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1.
Carrara大理岩高温高压变形实验研究   总被引：1，自引：0，他引：1  
利用高精度的Paterson高温高压流变仪对Carrara大理岩在高温(873~1173K)高压(~300MPa)以及约10-6~10-3s-1应变速率下进行了三轴压缩变形实验。结果表明,在等应变速率条件下,其强度随着温度的升高而降低;在等温和等压条件下,其强度随着应变速率的增加先快速增加而后缓慢增加。在应变速率对差应力的双对数投图中,我们发现随着温度的升高拟合直线的斜率减小,并且在873K和高应变速率时973K温度下Carrara大理岩的流变本构方程服从指数律变化关系;而在高温(1073K和1173K)和973K低应变速率条件下Carrara大理岩的应力指数n为5.3~7.7,且服从幂次律变化关系。因此,Carrara大理岩在本研究的实验条件下主要有两种变形机制,一种是用指数律表示的高应力变形机制;另一种是用幂次律表示的中等应力变形机制。  相似文献   

2.
The effects of pore water on the mechanical behaviour of Solnhofen Limestone and Carrara Marble at various temperatures and confining pressures at constant strain-rate have been experimentally investigated. It is shown that water affects the strength and ductility of calcite rocks through
1.
(1) physico-chemical action at grain boundaries, and  相似文献   

3.
Folding experiments have been carried out on single-layers of Carrara marble and Solnhofen limestone at a confining pressure of 275 bars, temperature of 400°C, and strain rates of 5.5×10−7 to 8.2×10−7. The marble and limestone layers were embedded in a rock-salt matrix and in a matrix of a mixture of 60% fine-grained halite and 40% fine-grained calcite, respectively, and deformed to different percentages of bulk shortening. Aspect ratios of the layers varied between 11.25 and 15. The stress-strain relationship reveals that strain increased with a very small increment in compressive stresses, once folding was initiated.With progressive deformation the bulk strain is compensated by folding along one fold hinge. The resulting folds are concentric and a combination of class 1a, 1b and 3 type. The changes in the arc length, layer thickness, limb dip and wavelength with progressive folding in marble layers, are discussed.The microstructure and texture of the folded marble and limestone layers have been investigated optically and by means of an X-ray texture goniometer. The inner fold arc exhibits a strong preferred orientation, whereas in the outer fold are the preferred orientation is poorly developed. Differences in the fabric in medium-grained marble and fine-grained limestone layers have been attributed to the difference in mechanism of deformation.  相似文献   

4.
Post-deformational annealing of calcite rocks   总被引：3，自引：3，他引：3  
The evolution of microstructure and crystallographic preferred orientation (CPO) during post-deformational annealing was studied on three calcite rock types differing in purity and grain size: Carrara marble (98% calcite, mean grain size of 115 μm), Solnhofen limestone (96%, 5 μm) and synthetic calcite aggregates (99%, 7 μm). Samples were first deformed in torsion at 727 °C at a shear strain rate of 3 × 10− 4 s− 1 to a shear strain of 5 and subsequently heat-treated at 727 °C for various durations between 0 and 24 h. Microstructures and CPOs were analysed by optical microscopy, image analysis and electron backscatter diffraction (EBSD).All rock types deformed in the dislocation creep field at the same applied conditions, but their microstructures and CPOs after deformation and after annealing differed depending on starting grain size and material composition. In Carrara marble and in the synthetic calcite aggregate, a strong CPO developed during deformation accompanied by dynamic recrystallisation with significant changes in grain size. During annealing, widespread grain growth and subtle changes of CPO occurred, and equilibrated foam microstructures were approached after long annealing times. The CPO is the only feature in annealed samples indicating an earlier deformation phase, although it is not always identical to the CPO formed during deformation. In the more impure Solnhofen limestone, secondary phases on grain boundaries suppressed grain boundary mobility and prevented both the formation of a recrystallisation CPO during deformation and grain size modification during deformation and annealing.  相似文献   

5.
Folds are developed in thin limestone layers within slates of the McKay Formation exposed to the east of the Rocky Mountain Trench, British Columbia, Canada. They possess geometrical characteristics expected of development by buckling. Strain in the profile plane of a selected fold is similar to that predicted by tangential longitudinal strain, except that magnitudes are too low for the observed curvature. This is attributed to inhomogeneity of strain on the scale of measurement, largely because of pressure solution. Material removed by pressure solution from the inner arc of the fold appears to form veins perpendicular to the hinge, a direction of tectonic stretching. Bedding-parallel stylolites developed diagenetically prior to tectonism.Layer-parallel shortening during the initiation of buckling was less than 20%, and probably less than 10%. The mean arclength/thickness ratio is 6.5 and 7.1, with a dispersion of 0.48 and 0.37 for local and regional populations of 29 and 212 folds, respectively. Application of buckling theory to this data suggests that folding followed a non-linear flow law. The viscosity contrast between limestone and slate would be higher and the power law exponent lower, if initial irregularities in the layers were in the form of a constant amplitude spectrum rather than one of white roughness. The data do not allow a choice of initial amplitude spectrum to be made, nor do they closely constrain estimates of n the power law exponent and viscosity contrast.Deformation in the limestone layers was accommodated by intracrystalline flow (twin gliding), pressure solution, and extensional veining (the last two linked by diffusive mass transfer). The first two dominated deformation in the profile plane of the fold and the last, in association with fracturing, allowed for extension parallel to the hinge. Experimental and theoretical considerations suggest that deformation by a combination of these processes should be non-linear. The non-linear flow law deduced from buckling analysis is consistent with expectations based on observations of active deformation mechanisms.  相似文献   

6.
For technical reasons, virtually all plastic deformation experiments on geological materials have been performed in either pure shear or simple shear. These special case loading geometries are rather restrictive for those seeking insight into how microstructure evolves under the more general loading geometries that occur during natural deformation. Moreover, they are insufficient to establish how plastic flow properties might vary with the 3rd invariant of the deviatoric stress tensor (J3) which describes the stress configuration, and so applications that use those flow properties (e.g. glaciological and geodynamical modelling) may be correspondingly compromised. We describe an inexpensive and relatively straightforward modification to the widely used Paterson rock deformation apparatus that allows torsion experiments to be performed under simultaneously applied axial loads. We illustrate the performance of this modification with the results of combined stress experiments performed on Carrara marble and Solnhofen limestone at 500°–600 °C and confining pressures of 300 MPa. The flow stresses are best described by the Drucker yield function which includes J3-dependence. However, that J3-dependence is small. Hence for these initially approximately isotropic calcite rocks, flow stresses are adequately described by the J3-independent von Mises yield criterion that is widely used in deformation modelling. Loading geometry does, however, have a profound influence on the type and rate of development of crystallographic preferred orientation, and hence of mechanical anisotropy. The apparatus modification extends the range of loading geometries that can be used to investigate microstructural evolution, as well as providing greater scope for determining the shape of the yield surface in plastically anisotropic materials.  相似文献   

7.
Artificially prepared specimens of bischofite (MgCl2-6H2O) have been experimentally deformed at temperatures between 20 and 100°C, strain rates between 10−4 and 10−88 s−1, and confining pressures between 0.1 and 28 MPa. Development of microstructure with strain was studied by in-situ deformation experiments, and results of these were correlated with observations made on thin sections of deformed samples.In a first series of experiments the effect of grain size, impurity content and water content on the flow behaviour was investigated. Addition of about 0.1 wt.% water to dry samples was found to decrease the flow stress by a factor of 5. This effect was found to be associated with the formation of a thin fluid film on grain boundaries, strongly enhancing dynamic recrystallization due to the movement of high-angle grain boundaries, and possibly also to enhanced intracrystalline plasticity due to excess water present in the lattice. In a second series of experiments the strain-rate sensitivity of the flow stress of selected samples was investigated. Two regimes could be distinguished: one with a stress exponent n = 4.5 in the power law creep equation for values of the differential stress above 2.0 MPa, and one with n = 1.5 for stresses below this value.The main deformation mechanisms were intracrystalline slip, twinning, and grain-boundary sliding. Recrystallization occurred by subgrain rotation and high-angle grain-boundary migration. The rates of grain-boundary migration fell into two different regimes, one regime being distinguished by extremely fast migration rates. The applicability of the experimentally found flow law to the behaviour of bischofite rocks in nature is discussed.  相似文献   

8.
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9.

An overview is presented of the actinopterygian fishes from the Late Jurassic (Late Kimmeridgian and Early Tithonian) ‘Plattenkalke’ near Solnhofen (Solnhofen lithographic limestone), Bavaria, Germany. The fish fauna is very diverse, with the palaeonisciform Coccolepis, halecostomes such as Lepidotes, Heterostrophus, three genera of macrosemiids and six genera of pycnodontiforms, halecomorphs including two genera of caturids, two genera of amiids, Ophiopsis, ‘Furo’, Ionoscopus, Brachyichthys, Callopterus, Liodesmus, ?Lophiurus, five genera of pachycormids, three genera of pholidophorids, Pleuropholis, two genera of aspidorhynchids and eleven genera of basal teleosts. Although several groups have been subject of revision, most of the fauna remains poorly known. Study of this rich fauna will provide a lot of information on the phylogeny and interrelationships of halecostome fishes.

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10.
Evolution of grain size in synthetic marbles was traced from compaction of unconsolidated powder, through primary recrystallization and normal grain growth, to a size stabilized by second phases. To form the marbles, reagent grade CaCO3 was mixed with 0, 1 and 5 volume% mica and heat-treated under pressure with added water. Densification with negligible recrystallization occurred within one hour at 500° C and 500 MPa confining pressure. Primary recrystallization occurred at 500–550° C, causing increases of grain size of factors of 2–5. Resulting samples had uniform grain size, gently curved grain boundaries, and near-equilibrium triple junctions; they were used subsequently for normal grain growth studies. Normal grain growth occurred above 550° C; at 800° C, grain size (D) increased from 7 m (D 0) to 65 m in 24 hours. Growth rates fit the equation, D n -D 0 n =Kt, where K is a constant and n2.6. Minor amounts of pores or mica particles inhibit normal grain growth and lead to a stabilized grain size, D max, which depends on the size of the second phases and the inverse of their volume fraction raised to a power between 0.3 and 1. Once D max is reached, normal growth continues only if second phases are mobile or coarsen, or if new driving forces are introduced that cause unpinning of boundaries. Normal grain growth in Solnhofen limestone was significantly slower than in pure synthetic marble, suggesting that migration is also inhibited by second phases in the limestone.  相似文献   

11.
Superplastic flow in finegrained limestone   总被引：1，自引：0，他引：1  
Creep of Solnhofen limestone at temperatures between 600° and 900° C was found to fall into three different flow regimes: regime 1 with an exponential stress-dependence of strain rate, regime 2 with power-law creep and n ~ 4.7 and finally a superplastic regime 3 with n ~ 1.7. Within the superplastic regime the creep behaviour is strongly grain-size dependent, the strain rate increasing markedly with decrease in grain size at a given stress. Microstructural observations indicate that in regimes 1 and 2 intracrystalline plasticity is dominant whereas the superplastic regime is characterized by grain-boundary sliding. The crystallographic preferred orientation within the superplastic regime is weaker and of different geometry when compared with that in flow regimes 1 and 2. In a discussion on the deformation mechanisms it is suggested that flow regimes 1 and 2 are regimes of dis location creep in which the rate controlling step is diffusion assisted; for the superplastic regime existing models of grain-boundary sliding are compared with the observations Finally, the tectonophysical importance of superplasticity is discussed and by extra polating the observed creep behaviour to geological strain rates it is found that super plasticity in rocks is to be expected under a wide range of conditions, particularly at smal grain sizes.  相似文献   

12.
Turbidite bed thickness distributions are often interpreted in terms of power laws, even when there are significant departures from a single straight line on a log–log exceedence probability plot. Alternatively, these distributions have been described by a lognormal mixture model. Statistical methods used to analyse and distinguish the two models (power law and lognormal mixture) are presented here. In addition, the shortcomings of some frequently applied techniques are discussed, using a new data set from the Tarcău Sandstone of the East Carpathians, Romania, and published data from the Marnoso‐Arenacea Formation of Italy. Log–log exceedence plots and least squares fitting by themselves are inappropriate tools for the analysis of bed thickness distributions; they must be accompanied by the assessment of other types of diagrams (cumulative probability, histogram of log‐transformed values, q–q plots) and the use of a measure of goodness‐of‐fit other than R2, such as the chi‐square or the Kolmogorov–Smirnov statistics. When interpreting data that do not follow a single straight line on a log–log exceedence plot, it is important to take into account that ‘segmented’ power laws are not simple mixtures of power law populations with arbitrary parameters. Although a simple model of flow confinement does result in segmented plots at the centre of a basin, the segmented shape of the exceedence curve breaks down as the sampling location moves away from the basin centre. The lognormal mixture model is a sedimentologically intuitive alternative to the power law distribution. The expectation–maximization algorithm can be used to estimate the parameters and thus to model lognormal bed thickness mixtures. Taking into account these observations, the bed thickness data from the Tarcău Sandstone are best described by a lognormal mixture model with two components. Compared with the Marnoso‐Arenacea Formation, in which bed thicknesses of thin beds have a larger variability than thicknesses of the thicker beds, the thinner‐bedded population of the Tarcău Sandstone has a lower variability than the thicker‐bedded population. Such differences might reflect contrasting depositional settings, such as the difference between channel levées and basin plains.  相似文献   

13.
The relative nucleus density (RND) model of dynamically recrystallized grain size [Sakai, T., Jonas, J.J. 1984. Dynamic recrystallization: mechanical and microctructutal consideration. Acta metallurgica, 32, 198–209] was applied to experimentally and to naturally deformed marbles that have undergone dynamic recrystallization. The model shows that a relationship between initial grain size (D0) and stable dynamically recrystallized grain size (DS) for a given value of temperature-corrected strain-rate (Z) controls grain size evolution during dynamic recrystallization. New microstructural mechanism maps (MM-maps) for experimentally and naturally deformed marbles (based on previously published data) were defined in log grain size–log Z space and show two distinct regions of grain reduction and grain coarsening. The boundary between these two regions corresponds to an equation relating dynamically recrystallized grain size and temperature corrected strain rate, as proposed in this work. The new MM-map was used to trace semi-quantitatively microstructural and grain size evolution in naturally deformed marbles that underwent dynamic recrystallization at different thermal conditions. The boundary between grain coarsening and grain reduction does not necessarily coincide with the boundary between rotation and migration recrystallization mechanisms. Assessment of available natural data shows that the boundary condition D0 = 2DS between grain-coarsening and grain-reduction introduced by Sakai and Jonas [Sakai, T., Jonas, J.J. 1984. Dynamic recrystallization: mechanical and microctructutal consideration. Acta metallurgica, 32, 198–209] is not required for naturally deformed marble.  相似文献   

14.
The viscoelastic relaxation behaviour of lherzolite and marble and their temporal fractal properties are studied. Based on the high‐temperature viscoelastic behaviour for these rock types derived from the time–temperature superposition principle, the relaxation function for the viscoelastic behaviour of lherzolite and marble can be expressed as a flow law from a power‐law function of temperature‐reduced time given by normalizing the various temperature behaviours, with a non‐integer exponent. The relaxation function is thus time‐scale invariant, i.e. there is a temporal fractal property to the temperature‐reduced time. Their rheological behaviour over geological time‐scales at low temperature can be extrapolated from the experimental high‐temperature behaviour based on the temporal fractal property. Our derived flow law satisfies not only transient behaviour but also steady‐state behaviour.  相似文献   

15.
An independent approach, based on a power law relation interconnecting the lead time of precursory signals and the stress drop of forthcoming earthquake, confirms the reported evidence that the observed magnetic field anomaly and consequently, according to Maxwell’s laws, electric field anomaly prior to Mw 6.3 Aquila earthquake in 2009 exhibit features of criticality. Precisely, by inserting the data from Aquila earthquake in this power law, we get an exponent α = 0.329, which is in excellent agreement with previously found ones and falls within the range values (0.3–0.4) for critical exponents for fracture. This fact implies that upon the initiation of the observed magnetic field anomaly and the associated electric signal prior to Aquila earthquake, the prefocal area enters into a critical stage where nonlinear dynamic processes, typical behaviour of a system close to criticality, prevail.  相似文献   

16.
In the Tithonian Solnhofen Plattenkalk (Malm + 2) of southern Germany, layers of purely micritic limestone are rhythmically interbedded with ones of marly micritic limestone. It appears that this alternation was formed under control of the Tithonian orbital variations. The Fourier spectral analysis shows that, on a decimetric to metric scale, the long-term cyclicities in the number of laminae per centimetre are in agreement with those found in the bed-thickness series, varying from 0.7 to 1.3 m cycles. The number of laminae of the Solnhofen Formation ranges from about 5,800 to about 12,800 laminae per main cycle. This indicates that, under an assumption that the main cycle of the Solnhofen Formation corresponds to the Tithonian precessional one, a single lamina represents a multi-year time interval. Particularly, in the short-term cyclic domain, the laminated sequence contains clearly millimetric cycles consisting of about two to three cyclic components. It implies that laminae formation may result from the composite effect of two or three distinct climatic processes.  相似文献   

17.
Prediction of engineering properties of rocks from microscopic data   总被引：1，自引：0，他引：1  
The purpose of this study is to develop the empirical equations for the prediction of the physical and mechanical properties of limestone and marble from microscopic data including their mineralogical and petrographical properties and to test the validity of model equations by using multivariate statistical methods. This study was performed on 15 different rocks, composed of six limestone and nine marble samples. Stepwise multiple regression analysis was applied to predict the engineering properties of both the marble and limestone rock samples considering petrographical properties as inputs. In order to determine the overall significance of the empirical equations for prediction of the physical and mechanical properties of marble and limestone samples, the F test was also performed. As a result of this study, it is found that the empirical equations developed in this study are statistically significant.  相似文献   

18.
Physical Modelling of Stress-dependent Permeability in Fractured Rocks   总被引：2，自引：1，他引：1  
This paper presents the results of laboratory experiments conducted to study the impact of stress on fracture deformation and permeability of fractured rocks. The physical models (laboratory specimens) consisted of steel cubes simulating a rock mass containing three sets of orthogonal fractures. The laboratory specimens were subjected to two or three cycles of hydrostatic loading/unloading followed by the measurement of displacement and permeability. The results show a considerable difference in both deformation and permeability trends between the first loading and the subsequent loading/unloading cycles. However, the micrographs of the contact surfaces taken before and after the tests show that the standard deviation of asperity heights of measured surfaces are affected very little by the loadings. This implies that both deformation and permeability are rather controlled by the highest surface asperities which cannot be picked up by the conventional roughness characterization technique. We found that the dependence of flow rate on mechanical aperture follows a power law with the exponent n smaller or larger than three depending upon the loading stage. Initially, when the maximum height of the asperities is high, the exponent is slightly smaller than 3. The first loading, however, flattens these asperities. After that, the third loading and unloading yielded the exponent of around 4. Due to the roughness of contact surfaces, the flow route is no longer straight but tortuous resulting in flow length increase.  相似文献   

19.
The deformation history of a monophase calcite marble shear zone complex on Thassos Island, Northern Greece, is reconstructed by detailed geometric studies of the textural and microstructural patterns relative to a fixed reference system (shear zone boundary, SZB). Strain localization within the massive marble complex is linked to decreasing P–T conditions during the exhumation process of the metamorphic core complex. Solvus thermometry indicates that temperatures of 300–350°C prevailed during part of the shear zone deformation history. The coarse-grained marble protolith outside the shear zone is characterized by symmetrically oriented twin sets due to early coaxial deformation. A component of heterogeneous non-coaxial deformation is first recorded within the adjacent protomylonite. Enhanced strain weakening by dynamic recrystallization promoted strong localization of plastic deformation in the ultramylonite of the calcite shear zone, where high strain was accommodated by non-coaxial flow. This study demonstrates that both a pure shear and a simple shear strain path can result in similar crystallographic preferred orientations (single c-axis maximum perpendicular to the SZB) by different dominant deformation mechanisms. Separated a-axis pole figures (+a- and −a-axis) show different density distributions with orthorhombic texture symmetry in the protolith marble and monoclinic symmetry in the ultramylonite marble consistently with the observed grain fabric symmetry.  相似文献   

20.
High temperature creep of single crystal gadolinium gallium garnet (GGG) was studied in the temperature range of 1723–1853 K (0.86–0.94 Tm, Tm: melting temperature) and strain rate from 9 · 10?7 s?1 to 2 · 10?5 s?1. The compression tests were made along the 〈100〉 and 〈111〉 orientations. We have performed both constant strain-rate and stress-dip tests. For the 〈100〉 orientation, deformation occurs via the 〈111〉 slip systems. For the 〈111〉 orientation, both the 〈100〉 {010} and the 〈111〉 slip systems can be activated. GGG garnet is very strong under these conditions: σ/μ=(1–3)×10?3 (σ: creep strength, μ: shear modulus). The creep behavior is characterized by a power law with stress exponent n=2.9–3.3 and high activation energies E*=612–743 kJ/mol (E*～45×RTm, at zero stress which decrease with the increase of stress). Stress-dip tests suggest a small internal stress (σi/σ～0.62; σi: internal stress, σ: applied stress) compared to other materials. These results suggest that the high creep strength of GGG is mainly due to difficulty of dislocation glide rather than dislocation climb.  相似文献   

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