文探讨了直接测定三价铁的萃取比色法。该方法基于Fe~(3+)与8-羟基喹啉形成的络合物能被萃取入氯仿层,而在同一体系中的Fe~(2+)与邻菲咯啉形成的络合物却不然,这就使比色法测定有机相中的三价铁成为可能.本方法重现性好,准确度高,RSD％(n=10):1.44,适用于岩石、水系沉积物和土样中三价铁的测定。 相似文献
13.
本文研究了Ｄ_００１大孔阳离子强酸树脂从Ｈ_２ＳＯ_４－ＣＳ（ＮＨ_２）_２溶液中，富集及分离Ａｕ（Ｉ）、Ａｇ（Ｉ）的性能。表明在ｐＨ＝２．０左右，树脂对Ａｕ（Ｔｕ）￣＋_２、Ａｇ（Ｔｕ）￣＋_２（Ｔｕ＝硫脲）有良好的吸附性能，Ａｕ和Ａｇ的吸附容量分别为６１．１８ｍｇ／ｇ－Ｒｅｓｉｎ和９９．１１ｍｇ／ｇ—Ｒｅｓｉｎ。负载柱上的Ａｕ、Ａｇ可分别用ＮａＣＮ—ＮａＯＨ和Ｈ_３ＢＯ_３－ＮａＯＨ－Ｎａ_２Ｓ_２Ｏ_３定量洗脱。可进行一定程度的Ａｕ、Ａｇ分离。 相似文献
14.
Huguangyan Maar Lake is a typical maar lake in the southeast of China.It is well preserved and not disturbed by anthropogenic activities.In this study,microbial community structures in sediment and water samples from Huguangyan Maar Lake were investigated using a high-throughput sequencing method.We found significant differences between the microbial community compositions of the water and the sediment.The sediment samples contained more diverse Bacteria and Archaea than did the water samples.Actinobacteria,Betaproteobacteria,Cyanobacteria,and Deltaproteobacteria predominated in the water samples while Deltaproteobacteria,Anaerolineae,Nitrospira,and Dehalococcoidia were the major bacterial groups in the sediment.As for Archaea,Woesearchaeota(DHVEG-6),unclassified Archaea,and Deep Sea Euryarchaeotic Group were detected at higher abundances in the water,whereas the Miscellaneous Crenarchaeotic Group,Thermoplasmata,and Methanomicrobia were significantly more abundant in the sediment.Interactions between Bacteria and Archaea were common in both the water column and the sediment.The concentrations of major nutrients(NO_3~-,PO_4~(3-),SiO_3~(2-)and NH_4~+)shaped the microbial population structures in the water.At the higher phylogenetic levels including phylum and class,many of the dominant groups were those that were also abundant in other lakes;however,novel microbial populations(unclassified)were often seen at the lower phylogenetic levels.Our study lays a foundation for examining microbial biogeochemical cycling in sequestered lakes or reservoirs. 相似文献
15.
《山地科学学报》2020,(2)
The Sugan Lake Basin is located in the inland arid region of northwestern China,in which groundwater is of great significance to human and ecology.Therefore,it is necessary to understand the chemical characteristics and quality of groundwater in the basin.Based on samples collected from 35 groundwater wells in Sugan Lake Basin,the spatial distribution characteristics of groundwater chemistry,main hydrogeochemical processes and groundwater quality have been discussed in this paper by using the multivariate statistics and hydrochemistry analysis methods.The results showed that the groundwater is weakly alkaline,and its total dissolved solid(TDS)and total hardness(TH) are high,with the average values of 1244.03 mg/L and 492.10 mg/L,respectively.The types of groundwater are mainly HCO_3~--SO_4~(2-)-Ca~(2+)type in the runoff area and Cl~--SO_4~(2-)-Na~+type in the catchment area.Rock weathering and ion exchange are the main controlling factors of regional groundwater chemistry,followed by evaporative crystallization,and human activities have less impact on groundwater.The spatial difference of groundwater quality is obvious,the water quality of the catchment area is not suitable for drinking,and the suitability for plant growth is also poor.The groundwater in the runoff area can be used for drinking,but the hardness is slightly higher,which is more suitable for ecological purpose. 相似文献
16.
《中国海洋湖沼学报》2021,(3)
Bacteria are important regulators of carbon cycling in lakes and are central to sediment ecosystem processes. However, the sediment microbial communities and their respiratory responses to the lake wetland succession are poorly understood. In this study, we collected sediment samples from four different succession points(the Potamogeton lucens zone, the Scirpus tabernaemontani zone, the Scirpus triqueter zone, and the Juncus effusus zone) in the Caohai Wetland of the Guizhou Plateau(China). The bacterial communities at these succession points were studied using a high-throughput sequencing approach. The sediment microbial respiration(SR) was measured using static chambers in the field and basal respiration(BR) was determined in the laboratory. The results show that the dominant bacterial taxa in the sediment was Proteobacteria(34.7%), Chloroflexi(17.8%), Bacteroidetes(7.3%), Acidobacteria(6.6%), and Cyanobacteria(6.1%). Principal coordinate analysis showed that the microbial community structure differs significantly at different sampling points along the successional gradient, indicating that the bacterial community structure is sensitive to the lake wetland succession. Different hydrological regimes and soil characteristics such as NH_4~+-N, Fe~(2+), Mn~(2+), and sediment organic carbon(SOC) content may be important factors responsible for the differences in the sediment microbial characteristics of the different successional stages in the Caohai wetland. Additionally, it was found that the SR increased significantly from the P. lucens zone to the J. effusus zone, but BR had the opposite response. The shifts in the bacterial community structure along the successional gradient may be the main reason for the observed differences in sediment respiration. 相似文献
17.
Shipika Sundriyal Tanuj Shukla Lekhendra Tripathee Dwarika Prashad Dobhal Sameer Kumar Tiwari Uday Bhan 《山地科学学报》2018,15(10):2236-2246
The uncertainty in assessing the numerous atmospheric pollutants transported via wind from arid and semi-arid regions is affecting the glacial ecosystem. In our study area due to the complexity of the system, a prominent seasonal difference noticed among major ions(Ca~(2+), Mg~(2+), SO_4~(2-), and NO_3~-). There is a need for understanding the ions cycling as a whole and the directionality of the feedback loops in the system. Therefore, we provide an appraisal of our current hypothesis for seasonal difference in major ion concentration from snow samples for two corresponding years(2013 and 2015) at Dokriani Glacier. A systematic study of chemical compositionsin the shallow snow pit from Dokriani Glacier was undertaken for the pre-monsoon season to understand the cycling of major ions from atmosphere to solute acquisition process. The intimating connections of ions cycling in snow and its temporal behavior was observed and analyzed through various statistical tests. Among major ions, the SO_4~(2-)has the highest concentration among anions on an average considered as 14.21% in 2013 and 29.46% in 2015. On the other side Ca~(2+) is the dominant cation contributing 28.22% in 2013 and 15.3% in 2015 on average. The average ratio of Na+/Cl-was higher in 2013 whereas lower in 2015. The backward trajectory analysis suggests the possible sources of the ions transported from Central Asia through the Western Disturbance(WD) as a prominent source of winter precipitation mainly in the Central Himalaya. Ionicconcentration of Ca~(2+) in cations was highly dominated while in anion SO_4~(2-)played the major role. Factor analysis and correlation matrix suggested that, the precipitation chemistry is mostly influenced by anthropogenic, crustal, and sea salt sources over the studied region. The elemental cycling through ocean, atmosphere and biosphere opens up new ways to understand the geochemical processes operating at the glacierized catchments of the Himalaya. Moreover, increasing the field-based studies in the coming decades would also have the certain advantage in overcoming the conceptual and computational geochemical modelling difficulties. 相似文献
18.
基于紧凑约束最小二乘优化反演算法，利用2014~2017年地表重力变化观测成果，反演得到2017年九寨沟MS7.0地震前震中及周边地区的地壳三维密度变化。结果表明：1）在震中及周边地区出现大范围的重力变化，并沿张掖-西宁-九寨沟一带形成最大值达9 μGal的重力变化梯度带；2） 地壳密度变化量随深度增加而增大，其中在45 km附近达到最大，为0.2 g/cm3；3） 震中及邻区范围内形成密度变化的正负四象限分布（2014-04~2017-04），其表现的物质运移方向呈左旋走滑式分布，与震源机制解基本一致。据此推断，在震前产生了与地震孕育相关的深部构造运动，而强震易发生在物质运移汇聚地方。 相似文献
19.
吉林西部地区第四系潜水水质影响因素的R型因子分析 总被引：7，自引：0，他引：7
利用R型因子分析法对吉林西部地区第四系潜水样的水化学数据进行分析,识别出影响地下水化学组成的4个主因子。因子1以Na ,HCO3-和F-为主,揭示了土壤的溶滤作用对地下水化学成分的影响;因子2以Cl-,SO42-和Ca2 为主,反映蒸发浓缩作用对地下水化学成分的影响;因子3以K 和pH值为主,代表地下水的弱碱环境地球化学背景;因子4以NO3-为主,反映了人类活动(化肥和农药的广泛施用、大中城市的生活污水和工业污水的污染)对地下水化学成分的影响作用。 相似文献
20.
魏艳华 《成都信息工程学院学报》2007,22(1):84-87
跳频通信是一种有效的抗干扰通信技术，跳频序列的性能对跳频通信系统的性能有着决定性的影响。重点阐述了RS码作为跳频序列的编码方法及其性能，介绍了RS码序列的具体编写方法，并进行了计算机仿真，计算了所生成RS跳频序列的汉明相关性能。 相似文献