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71.
南沙群岛永暑礁7个表层礁坪原生块状珊瑚的高精度TIMS U-Th和12个常规^14C测年结果表明,永暑礁表层礁坪形成于现代,与钻探研究结果吻合。全新世永暑礁系从约7300aBP开始,以现代礁坪面以下17m左右的晚更新世礁灰岩为基底连续发育至今,因此,与南海周边地区的珊瑚礁不同,南沙群岛珊瑚礁的表层块状珊瑚不能够提供全新世高海平面的证据。由于现代珊瑚礁的堆积速率大于地壳沉降速率,可能会形成更多的灰沙洲或灰沙岛。 相似文献
72.
应用锆石TIMSU-Pb测年获得西昆仑山奇台达坂花岗岩年龄为(202.2士3.4)Ma(MSWD=8.65);利用不同海拔高度获得磷灰石裂变径迹测定年龄为24.8~14.0Ma。通过裂变径迹热史模拟,并结合前人40Ar-39Ar测年数据,得出西昆仑山奇台达坂花岗岩就位以来,至少经历了三快二慢的冷却降温(隆升剥蚀)过程:即202.2~195.6Ma、26~15Ma和5Ma以来3个阶段的快速降温(隆升剥蚀),195.6~26Ma和15~5Ma2个阶段的缓慢冷却降温(隆升剥蚀)。西昆仑山地壳最上部约3km的快速去顶作用主要发生于26~15Ma和5Ma以来,它是印度板块向欧亚板块碰撞的结果。 相似文献
73.
This brief contribution presents new boron isotopic data for a set of proposed borosilicate reference minerals, most of which are described in the companion paper by Dyar et al.2001 . The results for a variety of minerals (tourmalines, danburite, prismatine, serendibite, ferroaxinite and a Li mica) show that it is generally possible to reproduce the 11 B/10 B ratio within ± 0.5 per mil with replicate chemistry and mass spectrometry over long time spans. Because the accuracy of boron isotopic analysis is commonly determined by reference to secondary standards, it is suggested that some of the samples used in this study be adopted for interlaboratory comparisons and for quality control on boron isotopic analyses produced by a variety of analytical methods. 相似文献
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75.
不平衡铀系定年的新技术突破——高精度、高灵敏度238U-234U-230Th同位素质谱测定和应用 总被引:3,自引:0,他引:3
80年代中期发展起来的高精度、高灵敏度不平衡铀系热电离质谱定年新技术是同位素定年技术的一次革命性突破,并已在古气候、古环境、古海洋、考古学以及近代火山—岩浆作用研究中取得了一系列重要成果,本文介绍了这方面的研究进展。这一新技术已引起越来越广泛的重视,显示出巨大的应用前景。尽快开展不平衡铀系热电离质谱定年技术的应用,对提高我国的高分辩率第四纪年代学分析技术和应用研究水平有重要意义。 相似文献
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77.
Accurate Isotopic and Concentration Analyses of Small Amounts of Pb Using Isotope Dilution Coupled with the Double Spike Technique 总被引:1,自引:0,他引:1
Takeshi Kuritani Tomohiro Usui Tetsuya Yokoyama Eizo Nakamura 《Geostandards and Geoanalytical Research》2006,30(3):209-220
A new method has been developed for the simultaneous determination of Pb abundance and Pb isotopic composition with high precision and accuracy for small test portion masses by thermal ionisation mass spectrometry. In this method, a 205 pb-204 pb double spike is added to samples prior to the chemical separation of Pb, and the isotopic composition of the spike-sample mixture is determined rigorously by the double spike technique using a 207 Pb-204 Pb spike. The isotopic composition and concentration of Pb in the sample are then obtained by utilising the principle of isotope dilution. Using this technique, replicate determinations of Pb from NIST SRM 981 and GSJ JP-1 (peridotite; 0.07 μg g−1 Pb) were performed. The measured concentration and isotopic data were identical, within uncertainty, to published data or to data that were determined independently in this study. The application of this method to U-Pb dating and the determination of the "initial" Pb isotopic composition was also tested. Lead isotopic compositions and the concentrations of Pb, Th and U were determined for a single batch of samples, through the addition of 205 pb-204 pb, 230 Th and 235 U spikes to samples prior to chemical separation. Also in these experiments, we confirmed that this routine gives accurate data for Pb, Th and U concentrations and Pb isotopic compositions. 相似文献
78.
The double‐spike approach for correction of instrumental mass bias in mass spectrometry data is well established. However, there is very little consistency within the scientific community in terms of double‐spike data reduction. Double‐spike solutions require computer calculation, using either geometric or algebraic approaches, and are often performed using spreadsheet calculations that vary from group to group and between isotope systems. Here, we present IsoSpike, a generalised computer procedure for the processing of double‐spike mass spectrometry data, built as an add‐on for the Iolite data‐reduction package ( www.iolite.org.au ). Use of this software permits visualisation of mass spectrometry data in a time window, and rigorous treatment and screening of data. Additionally, IsoSpike uses an integration‐by‐integration approach where the double‐spike calculations are performed on every integration within an analysis, providing straightforward quantification of uncertainties on double‐spike‐corrected isotope ratios. The advantages of this approach over traditional methods are discussed here. Platinum stable isotope data are presented as an example data set, although the procedure is applicable to any double‐spike system. IsoSpike is freely available from www.isospike.org . 相似文献