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硼酸三甲酯是合成储氢材料硼氢化钠的重要原料,以硼酸、甲醇为原料合成硼酸三甲酯是目前硼酸三甲酯合成的重要方法之一。提供了一种测定硼酸、甲醇合成硼酸三甲酯蒸馏混合物中硼酸三甲酯成分、含量的测定方法,即气相色谱一质谱法(GC-MS)。该方法简单、快捷、准确。确定了优化的GC-MS测定条件,适合不同合成条件下蒸馏后混合物中硼酸三甲酯的定性、定量。测定结果表明,该方法对同一条件下合成混合物中硼酸三甲酯做测定分析,加标回收率在91.8%100.5%,相对标准偏差1.9%100.5%,相对标准偏差1.9%4.1%,检出限3.64 mg/mL。通过对16组不同工艺合成条件下混合物中硼酸三甲酯的测定分析,该方法重复性较好,较为稳定,对硼酸三甲酯检测分析具有重要意义。 相似文献
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采用人工配制系列标准样,硼酸镶边垫底粉末压片方法制样,建立X射线荧光光谱法测定SrCO3产品中锶钙钡镁含量的定量分析曲线。由于SrCO3产品中锶含量极高,按照仪器给定的测量条件进行测量会产生谱峰饱和现象,造成计数率溢出,分析结果误差较大;文章对锶的分析条件进行了研究,提出降低锶的测定功率来降低计数率,以达到测量目的。同时还对自成特性很差的SrCO3产品的压片条件进行了讨论。使用α经验系数法校正基体效应,通过对实际样进行检验,测量值与化学分析值结果吻合。方法的检出限和准确度均满足分析要求。方法的RSD分别为Sr0.029%,Ba0.17%,Ca0.89%,Mg0.20%。 相似文献
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氯氧镁胶凝材料的总Cl-含量是衡量产品吸潮、返卤和泛霜性能的关键指标之一。讨论了样品粉碎方式及硝酸酸溶浸取条件对样品中总Cl-测定的影响,并用优化后的预处理方法和台湾标准CNS14164方法对样品中总Cl-含量进行了分析。结果表明,手工研磨样品比机械粉碎样品中的总Cl-测定值偏高0.37%,相对偏差为3.91%;硝酸浓度对总Cl-的浸取有一定影响。经优化后的预处理方法为,取1 g用机械粉碎至88μm的粉末样品,用40 mL体积比为15/85的稀硝酸浸取20 min,再过滤洗涤得到待分析液。优化预处理方法后,测定Cl-的相对误差在0.44%以内,且有利于后续的滴定分析操作,精密度和准确度均优于CNS14164方法。 相似文献
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《The Professional geographer》1984,36(1):106-142
Book Reviewed in this article: Development and Environment in Peninsular Malaysia . S. Robert Aiken, Colin H. Leigh, Thomas R. Leinbach, Michael R. Moss. The Rural-Urban Fringe: Canadian Perspectives . Ken B. Beesley and Lorne H. Russwurm, eds. Women and Development . Lourdes Benería, ed. The Border that Joins: Mexican Migrants and U.S. Responsibility . Peter G. Brown and Henry Shue, eds. Cities of the World: World Regional Urban Development . Stanley D. Brunn and Jack L. Williams, eds. Time Resources, Society, and Ecology: On the Capacity for Human Interaction in Space and Time (Vol. I, Preindustrial Societies). Tommy Carlstein. Urban Geography . David Clark. Spanish City Planning in North America . Dora P. Crouch, Daniel J. Garr, and Axel I. Mundigo. Not On Our Street: Community Attitudes to Mental Health Care . M. J. Dear and S. M. Taylor Unequal growth: Urban and Regional Employment Change in the U.K. Stephen Fothergill and Graham Gudgin. Agricultural Land in an Urban Society . Owen J. Furuseth and John T. Pierce. The Petroleum Industry in Oil-Importing Developing Countries . Fariborz Ghadar. Historical Understanding in Geography, An Idealist Approach . Leonard Guelke. Regional Planning in Europe . R. Hudson and J. R. Lewis, eds. Remote Sensing for Resource Management . Chris J. Johannsen and James L. Sanders, eds. Geography and The State . R. J. Johnston. Texas Graveyards: a Cultural Legacy . Tlrry G. Jordan. The Politics of Location: An Introduction . Andrew Kirby. A Social Geography of the City . David Ley. Energy and the Future . Douglas MacLean and Peter Brown, eds. The Natural Environment of Newfoundland Past and Present . A. G. Macpherson and J. B. Macpherson, eds. Tourism: Economic, Physical and Social Impacts . Alister Mathieson and Geoffrey Wall. Railroads and Land Grant Policy: A Study in Government Intervention . Lloyd J. Mercer. Progress in Rural Geography . Michael Pacione, ed. Progress in Urban Geography . Michael Pacione, ed. Models of Spatial Inequality: Settlement Patterns in Historical Archaeology . Robert Paynter. Natural Hazard Risk Assessment and Public Policy, Anticipating the Unexpected . William J. Petak and Arthur A. Atkisson. The Nature of Geomorphology . Alistair F. Pitty. Regional Conflict and National Policy . Kent A. Price Women and Spatial Change: Learning Resources for Social Science Courses . Arlene C. Rengert and Janice J. Monk, eds. Urban and Regional Analysis for Development Planning . Richard Rhoda. Rivers: Form and Process in Alluvial Channels . Keith Richards. This Remarkable Continent: An Atlas of United States and Canadian Society and Culture . John F. Rooney, Jr., Wilbur Zelinsky, and Dean R. Louder, gen. eds. The Origins of Open-Field Agriculture . Trevor Rowley, ed. Residential Location Determinants of the Older Population . Gundars Rudzitis. Borderland Sourcebook: A Guide to the Literature on Northern Mexico and the American Southwest . Ellwyn R. Stoddard, Richard L. Nostrand, and Jonathan P. West, eds. Arctic and Antarctic . David Sugden. Tall Timbers Ecology and Management Conference, February 22–24, 1979, Proceedings No. 16 . Graphic Communication and Design in Contemporary Cartography (Progress in Contemporary Cartography , Vol. II). D. R. Fraser Taylor, ed. Living with Energy Shortfall: A Future for American Towns and Cities . Jon Van Til. The United States: Habitation of Hope . J. Wreford Watson. Air Photo Interpretation for Archaeologists . D. R. Wilson. Urban and Rural Change in West Germany . Trevor Wild, ed. Population and Resources . Harry Robinson. 相似文献
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《The Professional geographer》1984,36(2):250-283
Book Reviewed in this article: Geography and the Third World. International Seminar, 14–18 May 1980, Kuala Lumpur, Malaysia . Ishmail Ahmad and Jamaluddin Md Jahi, eds. The Growth Dilemma: Residents' Views and Local Population Change in the United States . Mark Baldassare. Sport and Place: A Geography of Sport in England, Scotland & Wales . John Bale. The Deindustrialization of America: Plant Closings, Community Abandonment, and the Dismantling of Basic Industry . Barry Bluestone and Bennett Harrison. Selected Essays 1963–1975: Carl O. Sauer . Bob Callahen, ed. Housing and Planning in the Countryside . G. Clark. Conflict, Politics and the Urban Scene . Kevin R. Cox and R. J. Johnston, eds. Thematic Maps: Their Design and Production . David J. Cuff and Mark T. Mattson. Wine: A Geographic Appreciation . Harm Jan de Blij. USSR in Maps . J. C. Dewdney. Political Geography: A Contemporary Perspective . Ramesh D. Dikshit. Rethinking Human Adaptation . Rada Dyson-Hudson and Michael A. Little, eds. Sacred Sands: The Struggle for Community in the indiana Dunes . J. Ronald Engel. Geography of the Biosphere . A. Furley and Walter W. Newey. Disaster and Reconstruction . Robert Geipel. Glasgow: The Making of a City . Andrew Gibb. Design for Arid Regions . Giden S. Golany, ed. Urbanization and Cancer Mortality: The United States Experience, 1950–1975 . Michael R. Greenberg. Geology in the Nineteenth Century: Changing Views of a Changing World . Mott T. Greene. Colonización y Destrucción de Bosques en Panamá . Stanley Heckadon Moreno and Alberto McKay, eds. Urban Geography: A First Approach . David T. Herbert and Colin J. Thomas. The Visual and Spatial Structure of Landscapes . Tadahiko Higuchi. Climate from Tree Rings . M. K. Hughes, P. M. Kelly, J. R. Pilcher, and V. C. LaMarche, Jr., eds. The structure of Nineteenth Century Cities . James H. Johnson and Colin G. Pooley, eds. The American Planner: Biographies and Recollections . Donald A. Krueckeberg, ed. Urban Land Policy For the 1980s, the Message for State and Local Government . George Lefcoe, ed. Regional Planning: Evolution, Crisis and Prospects . Gill C. Lim, ed. Relevance and Ethics In Geography . Bruce Mitchell and Dianne Draper. China: The Geography of Development and Modernization . Clifton W. Pannell and Laurence J. C. MA. The Urban Retailing System . Robert B. Potter. Hants. Nonconventional Energy Resources . Philip R. Pryde. Caribbean Migrants: Environment and Human Survival on St. Kitts and Nevis . Bonham C. Richardson. Population and Resources . Harry Robinson. East Los Angeles: History of A Barrio . Ricardo Romo. Integrated Impact Assessment . Frederick A. Rossini and Alan L. Porter, eds. Environmental Aesthetics: Essays in Interpretation . Barry Sadler and Allen Carlson, eds. Earthwatch . Charles Sheffield. Field Techniques and Research Methods in Geography . Robert H. Stoddard. Haiti: Land of Poverty . Robert J. Tata. Weathering and Erosion: Sources and Methods in Geography . Stephen T. Trudgill. Once Beneath the Forest. Prehistoric Terracing in the Río Bec Region of the Maya Lowlands . B. L. Turner, II. The Historical Geography of Scotland since 1707 . David Turnock. 相似文献
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《The Professional geographer》2013,65(1):85-89
Reviews of geographic software in this article: DEMO-GRAPHICS: WORLD POPULATIONS AND PROJECTIONS. ESP GAUSS. CEMODEL S. Damus LIMDEP. William H. Greene MICROSTAT 4.1 OTIS PCIPS. (Personal Computer Image Processing System). H.J. Meyers and R. Bernstein. REGRESSION ANALYSIS OF TIME SERIES (RATS) SPSS/PC+ URBAN DATA MANAGEMENT SOFTWARE (UDMS) 相似文献
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《The Professional geographer》1983,35(2):230-260
Book Reviewed in this article: Rabat: Urban Apartheid in Morocco . Janet Abu -Lughod . Marketplaces in a Developing Country: The Case of Western Nigeria . Isaac Ayinde Adalemo . Farming Development and Space: A World Agricultural Geography . Bernd Andreae . Section and Party: A Political Geography of American Presidential Elections, from Andrew Jackson to Ronald Reagan . J. Clark Archer and Peter J. Taylor . Women and Space: Ground Rules and Social Maps . Shirley Ardener , ed. European Progress in Spatial Analysis . R. J. Bennett , ed. The Origins of Academic Geography in the United States . Brian W. Blouet Geographic Perspectives on Global Problems . Ronald Reed Boyce . Seasonal Dimensions to Rural Poverty . Robert Chambers , Richard Longhurst and Arnold Pacey eds. The New Nationalism and the Use of Common Spaces: Issues in Marine Pollution and the Exploitation of Antarctica . Jonathan I. Charney , ed. Communications Tomorrow: The Coming of the Information Society . Edward Cornish , ed. The Design of Suburbia . Arthur Edwards . Explorer on the Northern Plains: Lieutenant Gouverneur K. Warren's Preliminary Report of Explorations in Nebraska and Dakota in the Years 1855–56–57. With an Introduction by Frank N. Schubert . The Changing Climate: Responses of the Natural Flora and Fauna . Michael J. Ford . Essentials of Physical Geography . Robert E. Gabler , Robert J. Sager , Sheila Brazier , and Daniel L. Wise. The Road to Jaramillo . William Glen . Valued Environments . John R. Gold and Jacquelin Burgess , eds. Proximity and Preference: Problems in the Multidimensional Analysis of Large Data Sets . Reginald G. Golledge and John N. Rayner , eds. A Search for Common Ground . Peter Gould and Gunnar Olsson , eds. Geography: Its History and Concepts . Arild Holt -Jensen . A Population Geography . Huw R. Jones . The Human Mosaic: A Thematic Introduction to Cultural Geography, 3rd ed. Terry G. Jordan and Lester Rowntree . Urban Social Geography: An Introduction . Paul Knox . The Anatomy of Job Loss: The How, Why and Where of Employment Decline . Doreen Massey and Richard Meegan . The Information Society as Post-Industial Society . Yoneji Masuda . Map Librarianship, 2nd ed. Harold Nichols . India: Cultural Patterns and Processes . Allen G. Noble and Ashok K. Dutt , eds. The God that Limps: Science and Technology in the Eighties . Colin Norman . Geography: An Introductory Perspective . Robert E. Norris , Keith D. Harries and John D. Vitek . The Politics of Technology Assessment . David M. O'Brien and Donald A. Marchand . Ethnic Segregation in Cities . Ceri Peach , Vaughan Robinson and Susan Smith , eds. Churches and Church Membership in the United States, 1980 . Bernard Quinn , Herman Anderson , Martin Bradley , Paul Goetting and Peggy Shriver . Energy in Australia: Politics and Economics . Hugh Saddler . Development from Above or Below? The Dialectics of Regional Planning in Developing Countries . Walter B. Stóuhr and D. R. Fraser Taylor , eds. Human Impact on the Ecosystem . Joy Tivy and Greg O'Hare . Plants and People: Vegetation Change in North America . Thomas R. Vale . The Mapmakers: The Story of the Great Pioneers in Cartography from Antiquity to the Space Age . John Noble Wilford . 相似文献
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Raanan Katzir 《寒旱区科学》2013,5(6):0767-0768
Desertification is a global phenomenon that affects about two billion people. It occurs in arid zones where the annual precipitation is below 400 mm, partic- ularly in the marginal areas of the world＇s largest deserts. It is a result of water and wind erosion, over- grazing, global warm-ing, improper soil cultivation, and increased pressure ot population growth, and it causes degradation of soil and natural and agricultural vegetation. The direct result is less food for people and livestock, which influences pop- ulation and animal husbandry fluctuations. Despite ef- forts to combat and reduce desertification, the affected areas are annually increasing. 相似文献
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《The Professional geographer》1987,39(1):94-129
Book Reviewed in this article: The Rice Economy of Asia . Randolph Barker and Robert W. Herdt with Beth Rose. Using Microcomputers: A Guidebook for Writers, Teachers, and Researchers in the Social Sciences . Blaine A. Erie—the Lake that Survived . Noel M. Burns. Geology and Society . Donald R. Coates. Caves and Karst of Kentucky . Percy H. Dougherty, ed. Altered Harvest: Agriculture, Genetics, and the Fate of the World's Food Supply . Jack Doyle. The Middle East and North Africa, A Political Geography . Alasdair Drysdale and Gerald H. Blake. Clamor at the Gates. The New American Immigration . Nathan Glazer, ed. Development and the Landowner: An analysis of the British experience . Robin Goodchild and Richard Munton. Discovering Landscape in England and Wales . Andrew Goudie and Rita Gardner. The Modern Plantation in the Third World . Edgar Graham and Ingrid Floering. Social Relations and Spatial Structures . Derek Gregory and John Urry, eds. The World Food Problem 1950–1980 . David Grigg. Costa Rica: A Geographical Interpretation in Historical Perspective . Carolyn Hall. The Urbanization of Capital: Studies in the History and Theory of Capitalist Urbanization . David Harvey Consciousness and the Urban Experience: Studies in the History and Theory of Capitalist Urbanization . David Harvey. Reviving Main Street . Deryck Holdsworth, ed. Rural Roads and Poverty Alleviation . John Howe and Peter Richards, eds. Uneven Development in Southern Europe: Studies of Accumulation, Class, Migration and the State . Ray Hudson and Jim Lewis, eds. Karst Geomorphology . J. N. Jennings. The Geomorphology of North-west England . R. H. Johnson, ed. Climate Impact Assessment: Studies of the Interaction of Climate and Society . Robert Kates, Jesse Ausubel, Mimi Berberian, eds. Public Service Provision and Urban Development . Andrew Kirby, Paul Knox, and Steven Pinch, ed. State and Market: The Politics of the Public and the Private . Jan-Erik Lane, ed. Living Cities . Twentieth Century Fund Task Force on Urban Preservation Policies. World Climatic Systems . John G. Lockwood. Urban Ethnicity in the United States. New Immigrants and Old Minorities . Lionel Maldonaldo and Joan Moore, eds. Culture and Conservation: The Human Dimension in Environmental Planning . Jeffrey A. McNeely and David Pitt, eds. The Andean Past. Land, Societies, and Conflicts . Magnus Mörner. Gaia: An Atlas of Planet Management . Norman Myers, ed. Progress in Industrial Geography . Michael Pacione, ed. Progress in Political Geography . Michael Pacione, ed. Rivers and Landscape . Geoff Petts and Ian Foster. Urbanization and Planning in the 3rd World: Spatial Perceptions and Public Participation . Robert B. Potter. One Island, Two Nations? A Political Geographical Analysis of the National Conflict in Ireland . D. G. Pringle. Circulation in Third World Countries . R. Mansell Prothero and Murray Chapman. The Ozarks Outdoors: A Guide for Fishermen, Hunters, and Tourists . Milton D. Rafferty. Suburban Burglary: A Time and a Place for Everything . George Rengert and John Wasilchick. Geomorphology and Soils . K.S. Richards, R.R. Arnett, and S. Ellis, eds. The Homes and Homeless of Post-War Britain . Frederick Shaw. Indochinese Refugees in America . Paul J. Strand and Woodrow Jones, Jr. Wild Horses and Sacred Cows . Richard Symanski. Forever Wild: Environmental Aesthetics and the Adirondack Forest Preserve . Philip G. Terrie. The Regional Economic Impact of Technological Change . A.T. Thwaites and R.P. Oakey, eds. The Good Life . Yi-Fu Tuan. 相似文献
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《The Professional geographer》1987,39(1):85-94
Reviews of geographic software in this article: DEMO-GRAPHICS: WORLD POPULATIONS AND PROJECTIONS. ESP GAUSS. CEMODEL S. Damus LIMDEP. William H. Greene MICROSTAT 4.1 OTIS PCIPS. (Personal Computer Image Processing System) . H.J. Meyers and R. Bernstein. REGRESSION ANALYSIS OF TIME SERIES (RATS) SPSS/PC+ URBAN DATA MANAGEMENT SOFTWARE (UDMS) 相似文献
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《寒旱区科学》2014,(4):I0002-I0003
1. Aims and scope
Sciences in Cold and Arid Regions （SCAR） is a bimonthly journal that publishes in English the latest research achievements in processes and the pattems of the Earth surface system in cold and arid regions. Researches in cold regions emphasize particularly on the cold-region-characterized physical, 相似文献
Sciences in Cold and Arid Regions （SCAR） is a bimonthly journal that publishes in English the latest research achievements in processes and the pattems of the Earth surface system in cold and arid regions. Researches in cold regions emphasize particularly on the cold-region-characterized physical, 相似文献
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