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1.
碱消解-高效液相色谱-电感耦合等离子体质谱法测定生物样品中的甲基汞和乙基汞 总被引:7,自引:2,他引:5
建立了碱消解-高效液相色谱-电感耦合等离子体质谱联用系统测定生物样品中甲基汞(MeHg)与乙基汞(EtHg)的分析方法。为提高灵敏度,选用微流量的PFA雾化器,在优化的检测条件下,MeHg及EtHg检出限可达到0.036μg/L和0.03μg/L;线性范围达到4个数量级,两条工作曲线线性相关系数为1。对1.78μg/L MeHg、1.65μg/L EtHg的混合标准溶液重复测定7次,色谱峰面积的相对标准偏差(RSD)分别为1.79%和1.44%。对标准物质BCR 464(金枪鱼)的分析结果表明,测定值与标准值基本吻合,但略低于标准值;甲基汞和乙基汞的加标回收率分别为85.9%和84.5%。高效液相色谱与质谱联用技术的高灵敏度和低检出限能够满足生物样品中汞形态定量分析的要求。 相似文献
2.
Eleven surface soil samples from calcareous soils of industrial areas in Hamadan Province, western Iran were analyzed for
total concentrations of Zn, Cd, Ni, Cu and Pb and were sequentially extracted into six fractions to determine the bioavailability
of various heavy metal forms. Total Zn, Cd, Ni, Cu and Pb concentrations of the contaminated soils were 658 (57–5,803), 125.8
(1.18–1,361), 45.6 (30.7–64.4), 29.7 (11.7–83.5) and 2,419 (66–24,850) mg kg−1, respectively. The soils were polluted with Zn, Pb, and Cu to some extent and heavily polluted with Cd. Nickel values were
not above regulatory limits. Copper existed in soil mainly in residual (RES) and organic (OM) fractions (about 42 and 33%,
respectively), whereas Zn occurred essentially as RES fraction (about 69%). The considerable presence of Cd (30.8%) and Pb
(39%) in the CARB fraction suggests these elements have high potential biavailability and leachability in soils from contaminated
soils. The mobile and bioavailable (EXCH and CARB) fractions of Zn, Cd, Ni, Cu, and Pb in contaminated soils averaged (7.3,
40.4, 16, 12.9 and 40.8%), respectively, which suggests that the mobility and bioavailability of the five metals probably
decline in the following order: Cd = Pb > Ni > Cu > Zn. 相似文献
3.
Regional distribution pattern of groundwater heavy metals resulting from agricultural activities 总被引:18,自引:0,他引:18
Contaminations of groundwater by heavy metals due to agricultural activities are growing recently. The objective of this study
was to evaluate and map regional patterns of heavy metals (Cd, Zn and Cu) in groundwater on a plain with high agricultural
activities. The study was conducted to investigate the concentration of heavy metals and distribution in groundwater in regions
of Shush Danial and Andimeshk aquifers in the southern part of Iran. Presently, groundwater is the only appropriate and widely
used source of drinking water for rural and urban communities in this region. The region covers an area of 1,100 km2 between the Dez and Karkhe rivers, which lead to the Persian Gulf. For this study, the region was divided into four sub-regions
A, B, C and D. Additionally, 168 groundwater samples were collected from 42 water wells during the earlier months of 2004.
The flame atomic absorption spectrometry (AAS-Flame) was used to measure the concentration of heavy metals in water samples
and the Surfer software was used for determination of the contour map of metal distribution. The results demonstrated that
in all of the samples, Cd and Zn concentrations were below the EPA MCLG and EPA secondary standard, respectively. However,
the Cu contents of 4.8 % of all samples were higher than EPA MCL. It is also indicated that the concentrations of metals were
more pronounced at the southern part of the studied region than at the others. The analysis of fertilizers applied for agricultural
activities at this region also indicated that a great majority of the above-mentioned heavy metals were discharged into the
environment. Absence of confining layers, proximity to land surface, excess agricultural activities in the southern part and
groundwater flow direction that is generally from the north to the southern parts in this area make the southern region of
the Shush plain especially vulnerable to pollution by heavy metals than by other contaminants. 相似文献
4.
Abstract. The secondary production of Spisula subtruncata (somatic production) is calculated in the framework of a benthic monitoring study in a coastal area. The temporal trends of density, biomass and growth increments are examined in the three year-classes present. These are compared to certain physical and chemical parameters. 相似文献
5.
厦门海洋生物入侵的危害及管理对策 总被引:4,自引:1,他引:4
本文系统地分析了厦门海洋生物入侵的成因、现状、危害及治理方法,认为互花米草和海洋动物沙筛贝是主要的入侵物种,其严重的生态、经济和社会危害不可低估.同时明确防止海洋生物入侵的总体目标,进而提出强化管理的系列对策. 相似文献
6.
Roles of Biogeochemical Processes in the Oceanic Carbon Cycle Described with a Simple Coupled Physical-Biogeochemical Model 总被引:1,自引:0,他引:1
Masahiko?FujiiEmail author Motoyoshi?Ikeda Yasuhiro?Yamanaka 《Journal of Oceanography》2005,61(5):803-815
To evaluate the contribution of biogeochemical processes to the oceanic carbon cycle and to calculate the ratio of calcium
carbonate to organic carbon downward export, we have incorporated biological and alkalinity pumps in the yoked high-latitude
exchange/interior diffusion-advection (YOLDA) model. The biogeochemical processes are represented by four parameters. The
values of the parameters are tuned so that the model can reproduce the observed phosphate and alkalinity distributions in
each oceanic region. The sensitivity of the model to the biogeochemical parameters shows that biological production rates
in the euphotic zone and decomposition depths of particulate matters significantly influence horizontal and vertical distributions
of biogeochemical substances. The modeled vertical fluxes of particulate organic phosphorus and calcium carbonate are converted
to vertical carbon fluxes by the biological pump and the alkalinity pump, respectively. The downward carbon flux from the
surface layer to the deep layer in the entire region is estimated to be 3.36 PgC/yr, which consists of 2.93 PgC/yr from the
biological pump and 0.43 PgC/yr from the alkalinity pump, which is consistent with previous studies. The modeled rain ratio
is higher with depth and higher in the Pacific and Indian Oceans than in the Atlantic Ocean. The global rain ratio at the
surface layer is calculated to be 0.14 to 0.15. This value lies between the lower and higher ends of the previous estimates,
which range widely from 0.05 to 0.25. This study indicates that the rain ratio is unlikely to be higher than 0.15, at least
in the surface waters. 相似文献
7.
栉孔扇贝(Chlamys farreri) 血细胞类型及抗菌力的研究 总被引:1,自引:0,他引:1
用2种方法将栉孔扇贝血细胞分为2大类透明细胞、颗粒细胞.吉姆萨染色观察,透明细胞的细胞质中颗粒很少,细胞核圆形,居中,细胞质较少,核质比大;颗粒细胞比透明细胞大且多,染色深,但核质比小,在细胞质中有颗粒,有些颗粒细胞具双核.密度梯度离心结果,透明细胞主要位于上层,颗粒细胞则大部分位于下层.吞噬力、抗菌活力、溶菌活力及活性氧检测结果表明,颗粒细胞均强于透明细胞. 相似文献
8.
利用雨生红球藻生产虾青素的研究进展 总被引:20,自引:0,他引:20
作为天然虾青素的最佳生物来源,雨生红球藻已成为近年来国内外微藻研究的热点之一.本文综述了国内外雨生红球藻培养及虾青素积累的研究进展,介绍了国外天然虾青素商业生产的现状,并对现存的主要问题和发展方向做出阐述,以期推动国内利用雨生红球藻生产虾青素的商业化进程。 相似文献
9.
赤潮生物种类特征光谱获取技术 总被引:1,自引:0,他引:1
较为系统地研究了赤潮生物水体反射率曲线获取方法。通过对 2类反射率反演方法得出的反射率曲线与实际反射率曲线进行比较 ,得出在不具备大气环境参数的情况下 ,经验线性法的反演结果与实际反射率曲线最接近的结论 ,并进一步对正常海水和赤潮生物水体的光谱特性进行分析 ,提取出赤潮生物水体的特征光谱。这是进行赤潮监测和识别的重要前提 相似文献
10.