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121.
122.
Breakdown of hydrous ringwoodite to pyroxene and spinelloid at high P and T and oxidizing conditions
To get deeper insight into the phase relations in the end-member system Fe2SiO4 and in the system (Fe, Mg)2SiO4 experiments were performed in a multi-anvil apparatus at 7 and 13 GPa and 1,000–1,200°C as a function of oxygen fugacity.
The oxygen fugacity was varied using the solid oxygen buffer systems Fe/FeO, quartz–fayalite–magnetite, MtW and Ni/NiO. The
run products were characterized by electron microprobe, Raman- and FTIR-spectroscopy, X-ray powder diffraction and transmission
electron microscopy. At fO2 corresponding to Ni/NiO Fe-ringwoodite transforms to ferrosilite and spinelloid according to the reaction: 9 Fe2SiO4 + O2 = 6 FeSiO3 + 5 Fe2.40Si0.60O4. Refinement of site occupancies in combination with stoichiometric Fe3+ calculations show that 32% of the total Fe is incorporated as Fe3+ according to From the Rietveld refinement we identified spl as spinelloid III (isostructural with wadsleyite) and/or spinelloid V. As
we used water in excess in the experiments the run products were also analyzed for structural water incorporation. Adding
Mg to the system increases the stability field of ringwoodite to higher oxygen fugacity and the spinel structure seems to
accept higher Fe3+ but also water concentrations that may be linked. At oxygen fugacity corresponding to MtW conditions similar phase relations
in respect to the breakdown reaction in the Fe-end-member system were observed but with a strong fractionation of Fe into
spl and Mg into coexisting cpx. Thus, through this strong fractionation it is possible to stabilize very Fe-rich wadsleyite
with considerable Fe3+ concentrations even at an intermediate Fe–Mg bulk composition: assuming constant K
D independent on composition and a bulk composition of x
Fe = 0.44 this fractionation would stabilize spl with x
Fe = 0.72. Thus, spl could be a potential Fe3+ bearing phase at P–T conditions of the transition zone but because of the oxidizing conditions and the Fe-rich bulk composition
needed one would expect it more in subduction zone environments than in the transition zone in senso stricto.
相似文献
M. Koch-MüllerEmail: |
123.
Chris Soulsby Bernhard Scheliga Aaron Neill Jean-Christophe Comte Doerthe Tetzlaff 《水文研究》2021,35(6):e14206
The drought of summer 2018, which affected much of Northern Europe, resulted in low river flows, biodiversity loss and threats to water supplies. In some regions, like the Scottish Highlands, the summer drought followed two consecutive, anomalously dry, winter periods. Here, we examine how the drought, and its antecedent conditions, affected soil moisture, groundwater storage, and low flows in the Bruntland Burn; a sub-catchment of the Girnock Burn long-term observatory in the Scottish Cairngorm Mountains. Fifty years of rainfall-runoff observations and long-term modelling studies in the Girnock provided unique contextualisation of this extreme event in relation to more usual summer storage dynamics. Whilst summer precipitation in 2018 was only 63% of the long-term mean, soil moisture storage across much of the catchment were less than half of their summer average and seasonal groundwater levels were 0.5 m lower than normal. Hydrometric and isotopic observations showed that ~100 mm of river flows during the summer (May-Sept) were sustained almost entirely by groundwater drainage, representing ~30% of evapotranspiration that occurred over the same period. A key reason that the summer drought was so severe was because the preceding two winters were also dry and failed to adequately replenish catchment soil moisture and groundwater stores. As a result, the drought had the biggest catchment storage deficits for over a decade, and likely since 1975–1976. Despite this, recovery was rapid in autumn/winter 2018, with soil and groundwater stores returning to normal winter values, along with stream flows. The study emphasizes how long-term data from experimental sites are key to understanding the non-linear flux-storage interactions in catchments and the “memory effects” that govern the evolution of, and recovery from, droughts. This is invaluable both in terms of (a) giving insights into hydrological behaviours that will become more common water resource management problems in the future under climate change and (b) providing extreme data to challenge hydrological models. 相似文献
124.
通过详细的野外地质调查,发现扬子西缘小相岭地区苏雄组火山岩由巨厚的酸性-中酸性熔岩、火山碎屑岩和少量基性熔岩组成,在小相岭山脊两侧首次厘定4处古火山机构。其中,阳糯雪山古火山机构最壮观,是由火山颈相、溢流相、爆发相和火山沉积相构成的完整古火山机构。通过系统的地质剖面研究,发现该古火山机构存在2次喷发亚旋回和15个火山韵律,2次喷发亚旋回之间出现了1次明显的火山间歇期。小相岭地区古火山机构的发现,进一步厘定了苏雄组火山岩的喷发方式和构建特征,对进一步研究苏雄组酸性火山碎屑岩的起源及新元古代陆内裂谷作用具有重要意义。 相似文献
125.
目的:建立炎可宁丸质量标准。方法:采用显微鉴别法鉴别黄连。采用薄层色谱法(TLC)鉴别黄柏、大黄、黄芩、板蓝根、黄连。采用高效液相色谱(HPLC)法测定大黄素与大黄酚的含量,使用Phenomenex Luna C18色谱柱(4.6 mm ×250 mm,5μm),以甲醇-0.1%磷酸溶液(85∶15)为流动相,流速为1.0 ml/min,柱温为30℃,检测波长为254 nm。采用HPLC法测定黄芩苷的含量,使用CAPCELL PAK C18色谱柱(4.6 mm×250 mm,5μm),以甲醇-0.1%磷酸溶液(45∶55)为流动相,流速为1.0 ml/min,柱温为30℃,检测波长为280 nm。结果:薄层色谱斑点清晰;大黄素和大黄素酚的线性范围分别为9.3~465.0 ng、11.6~580.0 ng,加样回收率分别为93.3%、98.0%,RSD分别为1.8%、2.7%;黄芩苷的线性范围为68~3400 ng,加样回收率为97.2%,RSD为1.2%。结论:本法简便可靠、结果准确,可用于该制剂的质量控制。 相似文献
126.
Luis Andrés Guillén Mary Beth Adams Emily Elliot Jason Hubbart Charlene Kelly Brenden McNeil William Peterjohn Nicolas Zegre 《水文研究》2021,35(4):e14106
Long-term experimental watershed studies have significantly influenced our global understanding of hydrological processes. The discovery and characterization of how stream water quantity and quality respond to a changing environment (e.g. land-use change, acidic deposition) has only been possible due to the establishment of catchments devoted to long-term study. One such catchment is the Fernow Experimental Forest (FEF) located in the headwaters of the Appalachian Mountains in West Virginia, a region that provides essential freshwater ecosystem services to eastern and mid-western United States communities. Established in 1934, the FEF is among the earliest experimental watershed studies in the Eastern United States that continues to address emergent challenges to forest ecosystems, including climate change and other threats to forest health. This data note describes available data and presents some findings from more than 50 years of hydrologic research at the FEF. During the first few decades, research at the FEF focused on the relationship between forest management and hydrological processes—especially those related to the overall water balance. Later, research included the examination of interactions between hydrology and soil erosion, biogeochemistry, N-saturation, and acid deposition. Hydro-climatologic and water quality datasets from long-term measurements and data from short-duration studies are publicly available to provide new insights and foster collaborations that will continue to advance our understanding of hydrology in forested headwater catchments. As a result of its rich history of research and abundance of long-term data, the FEF is positioned to continue to advance understanding of forest ecosystems in a time of unprecedented change. 相似文献
127.
Equivalent continuum strain calculations based on 3D particle kinematic measurements of sand 下载免费PDF全文
Siavash Amirrahmat Khalid A. Alshibli Maha F. Jarrar Boning Zhang Richard A. Regueiro 《国际地质力学数值与分析法杂志》2018,42(8):999-1015
Constitutive modeling of granular materials has been a subject of extensive research for many years. While the calculation of the Cauchy stress tensor using the discrete element method has been well established in the literature, the formulation and interpretation of the strain tensor are not as well documented. According to Bagi, 1 researchers mostly adopt well‐known continuum or discrete microstructural approaches to calculate strains within granular materials. However, neither of the 2 approaches can fully capture the behavior of granular materials. They are considered complementary to each other where each has its own strengths and limitations in solving granular‐mechanics problems. Zhang and Regueiro 2 proposed an equivalent continuum approach to calculating finite strain measures at the local level in granular materials subjected to large deformations. They used three‐dimensional discrete element method results to compare the proposed strains measures. This paper presents an experimental application of the Zhang and Regueiro 2 approach using three‐dimensional synchrotron microcomputed tomography images of a sheared Ottawa sand specimen. Invariant Eulerian finite strain measures were calculated for representative element volumes within the specimen. The spatial maps of Eulerian octahedral shear and volumetric strain were used to identify zones of intense shearing within the specimen and compared well with maps of incremental particle translation and rotation for the same specimen. The local Eulerian volumetric strain was compared to the global volumetric strains, which also can be considered as an averaging of all local Eulerian volumetric strains. 相似文献
128.
Vajapeyam S. Srinivasan Hugo M. de Alcântara Carlos de O. Galvão Ulisses A. Bezerra John E. de Brito Leite Cunha 《水文研究》2021,35(5):e14194
Catchments have highly variable yields of runoff and soil erosion. The size, land use and the surface cover play a significant role and influence the catchment response and parameter values of simulation models. Two experimental basins—the Cariri basins—were equipped in a semi-arid region of Brazil, for obtaining runoff and sediment yield at different catchment scales, as well as, to evaluate the influence of the land use and surface cover. In the first basin, located in the municipality of Sumé, the field studies were carried out at two different scales: four micro-catchments with an area of around 0.5 ha and nine standard Wischmeier-type erosion plots of 100 m2. The experimental units had varied vegetation and management. They were subjected only to natural rainfall events, and were monitored from 1982 to 1991. The total runoff and total sediment yield were determined for each of the events. The installations in the second basin, in the municipality of São João do Cariri, from 1999, include two erosion plots, three micro-catchments, and two sub-catchments of a small basin. These basins are still being monitored for runoff and sediment production. Among the micro-catchments two are nested to detect any scale effect at the micro-catchment level. Nearly 600 events of precipitation, that produced runoff in at least one of the experimental units, have been registered. These data have been used to evaluate the influence of various factors, including cultivation practices and to calibrate hydrological models for plots and micro-catchments. Parameters have been tested by means of cross validations among micro-catchments and sub-catchments. The data sets are made available to all the catchment hydrology researchers and others at https://doi.org/10.5281/zenodo.4690886 . 相似文献
129.
北斗新一代试验星观测数据质量分析 总被引:1,自引:0,他引:1
5颗北斗新一代试验星搭载了包括B1C、B2a和B2b的诸多新体制民用信号,并且为了与北斗区域系统平稳过渡而搭载了B1I和B3I两个旧体制信号。采集了来自国内的6个监测站7 d的试验星观测数据,针对信号载噪比和码伪距多路径偏差分析了新一代试验星观测数据质量。结果表明,新一代试验星信号的各项指标整体较北斗区域系统卫星更好。前者载噪比较高,虽然仍发现了部分测站数据微小的多路径波动,但通过实时相位平滑伪距的方法可以很好地消除之;新一代试验星上B3I与B1I频点的载噪比最大,B2a和B2b次之,B1C的载噪比最小,且不同测站的观测结果存在明显差异;新一代试验星各频点的MP基本相同,但B2a、B2b和B3I频点MP的RMS明显小于B1I和B1C频点的结果。 相似文献
130.
鄂尔多斯盆地镇北地区长3储层微观非均质性的实验分析 总被引:10,自引:0,他引:10
油气储层的微观非均质性特征是储层地质学研究的重要内容之一。本文的目的是研究鄂尔多斯盆地镇北地区长3储层微观非均质性特征,研究方法是利用真实砂岩微观模型实验。通过实验发现鄂尔多斯盆地镇北地区长3和储层为致密型砂岩,真实砂岩微观模型实验直观地显示出鄂尔多斯盆地镇北地区长3储层具有很强的微观非均质性,砂岩的成岩作用和孔隙结构是影响本区长3储层微观非均质性的主要原因。在低渗透砂岩中,溶蚀作用引起砂岩产生强烈的非均质性,而这些砂岩则形成长3储层的高渗带。 相似文献