Combining ECCI and FIB milling techniques to prepare site-specific TEM samples for crystal defect analysis of deformed minerals at high pressure     

Nobuyoshi Miyajima  Tommaso Mandolini  Florian Heidelbach  Caroline Bollinger 《Comptes Rendus Geoscience》2019,351(2-3):295-301

Dislocation microstructures in experimentally deformed single-crystal pyrope-rich garnet, (Mg,Fe)₃(Al,Cr)₃Si₃O₁₂, and polycrystalline forsterite, Mg₂SiO₄, were investigated by using electron channeling contrast imaging (ECCI) and transmission electron microscopy (TEM) combined with a focused ion beam (FIB)-microsampling. In the orientation-optimized ECCI method, we successfully observed individual dislocations across subgrain boundaries in a low-atomic-number mineral, pyrope-rich garnet (averaged Z-numbers, AZs ～ 10). Dislocations in a deformed forsterite (iron-free olivine) were also visible in the ECCI. In the ECCI on the single-crystal garnet, deformation bands consisting of dislocations, unusual contrasts in stripes and inhomogeneous distributions of sub-micrometer-sized pores were found. Further site-specific TEM observation on the deformation band revealed a high density of partial dislocations and stacking fault ribbons. The site-specific characterizations from ECCI to TEM, with assistance of FIB, can provide a new approach to investigate dislocation microstructures of deformed materials at high pressure and high temperature.  相似文献   

The Effects of Different HITRAN Versions on Calculated Long-Wave Radiation and Uncertainty Evaluation   总被引：1，自引：0，他引：1       下载免费PDF全文

LU Peng  ZHANG Hu  JING Xianwen 《Acta Meteorologica Sinica》2012,26(3):389-398

Four editions of the High Resolution Transmission (HITRAN) databases (HITRAN96, HITRAN2K, HITRAN04, and HITRAN08) are compared by using a line-by-line (LBL) radiative model in the long-wave calculation for six typical atmospheres. The results show that differences in downward radiative fluxes between HITRAN96 and HITRAN08 at the surface can reach a maximum of 1.70 W m 2 for tropical atmospheres. The largest difference in heating rate between HITRAN96 and HITRAN08 can reach 0.1 K day 1 for midlatitude summer atmosphere. Uncertainties caused by line intensity and air-broadened halfwidths are also evaluated in this work using the uncertainty codes given in HITRAN08. The uncertainty is found to be 1.92 W m 2 for upward fluxes at the top of the atmosphere (TOA) and 1.97 W m 2 for downward fluxes at the surface. The largest heating rate caused by the uncertainty of line intensity and air-broadened half-width can reach 0.5 K day 1 . The differences in optical depths between 1300 and 1700 cm 1 caused by different HITRAN versions are larger than those caused by the uncertainties in intensity and air-broadened half-width. This paper suggests that there is inaccurate representation of line parameters over some spectral ranges in HITRAN and more attention should be paid to these ranges in fields such as remote sensing.  相似文献   

A highly wave dissipation offshore breakwater     

Sheng-Wen Twu  Cheng-Chung Chieu 《Ocean Engineering》2000,27(3):352

The aim of this paper is to develop an offshore breakwater, for which coefficients of both the wave reflection and transmission have low values. The breakwater is suggested to compose of n layers of porous materials with different porosities. A complex eigen function method is used in the theoretical analysis. Continuities of both mass flux and fluid pressure are assumed at interfaces between every two adjoining porous materials and at the interface between end materials and water region. Following a series of mathematical processes, the coefficients of the wave transmission and reflection along with the wave energy loss are calculated. The porosity of materials is varied in computations; and results are compared among structures composing of different layers of porous materials. A single layer offshore breakwater is shown to reduce simultaneously the coefficients of transmission and reflection only when the structure is very wide in the direction of wave propagation, and the structure material has a high porosity. A multilayer breakwater, however, can function well in reducing both coefficients at a much narrower width; structure having more layers can be more effective at narrower width. Finally, several experiments are conducted; theoretical computations and experimental results agree well.  相似文献   

Rock fracture compliance derived from time delays of elastic waves     

M. Möllhoff  C.J. Bean  P.G. Meredith 《Geophysical Prospecting》2010,58(6):1111-1122

The purpose of this study is to compare the reliability of various methods of estimating normal rock fracture compliance from elastic wave measurements. We compare ultrasonic through‐transmission laboratory measurements for a smooth fracture in a Westerly granite specimen with numerical simulations and analytical solutions. The focus is on deriving compliance from time delays. The influence of specimen and source transducer width was constrained using numerical wave simulations. We find that measured ultrasonic phase delays are better suited to estimate the fracture compliance than group delays. Using the frequency domain instead of the time domain increases the accuracy of the fracture compliance estimates. We further show that for cases where precise phase delay measurements are unavailable, employing first break times in conjunction with numerical simulations can be considered as an alternative.  相似文献   

多种传输方式在青海数字地震台网中的应用     

郭葆庆  孟鑫 《高原地震》2010,22(1):50-53

如何保障数据实时、连续的传输是数字地震台网运行的重要工作,本文就青海省数字地震台网所采用的几种传输方式进行了简单说明。经过近2年的运行,说明这几种传输方式在青海数字地震台网运行过程中经受住了考验,保证了台网的正常运行,同时也为以后的数据传输方式积累了经验。  相似文献   

Microbial remains in some earliest Earth rocks: Comparison with a potential modern analogue   总被引：1，自引：1，他引：0  

Miryam Glikson  Lawrence J. Duck  Suzanne D. Golding  Axel Hofmann  Robert Bolhar  Robyn Webb  Justice C.F. Baiano  Lindsay I. Sly 《Precambrian Research》2008,164(3-4):187-200

Carbonaceous matter (CM) from ca. 3.5 Ga hydrothermal black cherts of the Pilbara Craton of Western Australia and the Barberton Greenstone Belt of South Africa yielded transmission electron microscopy (TEM) images that are suggestive of microbial remains and possible remnants of microbial cell walls. These are compared to a potential modern analogue, the hyperthermophilic Methanocaldococcus jannaschii, derived from an active seafloor hydrothermal environment and cultured under similar conditions. A striking resemblance to the early Archaean forms was evident in wall structure and thermal degradation mode. Cell disintegration of the cultures occurred at 100 °C marking the limits of life. Complete disintegration, deformation and shrinkage occurred at 132 °C. A multidisciplinary approach to the characterisation of the CM was undertaken using organic petrology, TEM coupled with electron dispersive spectral analysis (EDS), high resolution TEM (HRTEM) to determine molecular ordering, and elemental and carbon isotope geochemistry. Reflectance measurements of the CM to determine thermal stress yielded a range of values corresponding to several populations, and pointing to different sources and processes. The δ¹³C values of Dresser Formation CM (−36.5 to −32.1‰) are negatively correlated with TOC (0.13–0.75%) and positively correlated with C/N ratio (134–569), which is interpreted to reflect the relative abundance of high R_o/oxidised/recycled CM and preferential loss of ¹²C and N during thermal maturation. TEM observations, inferred carbon isotopic heterogeneity and isotope fractionations of −27 to −32‰ are consistent with the activity of chemosynthetic microbes in a seafloor hydrothermal system where rapid silicification at relatively low temperature preserved the CM.  相似文献   

Experimental study on the performance of the multiple-layer breakwater     

Yongxue Wang  Guoyu Wang  Guangwei Li 《Ocean Engineering》2006,33(13):1829-1839

Based on the idea of disturbing the water motion in the upright direction, a new kind of multiple-layer breakwater is proposed in this article, which mainly consists of several horizontal plates. The breakwater's performance of dissipating waves has been investigated in detail in the regular wave tests. The factors identified with the characteristics of the breakwater are discussed, such as the relative width, the wave steepness and the models geometrical parameters (the width and the gap). The comparison and analysis of the transmission and reflection coefficients with respect to different factors are presented. The model test results indicate that the multiple-layer breakwater has the good characteristic of dissipating waves. Further more, only in a little extent can it reflect the waves. The multiple-layer breakwater proposed in the paper is very significative to promote the open type breakwater to be the permanent wave attenuator in the application.  相似文献   

Hydrodynamic pressures and forces on quadrant front face pile supported breakwater     

V. Sundar  B. V. V. Subba rao 《Ocean Engineering》2002,29(2):193-214

Quadrant front face pile supported breakwater is a combination of semicircular and closely spaced pile breakwaters which couples the advantages of these two types. This type of structure consists of two parts. The bottom portion consists of closely spaced piles and the top portion consists of a quadrant solid front face on the seaside. The leeward side of the top portion with a vertical face would facilitate the berthing of vessels. An experimental investigation on this breakwater model in a wave flume is carried out for three water depths. For each water depth, three different spacings between the piles were adopted for the investigation. The dynamic pressures exerted along the quadrant front face due to regular waves were measured. The variation of dimensionless pressures with respect to scattering parameter for different gap ratio (spacing between the piles/diameter of pile) and for relative pile depth (water depth/pile height) are presented and discussed. In addition, the dimensionless total forces exerted on the breakwater model as well as its reflection characteristics as a function of scattering parameter are reported.  相似文献   

日像仪的电磁干扰分析     

王威  陈志军  刘玉英  颜毅华  姬国枢 《天文研究与技术》2006,3(2):176-182

讨论了日像仪的干扰容限，列出了干扰源分布，估算出干扰测试仪灵敏度。计算了同步卫星干扰及干扰时间预测，也分析了中低轨道卫星干扰问题。对移动通信基站产生的干扰作了传播分析、计算，对脉冲雷达干扰作了谱分析及保守计算。  相似文献   

BPL脉位调制方案及数据传送     

吴海涛  边玉敬 《时间频率学报》2000,23(2):102-109

实现BPL长波信道能力扩展的一个重要技术环节是对组重复间隔（GRI）脉冲的脉位调制,在将信源消息变成脉位调制电平的数据传输过程中,还有一系列的信号格式转换,提出了实现脉位调制的若干方法,探讨了数据流的详细传送过程并给出了相应的软件。  相似文献