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1.
通过实验研究,笔者确定了激光烧蚀等离子体质谱法直接测定探针片中锆石、磷灰石U-Pb同位素年龄的流程,包括样品制备、矿物成因分析、仪器测试条件和测试过程。该方法最大的优势在于,可在探针片上确定测年矿物的共生组合及地质意义,将测得的年龄与特定地质事件,如变质事件、热液事件等相联系,对年龄数据给予合理的地质解释。利用此方法对一些岩石中的锆石、磷灰石在探针片上进行了测试,与用传统单矿物制靶方法测试的结果在误差范围内一致,表明在探针片上进行含铀矿物原地原位U-Pb测年是完全可行的。  相似文献   

2.
内蒙古凉城地区的石榴石二长花岗岩20世纪70年代初1∶20万区域地质调查时归入太古代早期侵入岩(γ11(2)),岩石定名为中粗粒似斑状花岗岩,称蛮汗山岩体。1∶25万区调将其划分为弱片麻状石榴二长花岗岩、弱片麻状变斑状含黑云石榴二长花岗岩等不同地质单元。为进一步研究该石榴石花岗岩的形成时代,本文对弱片麻状变斑状含黑云石榴二长花岗岩中锆石进行了LA-MC-ICP-MS U-Pb测年研究,获得其U-Pb年龄值(1933.3±9.8)Ma,为石榴石二长花岗岩原岩的形成年龄。岩石化学、地球化学分析表明该石榴石二长花岗岩为新太古界孔兹岩系部分熔融的产物,为强过铝S型花岗岩。结合已有的年龄数据推断,1900~2000 Ma(古元古代中期)华北克拉通曾发生过大规模的构造岩浆热事件。  相似文献   

3.
锆石U-Pb同位素测年原理及应用   总被引:5,自引:0,他引:5  
U-Pb法是国内目前最重要的同位素测年方法.通过分析锆石U-Pb同位素测年的基本原理、不同成因锆石的特征及常用测试技术,综述了该方法在母岩形成年龄、地质演化事件、碎屑沉积物来源、沉积时代等方面的应用.指出锆石微区U-Pb年龄测定技术的引进对我国的地质科学研究起到了巨大的推动作用,并且其应用领域仍在进一步扩展.  相似文献   

4.
内蒙古大青山地区哈拉合少岩体特征及成因   总被引:4,自引:0,他引:4  
通过对大青山哈拉合少岩体基本地质特征研究,包括岩石矿物学特征、岩石化学和地球化学特征、同位素年代分析等,对岩体形成时代和形成构造环境有了一些认识:锆石U-Pb等时线测年分析结果表明,206Pb/238U表面年龄计权重平均值为261.1 Ma±0.5 Ma,代表哈拉合少岩体侵位时代;岩石化学分析结果和岩石学特征表明,该岩体为I型与S型混合成因花岗岩,主要由壳源物质重熔形成。根据地球化学分析结果,结合形成的构造背景,认为该岩体是在西伯利亚板块向南俯冲与华北板块北缘碰撞晚期的应力松驰阶段形成的,属造山期同碰撞花岗岩。  相似文献   

5.
地衣测年是20世纪50年代提出并逐渐发展起来的一种测年方法,已被应用于冰川地貌、古滑坡、古地震等地质事件的测年中,尤其在侵蚀速率较大、沉积物难以保存的地区具有独特的优势。虽然地衣测年仍不完善、在具体应用中存在一些问题、国内外学者对该方法也有争议,但随着研究的深入以及相关问题的解决,其对于全新世以来地质事件的测年具有广泛的应用前景。本文整理了地衣测年的发展历史和存在问题,并展望了地衣测年的未来发展方向。  相似文献   

6.
40Ar-39Ar同位素测年方法及其应用   总被引:1,自引:0,他引:1  
刘艳红  刘永江 《世界地质》2004,23(3):245-251
^40Ar—^39Ar测年法的出现,为同位素地质年代学开辟了一个新的领域;但过剩氩的存在、年龄谱的分析方法,又制约着地质事件的年龄解释。在介绍该方法的原理、校正、年龄谱的分析和应用及过剩氩问题等方面内容的基础上,结合阿尔金断裂研究实例,对该断裂中的新生矿物进行了^40Ar-^39Ar测年,进而确定了阿尔金断裂走滑活动的年龄。  相似文献   

7.
通过对内蒙古中部新太古代似斑状含榴石花岗岩进行岩相学及岩石地球化学方面的研究,并与黑云片麻岩进行岩石地球化学特征对比,发现两者在宏观地质特征与岩石地球化学特征上具有紧密的继承性,因此认为该花岗岩为新太古代区域变质岩在高级变质作用条件下经历原地经深熔作用、混合岩化作用所形成。  相似文献   

8.
含U副矿物的地质年代学研究综述   总被引:11,自引:0,他引:11  
简要介绍了目前已经发展起来的各种微区原位测年技术的特点和研究矿物内部结构的技术。微区原位测年技术有离子探针、激光探针同位素测年技术、电子探针、质子探针和X射线荧光探针Th U 全Pb化学等时线年龄技术。综述了锆石、独居石、磷钇矿、榍石、磷灰石、金红石、斜锆石等含U副矿物在U Th Pb年代学研究方面的应用及进展,并介绍了锆石、独居石、磷钇矿、榍石等具有多世代性的矿物的成因判别方法,概括了用于岩浆过程、变质过程和沉积过程年代学研究常用的含U副矿物,及其相应的年代学研究需要注意及可解决的地质问题和适用性。总结了岩石年代学研究的主要进展和提取贮存在副矿物中有价值的年龄和成因信息需要解决的问题。  相似文献   

9.
根据地表暴露岩石或埋藏物中宇宙成因核素浓度可计算样品的暴露年龄或埋藏年龄,从而估算出研究区域的侵蚀速率和抬升速率等重要地质信息,该方法现已成为晚新生代地质和地貌变化研究的重要手段。概述了近5年来国内外宇宙成因核素在地质年代学研究中的最新进展,主要包括以下几个方面:①10Be研究进展,26Al/10Be双核素测年计算模型的改进和完善,以及21Ne的加入对26Al-10Be测年方法的拓展;②宇宙成因36Cl在碳酸盐岩中的研究和应用进展;③53Mn、41Ca等新核素的研究和应用;④宇宙成因核素测年技术在国内的应用进展。最后,分析了宇宙成因核素测年存在的主要问题及下一步重点研究方向。  相似文献   

10.
指出了《冀北兰城子-蔡家营子-带红旗营子群的Sm-Nd同位素年龄及其地质意义》一文中有违地质学原理和同位素测年方法及解释方面的不当之处。在列举变质作用中流体导致岩石同位素体系再次均一化实例;讨论测年数据的地质意义与地质关系的相互检验和不同测年方法的合理使用问题;深入分析研究红旗营子群内Sm-Nd测年样品的特征之后,认为宜将红旗红旗营子群的生成年代定为新太古代。  相似文献   

11.
Proton microprobe for chemical dating of monazite   总被引:1,自引:1,他引:0  
Although quantitative chemical analysis by proton microprobe has become an established technique, it has been rarely applied to problems in the earth sciences. The method, having lower detection limit (better than 10 ppm for U, Th and Pb) and higher spatial resolution than electron microprobe (typically 1 μm vs 3 μm), can be successfully used in geology. Here, we present a procedure for the chemical dating of monazite, (REE)PO4, by proton microprobe. The procedure is compared with electron probe microanalysis technique (EPMA).  相似文献   

12.
以化学法独居石电子探针定年的原理以及前人改良过的年龄计算公式为基础,利用全微分和最大误差原理,确定了年龄误差计算新方法。并用Visual C语言在Windows平台下编制出了计算年龄和年龄误差的计算机程序。运用此程序对前人公开发表的分析资料和计算的年龄以及年龄误差数据进行了重新计算,验证了给出的误差公式的可靠性。同时,利用JXA—8100电子探针仪对新疆东天山变质沉积岩的两个样品(KM2127—5,DK2107—2)中的独居石进行了电子探针微区U—Th—Pb成分分析。结果表明,样品DK2107—2记录了两期变质作用,峰期年龄分别是341.0±3.9Ma和255.2±3.3Ma,其中最主要的变质峰期年龄为341.0±3.9Ma,该期的矿物组合为Ky+St+Bt+Pl+Q+/-Or;而255.2±3.3Ma和样品KM2127-5记录的变质峰期年龄262.3±4.4Ma为次要变质峰期年龄,该期矿物组合是Cord+Bt+Pl+Or+Q。分析结果与前人用^40Ar—^39Ar法得到的结果相吻合,表明独居石电子探针定年技术是一种可靠有效的测年方法。  相似文献   

13.
The question of the Yangtze’s origins has been extensively researched by geologists and geomorphologists for more than a century, and a widely-accepted answer is still pending. Evidence of river piracy, diversion and incision in the upper river segment from Shigu town in Yunnan Province to Yichang City has been used to reconstruct the history of the Yangtze drainage system, and constrain the timing of the upper Yangtze diversion from south flowing to east, debouching into the East China Sea. There is much diversity in fluvial deposits and landforms even over small spatio-temporal scales in tectonic highly active regions. They are also liable to latter reworking by external forces, making their paleo-geographical interpretation a more complex and controversial matter. Based on evidence from fluvial strata and landforms, various hypotheses have been proposed with considerable discrepancies for the timing of the Jinsha River diversion from the south flowing into the east, and the timing of the upper Yangtze channeling through the Three Gorges area. The Yangtze was controversially assumed to be: (1) a very old river in existence since the Cretaceous and earlier, (2) a very young river that came into being only during the past several hundred thousand years, or (3) any age in between these two extremes. Techniques in microprobe dating of single crystalline grains have greatly improved, and they have been widely and successfully used in provenance studies, drainage evolution reconstruction, and tectonic history restoration through dating detrital zircon/monazite grains from the onshore/offshore deposits. The timing of the Yangtze formation was estimated at ca. 2.58 Ma based on analyses of time-series variation of EMP (electron microprobe) monazite ages in the late Cenozoic strata of the Yangtze delta. By revisiting fluvial deposits and landforms in the upper Yangtze drainage basin, some references also state the initiation time of the Yangtze at between the late Pliocene and early Pleistocene. This indicates that microprobe dating of single detrital mineral grains is an effective tool to study sedimentary provenance and reconstruct the evolution history of large rivers, like the Yangtze. Laser ablation-ICPMS, a newly-developed microprobe dating technique characterized by minimal sample preparation, low cost and high throughput, and high precision, makes it possible to date large volumes of single detrital mineral grains for provenance studies. Its application is expected to increase the precision of the timing of the Yangtze formation. __________ Translated from Marine Geology and Quaternary Geology, 2007, 27(2): 121–131 [译自: 海洋地质与第四纪地质]  相似文献   

14.
Laser microprobe (U-Th)/He geochronology   总被引:3,自引:0,他引:3  
A new analytical method had been developed to enable high-spatial-resolution (U-Th)/He dating of accessory minerals. It involves the use of a focused ArF excimer to ablate pits in a polished grain surface, with the evolved gases spiked for isotope-dilution measurement of radiogenic 4He. These data are converted to concentrations by precise measurement of each pit using an optical interferometric microscope. U, Th, and Sm concentration measurements are made using one of several alternative microanalytical techniques (e.g., wavelength-dispersive electron microprobe analysis or laser-ablation, inductively coupled plasma mass spectrometry). By way of illustration, we present both conventional and laser microprobe (U-Th)/He dating results for a Brazilian monazite sample. Laser microprobe data (28 measurements on two crystal fragments) yield a weighted mean (U-Th)/He date of 455.3 ± 3.7 Ma (2SE). This result is statistically indistinguishable from the mean conventional (U-Th)/He date for three separate grain fragments: 449.6 ± 9.8 Ma (2SE). The agreement of conventional and laser ablation dates should encourage a wide variety of applications of the technique, including: (1) detrital mineral dating for provenance and unroofing studies; (2) the dating of broken, included, highly zoned, or irregular grains which are not easily corrected for α-ejection; and (3) measuring 4He loss profiles that can be inverted to determine cooling histories.  相似文献   

15.
电子探针化学测年技术及其在地学中的应用   总被引:2,自引:0,他引:2  
电子探针主要应用于固体无机材料的微区化学成分定量测定和表面形貌研究。近十年来电子探针化学测年技术发展迅速,并取得了丰富的研究成果。本文在简单介绍该技术发展历程后,进一步详细介绍该技术的基本原理、样品制备与分析、年龄计算方法等内容,最后讨论了该技术的优缺点,同时指出电子探针测年技术在地学中的具有广泛的应用前景。  相似文献   

16.
Chemical Th–U–total Pb (CHIME) dating of monazite by electron probe microanalyzer (EPMA) and proton microprobe (PIXE) was carried out on felsic granulites from Stary Gierałtów, Poland, which represent part of the Orlica-Śnieżnik Dome in the NE Bohemian Massif. Analyzed monazite is characterized by mosaic zoning rather than simple core-to-rim growth, and strontium contents of up to 750ppm. An isochron age of 347 ± 13Ma represents timing of amphibolite-facies metamorphism, in agreement with previously published estimates.  相似文献   

17.
The metamorphic evolution of micaschists in the north‐eastern part of the Saxothuringian Domain in the Central European Variscides is characterized by the early high‐pressure M1 assemblage with chloritoid in cores of large garnet porphyroblasts and a Grt–Chl–Phe–Qtz ± Pg M2 assemblage in the matrix. Minerals of the M1–M2 stage were overprinted by the low‐pressure M3 assemblage Ab–Chl–Ms–Qtz ± Ep. Samples with the best‐preserved M1–M2 mineralogy mostly appear in domains dominated by the earlier D1 deformation phase and are only weakly affected by subsequent D2 overprint. Thermodynamic modelling suggests that mineral assemblages record peak‐pressure conditions of ≥18–19 kbar at 460–520 °C (M1) followed by isothermal decompression 10.5–13.5 kbar (M2) and final decompression to <8.5 kbar and <480 °C (M3). The calculated peak P–T conditions indicate a high‐pressure/low‐temperature apparent thermal gradient of ~7–7.5 °C km?1. Laser ablation inductively coupled plasma mass spectrometry isotopic dating and electron microprobe chemical dating of monazite from the M1–M2 mineral assemblages give ages of 330 ± 10 and 328 ± 6 Ma, respectively, which are interpreted as the timing of a peak pressure to early decompression stage. The observed metamorphic record and timing of metamorphism in the studied metapelites show striking similarities with the evolution of the central and south‐western parts of the Saxothuringian Domain and suggest a common tectonic evolution along the entire eastern flank of the Saxothuringian Domain during the Devonian–Carboniferous periods.  相似文献   

18.
《Gondwana Research》2009,15(4):675-685
Chemical Th–U–total Pb (CHIME) dating of monazite by electron probe microanalyzer (EPMA) and proton microprobe (PIXE) was carried out on felsic granulites from Stary Gierałtów, Poland, which represent part of the Orlica-Śnieżnik Dome in the NE Bohemian Massif. Analyzed monazite is characterized by mosaic zoning rather than simple core-to-rim growth, and strontium contents of up to 750ppm. An isochron age of 347 ± 13Ma represents timing of amphibolite-facies metamorphism, in agreement with previously published estimates.  相似文献   

19.
对电子探针U-Th-Pb定年方法的基本原理、样品的制备和分析、年龄计算方法和误差分析进行了较系统的介绍,并对电子探针定年在构造分析中的应用前景作了展望.电子探针定年方法适用于经历了包括流体作用和重结晶作用变质事件的单一和复杂成因的独居石、锆石矿物,不仅是一个评价变质和变形时间的有效普查工具,而且它的原位性和高分辨能够用来制约构造变形和变质作用过程的绝对时间和速率,在构造分析中具有广阔的应用前景.  相似文献   

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