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121.
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Taeko Shinonaga Helmuth Aigner Dilani Klose Peter Spinder Heinz Fröschl David Donohue 《Geostandards and Geoanalytical Research》2008,32(1):93-101
The recommended concentrations of 239Pu, 240Pu and 239+240Pu in reference material IAEA‐315 (marine sediment) were estimated by three analytical methods: isotope dilution thermal ionisation mass spectrometry (TIMS), isotope dilution inductively coupled plasma‐mass spectrometry (ICP‐MS) and alpha spectrometry. The determination of 239Pu and 240Pu (239+240Pu by alpha spectrometry) was carried out with samples from randomly selected bottles using each method. Plutonium‐238 was also measured by alpha spectrometry. A plutonium‐242 reference material was used as a spike for the quantitative analysis. The influence of 242Pu in the samples was therefore calculated; however, this contribution was less than the range of uncertainty and did not influence the final results. The obtained data were statistically analysed using variance component analysis and paired comparison. The combined standard uncertainties from “method/measurement”, “bottle” and “sub‐sample” were in the order of 3 to 6%. The main contributions to the uncertainty were from the material heterogeneity and from systematic differences between methods. Based on this study with twenty‐seven analyses using 10–14 g sample mass, concentrations of (38 ± 3) Bq kg?1, (28 ± 3) Bq kg?1 and (66 ± 4) Bq kg?1 are proposed as recommended values for 239Pu, 240Pu and 239+240Pu, respectively, and (9.5 ± 0.4) Bq kg?1 for 238Pu as an information value in reference material IAEA‐315. In mass concentration units, these amount to (16.4 ± 1.2) ng kg?1, (3.3 ± 0.4) ng kg?1 and (0.015 ± 0.003) ng kg?1 for 239Pu, 240Pu and 238Pu, respectively. The certified reference materials NIST 4350B and NIST 4354 were also analysed by TIMS for quality assurance of the method used in this study. 相似文献
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利用傅立叶变换红外光谱(FTIR)分析技术,对乌达矿区低温氧化和新鲜煤样进行了红外光谱测试,通过两类煤样的特征官能团吸光度的对比分析.揭示了煤在氧化前后特征官能团的变化规律:氧化后的煤样中脂肪族和芳烃CH减少,酸酐C=O从无到有,芳烃骨架C=C基本不变,进而研究了其对煤自燃倾向性的影响。结果表明脂肪族和羟基含量越高,煤自燃倾向性越大。 相似文献
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126.
J. B. W. Day 《Environmental Geology》1996,27(2):77-78
Predictably, in a country such as Britain, with its preponderance of consolidated, sedimentary, mainly fissure-flow aquifers, there is a very large number of springs, many of which are, or have been, used for public supply. Migratory springs are a feature of the British (Ur. Cretaceous) Chalk, the most important British aquifer. The Chalk's low specific yield and high capillary moisture retention together give rise to very considerable fluctuations (more than 33 m in some areas) of the unconfined water table. Along the gentle dip slopes of the Chalk (North and South Downs of southern and southeastern England) springs may migrate laterally for several miles, giving rise to seasonal streams locally known as bournes or lavants. However, springs such as at Duncton, West Sussex, at the base of the much steeper scarp slopes of the Chalk, form point sources, the flows from which tend to be relatively steady; such springs commonly supply and are the original reason for the existence of many of the small towns and villages which nestle along the bases of the chalk scarps of Sussex and Kent.Where the Chalk forms coastal cliffs, a number of springs break out at the base of the cliff between high and low tide levels; there are major chalk coastal springs, for instance, at St. Margaret's Bay (Kent) and at Arish Mells, east of Lulworth Cove, Dorset. Such springs are not used for direct supply (their salinity is usually too high) but are indicators of the presence of local reserves of groundwater for possible future development. 相似文献
127.
Summary The newly developed light sectioning method has been used to investigate some of the causes and costs of overbreak and underbreak. Investigations at the Aquamilpa Hydroelectric Project in Mexico have shown decreased overbreak and increased underbreak as a result of increased rock quality and decreased explosive energy. A new measure of explosive energy, the perimeter powder factor (PPF), has been defined and shown to be useful in the context of tunnel-wall rock damage. Tentative results indicate that explosive energy (PPF) may be a more important factor in producing underbreak, whereas rock quality may be a greater factor in producing overbreak. A site-specific equation is given for predicting overbreak or underbreak as a function of rock quality and explosive energy, with an evaluation of the cost of underbreak and overbreak. 相似文献
128.
We have obtained infrared colors and limiting magnitudes from 1.25–4.8µm for a sample of 26 of the cm continuum radio sources located in the core of the Oph molecular cloud. Their colors demonstrate that the majority of the sources appear to be heavily reddened objects surrounded by circumstellar accretion disks. In these cases the radio emission most likely diagnoses accretion driven energetic outflow phenomena: either ionized winds or possibly synchrotron emission from shocked gas associated with stellar jets. 相似文献
129.
为研究天环坳陷北段下古生界天然气成藏规律,利用探井资料和有机地球化学方法,评价了天环坳陷北段奥陶系烃源岩特征并恢复其成熟演化史。天环坳陷北段奥陶系乌拉力克组和克里摩里组烃源岩有机碳含量和生烃潜量相对较高,烃源岩有机质丰度以中等—好为主,少部分为差烃源岩;三道坎组和桌子山组烃源岩以差为主。干酪根组分鉴定表明,天环坳陷北段奥陶系烃源岩主要为Ⅱ1~Ⅰ型干酪根,热演化程度高,处于生干气阶段。成熟演化史模拟显示,古生代—中生代早期地温梯度低,地层埋藏浅,烃源岩成熟演化程度低。燕山期,由于构造热事件,地温梯度迅速升高,早白垩世烃源岩经历的最高温度超过200℃,达到生气高峰期,早白垩世是油气成藏的主要时期。早白垩世之后,鄂尔多斯盆地整体抬升,地温梯度减小,生烃作用停止。 相似文献
130.
为了研究福建省有效致灾雷电的分布情况,基于福建省2004—2012年闪电定位数据及雷击人员伤亡数据、福建省L17级谷歌遥感影像瓦片,引入卷积神经网络模型对遥感影像所在区域是否属于人员活动的属性进行建模、训练和预测,得到福建省人员活动属性的格点产品,结合福建省历史雷电数据对有效致灾的雷电分布情况进行了分析,结果表明:①设计的遥感影像+CNN识别模型具有一定的可行性和准确率,通过显著性水平为0.01的假设检验;②福建省有63.55%的格点为无人员活动区域;③平均有45.36%的闪电落在无人员活动的区域,因地制宜地对其他致灾闪电进行预警是提高应急减灾服务效果的可行途径;④有效致灾雷电密度与历史雷击人员伤亡数据的相关性远大于常规雷电密度与历史雷击人员伤亡数据的相关性,有效致灾雷电分布在表征雷电灾害上比常规雷电分布更具有指示意义。 相似文献