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QiaoQin Xie TianHu Chen XiaoChun Xu ChengSong Qing HuiFang Xu YuBing Sun JunFeng Ji 《中国科学D辑(英文版)》2009,52(3):313-322
The dominant magnetic minerals and carriers of magnetic signals within the Chinese Loess Plateau are magnetite, maghemite,
hematite, and goethite. In this study, we investigated the provenance and evolution of magnetic minerals during loess pedogenesis,
using X-ray diffraction (XRD) and optical and electron microscopy, including field emission scanning electron microscopy (FESEM)
and high-resolution transmission electron microscopy (HRTEM). Our results reveal that single- and multiphase mineral assemblages
among magnetic minerals in the loess-paleosol sequence have been formed. Partial oxidation of coarse eolian magnetite has
occurred in the desert source area and the oxidation degree is enhanced after deposition of the dust upon the Chinese Loess
Plateau. This mode of origin resulted in a microtexture consisting of an inner magnetite core surrounded by a hematite rim,
and strongly affected the magnetic characteristics of the loess. Goethite coexists with hematite in the loess and paleosol,
and nanometer-scale hematite is formed upon goethite rims via dehydration. Our study provides direct mineralogical evidence
of the magnetic record and paleoclimatic implications of the loess-paleosol sequence of the Chinese Loess Plateau.
Supported by National Natural Science Foundation of China (Grant Nos. 40772032 and 40573054) and National Basic Research Program
(Grant No. 2007CB815603) 相似文献
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自从大荔人化石被发现以来,其遗址剖面便成为研究热点.先前的研究主要集中在地层的对比划分与头盖骨年龄的推断方面,然而对于载磁矿物的鉴定及其古气候含义方面的研究却相对较少.鉴于此,本文运用热磁分析、饱和等温剩磁和剩磁矫顽力谱分析、磁滞回线分析、频率磁化率分析、热退磁分析等方法,对大荔人遗址剖面进行了系统的岩石磁学性质研究,鉴定出其主要载磁矿物为磁铁矿,赤铁矿,磁赤铁矿,磁畴状态主要是似单畴.磁铁矿,赤铁矿是样品中特征剩磁的携带者;主要起源于成土作用的超顺磁颗粒和新生成的亚铁磁性矿物,是古土壤样品磁化率增强的主要贡献者;古土壤中软磁性矿物的含量高于黄土.样品中磁赤铁矿的含量并不高.黄土-古土壤样品的频率磁化率曲线,古里雅冰芯氧同位素、细微粒浓度曲线,岐山五里铺剖面有机质含量曲线在古气候记录方面具有一致性,都展示出至少从MIS5以来,气候从冰期到间冰期的变化是渐变的,反之则表现了突变特征.上述岩石磁学研究丰富了大荔剖面的磁学领域研究内容,为相关课题的深入研究提供了依据. 相似文献
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本文对发育在澳大利亚悉尼附近的Long Reef Beach中新世古土壤剖面进行了系统的岩石磁学研究,测量了磁化率、饱和磁化强度、饱和等温剩磁、非磁滞剩磁等常温磁学参数和磁滞回线,并对所有样品进行了热磁分析.实验结果表明:全新世软土层主要磁性矿物为MD颗粒磁铁矿,磁性矿物含量与黄土高原黄土层相当.中新世老成土层随地层深度增加主要磁性矿物由磁铁矿转变为磁赤铁矿,随着磁铁矿向磁赤铁矿的转化,开始出现赤铁矿;磁性矿物粒径分布较广,以PSD颗粒为主,其次为SD颗粒,同时含有少量MD颗粒;磁性矿物含量高于黄土高原强发育古土壤层.中新世红土矿层主要磁性矿物为赤铁矿,同时含有少量磁赤铁矿和针铁矿,属于铁的富集层,赤铁矿以SD颗粒为主,含少量PSD和MD颗粒.Long Reef Beach中新世古土壤形成时期,对应着一种全球性高温多雨气候,地表化学风化作用十分强烈.丰富的降水,导致中新世老成土层发生淋溶作用,磁铁矿在向下淋溶迁移过程中逐渐氧化为磁赤铁矿和赤铁矿,铁氧化物最终在红土矿层淀积,磁赤铁矿经高温压实作用再结晶转化为赤铁矿.磁性矿物转化过程可概括为磁铁矿—磁赤铁矿化的磁铁矿—磁赤铁矿—赤铁矿,其中部分磁赤铁矿具有热稳定性,在空气(氩气)环境中加热到700℃未发生转化. 相似文献
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本研究选择川西高原、天山和西伯利亚Kurtak剖面的黄土古土壤样品及亚热带非风成样品进行CBD处理,系统测量并对比处理前后的磁学参数,包括低频磁化率、频率磁化率、非磁滞剩磁、饱和等温剩磁、剩磁矫顽力和热磁曲线(J-T曲线),分析处理前后磁性矿物种类、含量和磁畴的变化.结果表明,CBD方法对于磁性矿物的溶解并无明显的选择性,在温度与反应时间一定的条件下,磁性矿物的溶出量主要受控于其粒径分布.CBD方法可以非常有效地去除具有更大比表面积的细粒(< 1 μm)磁性矿物,同时溶解粗粒(>1 μm)磁性矿物外缘,使其粒径变细.CBD处理后磁化率变化存在多种可能,对于成土作用较强的古土壤,CBD方法可以较为准确地提取成土成因的磁性信息;而干旱和过度湿润条件下的风积黄土,不宜使用CBD方法区分原生与次生磁性矿物. 相似文献
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Rock-magnetic proxies of climate change from loess -paleosol sediments of the Czech Republic 总被引：6，自引：0，他引：6
Summary Rock-magnetic characteristics of late Pleistocene loess-paleosol sequences in the Czech Republic show patterns of variation
that reflect climate-related depositional and diagenetic processes which acted on the sedimentary profiles. Mass-normalized
magnetic susceptibility is high in interglacial and interstadial paleosols, while uniformly low values are measured in unweathered
loess horizons. Normalized ferrimagnetic susceptibility and anhysteretic remanent magnetization show an enhancement of ultrafine
(superparamagnetic, SP) and fine (single-domain, SD, and pseudo-single-domain, PSD) grains in chernozem paleosols correlated
with δ18O substages 5c and 5a as well as in the Holocene soil. The parabraunerde paleosol associated with peak interglacial conditions,
correlated with δ18O substage 5e, shows evidence of diagenetic loss of fine grained magnetic minerals, although coarse (multidomain, MD) grains
appear to be preserved.
Low temperature remanence behavior plus high temperature susceptibility measurements of representative samples from each lithologic
unit indicate that magnetite and maghemite are the dominant magnetic minerals within the sediments. Variations in concentration-independent
rock-magnetic parameters are therefore primarily a function of grain size variations through the profile. It is anticipated
that with additional magnetic and non-magnetic sedimentological and geochemical tests, a quantitative rock-magnetic — paleoclimate
model can be developed for the central European loess region. 相似文献
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风成黄土是陆地上分布最广泛的沉积物之一,记载了各种古气候演化信息.目前巴基斯坦的黄土研究甚少,磁化率与气候对应的变化机制研究尚未开展.本文对位于巴基斯坦印度河平原Bahawalpur地区新发现的黄土-古土壤剖面进行系统的岩石磁学研究,结合粒度和漫反射光谱(DRS)数据,讨论巴基斯坦黄土的磁化率变化机制.实验结果显示:Bahawalpur(BH)剖面黄土层主要的载磁矿物为磁铁矿,同时含有少量磁赤铁矿和针铁矿,磁性颗粒以原生的MD和PSD颗粒为主.相对于黄土层,古土壤层则是以针铁矿为主,含有顺磁性矿物和少量磁铁矿.BH剖面磁化率与成土作用关系和中国黄土高原典型剖面相反,磁化率的变化可能存在一个阈值12.8×10-8 m3·kg-1,在阈值之上,强磁性矿物(磁铁矿、磁赤铁矿)占主导;阈值之下,以弱磁性矿物(主要是针铁矿)为主,这种磁性矿物的转变可能导致磁化率降低.本文可为今后利用磁化率解读该地区地层蕴含的古气候信息提供新线索. 相似文献
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The sand-hill section in Hongguang, Pengze County, Jiangxi Province is composed of eolian sand beds interbedded with 12 weakly-pedogenetic
paleosols, and this sedimentary sequence was formed from about 25 to 13 kaBP. A detailed rock-magnetic study demonstrates
that the magnetic minerals in the sequence are dominated by multi-domain magnetite grains in addition to small amounts of
maghemite and hematite. Compared with the eolian sand beds, the paleosols are characterized by smaller magnetic particles,
higher proportion of low-coercivity minerals and markedly increase in the magnetic mineral content. In the section, various
magnetic parameters (K, ARM, SIRM and S ratios) display a roughly gradual increase from eolian sand beds to the overlying
paleosols but an abrupt decrease from paleosols to the overlying eolian sand beds. The content of low-coercivity magnetic
minerals shows the lowest values in the second eolian sand bed from the bottom of the section, and from the bed upwards it
gradually increases on the whole in the eolian sand beds. These magnetic properties reflect regional climatic changes during
the last glacial maximum. 相似文献
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QIANG Xiaoke AN Zhisheng LI Huamei CHANG Hong & SONG Yougui . SKLLQG Institute of Earth Environment Chinese Academy of Sciences Xi’an China . Guangzhou Institute of Geochemistry Chinese Academy of Sciences Guangzhou China 《中国科学D辑(英文版)》2005,48(8):1234-1245
Rock magnetism research on eolian deposits from the Chinese Loess Plateau shows that magnetite, maghe- mite and hematite are the main magnetic minerals in loess-paleosol sequences and red clay se-quences[1―8], and finds that the magnetic susceptibility increase is positively correlated to the content of ultra-fine minerals and relatively strong pedogene- sis[7―15]. This offers significant information in studying the Late Cenozoic paleoclimatic history of Chinese Loess Plateau[1,5―8,10―22… 相似文献
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Detailed rock magnetic investigations and X-ray diffraction (XRD)were carried out on loess-paleosol sequences of the last interglacial-glacial at Znojmo section in Czech Republic. The results indicate that pedogenesis causes susceptibility enhancement in the paleosols, which is similar to that observed in the Chinese Loess Plateau. k-T curves, IRM, and XRD show that magnetite is the dominant magnetic mineral in the loess-paleosol sequences at the Znojmo section, while maghemite, hematite, and pyrite/pyrrhotite are minor minerals. Measurements of anisotropy of magnetic susceptibility (AMS) indicate that the magnetic lineation is smaller than the foliation. The susceptibility ellipsoids are oblate and the directions of the maximum principal axes (Kmax) are distributed randomly, and cannot be used to determine the paleo-wind direction. 相似文献
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The characteristics,origins, and geodynamic settings of supergiant gold metallogenic provinces 总被引：26，自引：6，他引：20
An investigation of the rock magnetic properties using stepwise isothermal remanence (IRM) acquisition, thermomagnetic analysis
and temperature-dependent susceptibility history, identifies magnetite as the carrier of the main fraction of the remanence,
associated with maghemite and hematite in Malan loess (L1), Holocene soil (S0) and last-glacial paleosol (S1). The presence
of short-lived direction fluctuations indicates that no significant smoothing occurs in L1 when its remanence is locked, and
thus L1 is capable of recording the geomagnetic secular variation (PSV), while the PSV has been severely smoothed or wiped
out by pedogenic processes during S1 formation. It has been suggested that the Mono Lake and Laschamp excursions are two independent
geomagnetic events based on this study. 相似文献
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《Earth and Planetary Science Letters》2006,241(1-2):248-259
A high-resolution mineral magnetic investigation has been carried out on the Jingbian loess/paleosol sequence at the northern extremity of the Chinese Loess Plateau. Results show that the magnetic assemblage is dominated by large pseudo-single domain and multidomain-like magnetite with associated maghemite and hematite. Variations in the ratios of SIRM100mT/SIRM, SIRM100mT/SIRM30mT and SIRM100mT/SIRM60mT (SIRM is the saturation isothermal remanent magnetization; SIRMnmT represents the residual SIRM after an n mT alternating field demagnetization) have been used to document regional paleoclimate change in the Asian interior by correlating the mineral magnetic record with the composite δ18O record in deep-sea sediments. The long-term up-section decreasing trend in those ratios in both loess and paleosol units has been attributed to a long-term decrease in the relative contributions of eolian hematite during glacial extrema and of pedogenic hematite during interglacial extrema, respectively, which reveals a long-term decreasing trend in chemical weathering intensity in both glacial-stage source region (the Gobi and deserts in northwestern China) and interglacial-stage depositional area (the Loess Plateau region). We further relate this long-timescale variation to long-term increasing aridification and cooling, during both glacial extrema in the dust source region and interglacial extrema in the depositional area, over the Quaternary period. Changes in those ratios are most likely due to Quaternary aridification and cooling driven by ongoing global cooling, expansion of the Arctic ice-sheet, and progressive uplift of the Himalayan–Tibetan complex during this period. 相似文献
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S. Spassov F. Heller R. Kretzschmar M. E. Evans L. P. Yue D. K. Nourgaliev 《Physics of the Earth and Planetary Interiors》2003,140(4):255-275
A detailed rock magnetic investigation of loess/palaeosol samples from the section at Lingtai on the central Chinese Loess Plateau (CLP) is presented. Thermal demagnetisation of isothermal remanent magnetisation (IRM) and Curie temperature measurements suggest the presence of magnetite, maghemite and hematite as remanence carrying components. Bulk and grain size fractionated samples have been analysed using coercivity spectra of remanence acquisition/demagnetisation curves, which identify four main remanence carriers in different grain size fractions of loesses and palaeosols. A linear source mixing model quantifies the contribution of the four components which have been experimentally derived as dominating endmembers in specific grain size fractions. Up to two thirds of the total IRM of the palaeosols are due to slightly oxidised pedogenic magnetite. Two detrital components dominate up to 90% of the IRM of the loess samples and are ascribed to maghemite of different oxidation degree. Detrital hematite is present in all samples and contributes up to 10% of the IRM. The iron content of the grain size fractions gives evidence that iron in pedogenically grown remanence carriers does not originate from the detrital iron oxides, but rather from iron-bearing clays and mafic silicates. The contribution of pedogenic magnetite to the bulk IRM increases with the increasing degree of pedogenesis, which depends in turn on climate change. 相似文献
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P. S. Minyuk T. V. Subbotnikova A. A. Plyashkevich 《Izvestiya Physics of the Solid Earth》2011,47(9):762-774
Magnetic susceptibility (MS) of natural specimens of hematite and goethite is studied under continuous heating with various
additives: with carbon (sugar), nitrogen (carbamide), and elemental sulfur. It is found that heating of hematite with carbon
above 450°C results in the formation of single-domain magnetite, while the magnetic susceptibility rises by a factor of 165.
The increase in magnetic susceptibility on heating of hematite with nitrogen above 540°C reflects the generation of a single-domain
maghemite with the Curie point of about 650°C, which is stable to heating. After the first heating, the magnetic susceptibility
increases by 415 times. The subsequent cycle of thermal treatment results in the transition of maghemite to hematite, a decrease
of MS, and an increase of coercivity. Heating with sulfur produces a stable single-domain magnetite at a temperature above
the Curie point, which is manifested in the cooling curves. Here, the MS increases by a factor of 400. The heating curves
for goethite exhibit a sharp drop in susceptibility to a temperature of 350–360°C, which reflects the transition of hematite
to goethite. Heating of hematite with carbon produces stable maghemite at above 530°C, and with sulphur and nitrogen, it produces
magnetite. When heated with pyrite, hematite reduces to magnetite under the action of sulfur released from pyrite. 相似文献
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陕西交道全新世黄土-黑垆土磁化率的CBD研究 总被引：16，自引：7，他引：9
根据黄士高原中部交道剖面全新世黄土－黑垆土剖面的非磁滞磁化率和ＣＢＤ提取前后的磁化率、频率磁化率以及热磁分析结果,分析了磁性矿物的种类和磁畴状态,讨论了古土壤的磁化率增强,指出ＣＢＤ技术强有力的支持古土壤磁化率增强的土壤成因观点．虽然ＣＢＤ能非常有效地溶解土壤成因的磁赤铁矿,但并不是完全选择性地溶解土壤成因的磁铁矿颗粒．此外,通过对样品ＣＢＤ处理前后磁化率数据的分析,从土壤化学角度为黄土的风成说提供了新证据。 相似文献
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《中国科学:地球科学(英文版)》2017,(3)
Aeolian loess deposits contain abundant information about the evolution of the paleoenvironment.For example,paleoclimate changes recorded in Chinese loess area obtained significant achievement in the past few decades.Compared to Chinese loess,research on Indian loess is lacking.Currently,most studies focus on the Kashmir area located in the southern Himalayas,and studies on other areas are rare.However,field observations demonstrate that the sediments around the New Delhi-Agra-Jaipur Plain are similar to Chinese loess-paleosol sequences.For example,the boundary between two strata is transitional and without horizontal bedding.Moreover,obvious pedogenic horizons developed among sediment sequences,probably indicating unrecognised aeolian deposits in the Indo-Gangetic Plain(IGP).To confirm this,pilot samples were obtained from the IGP and detailed indoor measurements conducted.The results indicate that the distribution patterns of particle size and rare earth elements(REE) of the pilot samples are similar to Chinese loess.Furthermore,the scanning electronic microscopy(SEM) images of pilot samples show obvious conchoidal fractures,dash-shaped concavities,and abundant small pits that usually form through mechanical impact.These are typical characteristics of aeolian particles.In addition,environmental and rock magnetic measurements indicate that the dominant magnetic minerals in the pilot samples are magnetite and maghemite,and that they likely contain small amounts of hematite.Furthermore,conventional magnetic parameters are comparable with Chinese loess.Based on this,aeolian loess deposits are widely distributed in the IGP,which may have promoted the development of Indian farming and contributed towards the prosperity of ancient Indian civilisation.This study also provides a new and valuable record for the research on paleoclimate changes in the study area in the future. 相似文献
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热磁测量,包括高温磁化率和高温磁化强度测量,是根据热磁曲线转折点的温度(居里点、尼尔点或相变点)鉴定样品中磁性矿物种类的有效方法.本文选取两个人工合成磁赤铁矿样品,利用四种热磁测量仪器分析不同的条件下测得的热磁曲线.依据样品与空气接触程度,将测量环境设为开放、封闭、封闭(通入氩气或氮气)三类.结果表明:热磁测量环境的开放程度对居里点和曲线可逆程度产生极大的影响.封闭环境下测得的居里点较开放环境下的低,分别对应磁铁矿和磁赤铁矿;开放系统的热磁曲线不可逆程度高于封闭系统.造成这些差异的原因是氧化还原条件的不同.本文的磁赤铁矿样品在封闭的条件下,加热至250 ℃左右开始转化为磁铁矿,因此无法通过居里点被正确识别;在开放的氧化环境下,加热的最终产物为赤铁矿,能够测得正确的居里点.本实验结果启发人们:在不同的加热环境下,磁性矿物可能表现出不同的热磁行为,根据单一的热磁曲线,很容易对样品中磁性矿物的种类造成误判.全面对比不同条件下的测量结果,才能够得出更为准确的结果. 相似文献
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对山西襄汾丁村文化遗址群内大柴剖面进行的磁性地层学研究表明,松山与布容的极性界线（M/B）出现在距剖面顶部45 m处;磁化率对比结果显示,此位置正好与S8上部对应.由这种极性和磁化率的对应结果可推断,下、中更新统（Q1/Q2）的地层分界也应在距剖面顶部45 m处的S8上部,而不是传统上认为的Q1/Q2的地层分界,在距剖面顶部80 m处.这种以古地磁学为基础的新的划分方案,对丁村遗址群的对比以及丁村遗址年代的最终确定都有重要的指示意义.根据其沉积环境和地层特征推断,采样部位下部的磁化率低值带应为水成黄土.而岩石磁学研究结果显示,磁铁矿、赤铁矿和热不稳定性磁赤铁矿是大柴剖面沉积物中主要的磁性矿物;磁铁矿和赤铁矿同为高温稳定性磁性载体. 相似文献