RP-HPLC法同时测定翅碱蓬中四种黄酮化合物的含量     

郭丽霞  宁寰宇  曹苇  李慧  孔亮  谭成玉 《海洋科学》2020,44(4):111-115

建立RP-HPLC(反相高效液相色谱法)同时测定翅碱蓬中四种黄酮化合物-芸香苷、槲皮素3-β-D-葡萄糖苷、水仙苷和槲皮素的含量。采用Kromasil C18色谱柱(4.6 mm×250 mm,5μm),检测波长为361nm,柱温为30℃,流动相为甲醇-0.4%冰乙酸(55︰45),流速1.0mL/min,四种黄酮类化合物得到很好的分离。芸香苷、槲皮素3-β-D-葡萄糖苷、水仙苷和槲皮素浓度均为0.001~0.01 mg/mL范围内呈现良好线性关系,相关系数R2在0.9990~0.9996,加标回收率(n=3)范围为82.39%~99.03%。该方法简单、快速、高效,可以用于翅碱蓬中四种黄酮化合物的含量分析。  相似文献   

碟形越浪式波能发电装置的三维数值模拟     

刘大方  刘臻  张国梁 《海岸工程》2020,39(4):237-245

基于计算流体力学软件的三维数值模拟技术,分析了碟形越浪式波能发电装置的越浪性能,通过构建基于水气两相VOF(Volume of Fluid)模型的三维数值波浪水槽对该装置进行三维数值模拟研究,数值计算结果与物理试验结果相互对比验证较为吻合,验证了所构建的三维数值波浪水槽的可靠性,通过考察装置的坡度、导流叶片个数、干舷高度对越浪性能的影响确定装置的最优结构参数。结果表明,在装置的斜坡面边缘增加回流板可减少波浪的反射,提高装置的越浪性能。在数值模拟中将装置的斜坡面边缘处安装回流板对碟形越浪式波能发电装置参数进行优化,通过分析回流板的长度对装置越浪性能的影响来探索最优回流板长度。  相似文献   

“数字海底”--海底数据集成管理与可视化研究     

肖鹏  王悦东  李安龙 《海洋信息》2020,35(1):40-45,51

针对目前"数字海底"建设中存在海底调查数据集成管理与三维可视化表达不足等问题,本文采用GIS技术,以黄河水下三角洲埕北海域为研究对象,利用地理空间数据集成理论与三维建模方法,建立了埕北海域三维海底空间数据库,实现了研究区域地形数据、地层数据、钻孔数据、表层沉积物数据的有效组织管理与可视化,并在此基础上,采用ArcGIS Engine 10.0,结合.NET平台,在Visual Studio 2010开发环境下,利用C#语言进行了二次开发,实现了基于C/S (Client/Server)架构的三维海底虚拟仿真系统的开发,设计了一套面向埕北海域的三维海底虚拟仿真原型系统。  相似文献   

2013—2019年度海洋科学技术奖计量统计及其科研合作网络分析          下载免费PDF全文

赵晓龙  李保石  王泉斌 《海洋开发与管理》2020,37(11):19-27

文章基于2013—2019年度海洋科学技术奖，运用计量统计、社会网络分析等研究方法，探究海洋科学技术奖获奖成果计量特征、学科分布、获奖机构及其科研合作关系等，直观揭示海洋科学技术奖所构成的科研合作范式、科研合作网络结构等，以期为海洋科研管理、科技创新和学科建设等提供科学参考。研究表明：整体上，海洋科学技术奖获奖成果呈逐年递增趋势，一等奖与二等奖的获奖等级比值呈下降趋势；学科划分上，获奖成果主要隶属于“海洋科学”学科，又以海洋生物学、海洋装备与设备、海洋化学和物理海洋学为主体；获奖机构方面，海洋科学技术奖已奖励包括中国海洋大学和中国科学院海洋研究所等涉海类高校和科研院所在内的各类海洋科技创新主体285家，分布在山东、浙江、广东、上海、北京、江苏等19个省（市、自治区）；科研合作方面，海洋科学技术奖获奖核心机构所构建的科研合作关系紧密，以自然资源部第二海洋研究所的中心度最高，中国海洋大学的中间中心度最高，其控制该科研合作网络中其他机构之间沟通交流的力度最大。  相似文献   

Effect of different registration methods on precision of orientation based on RTK registration/georeferencing mode     

Shengming Hu  Zhijian Chen  Chenghui Wan  Chun Tang  Wen Xiong 《Marine Georesources & Geotechnology》2020,38(4):385-392

Abstract

Compared with traditional methods, the three-dimensional laser-scanning (3D-LS) technique can efficiently acquire many high-quality geometric properties of rock discontinuities. In practice, engineers usually prefer to simplify the processing by using single-station point data and roughly orienting owing to the complexity of registration/georeferencing multi-station point data. However, prior published studies have paid little attention to the accuracy and reliability when determining discontinuity orientations using 3D-LS. We propose a reliable and accurate method with robust on-site applicability. As part of an ongoing effort, we are evaluating the precision of the commonly used coarse registration method and the fine registration method, and promoted the optimized coarse- and fine-registration methods and evaluated their precision. It is found that: (1) the common and the optimized registration method can meet our project’s engineering requirements, and the optimized registration method improved accuracy in the dip direction by approximately 1°; (2) fine registration using an iterative closest point (ICP) algorithm can correct both dip direction and dip angle; and (3) the orientation is of high precision with commonly used coarse and fine registration, whereas the optimization effect to correct the orientation is slightly limited.  相似文献   

NaHSO3对两种微藻生长及胞外多糖和藻胆蛋白含量的影响     

梁英  闫译允  黄徐林  田传远  胡乃霞  王帅 《中国海洋大学学报(自然科学版)》2020,(1):21-29

本文研究了0.25~3 mmol/L浓度的NaHSO3对紫球藻(Porphyridium violaceum)和0.06~0.96 mmol/L浓度的NaHSO3对蓝隐藻(Chroomonas placoidea)的叶绿素荧光参数(PSII最大光能转化效率Fv/Fm、相对电子传递速率rETR、光化学淬灭qP、非光化学淬灭NPQ)、细胞密度、干重、胞外多糖和藻胆蛋白含量的影响。研究表明,较低浓度的NaHSO3对紫球藻和蓝隐藻的生长及活性物质积累有促进作用,2种微藻进行生长和活性物质积累的最适NaHSO3浓度分别为0.5和0.12 mmol/L,此条件下,实验结束时,2种微藻的Fv/Fm、rETR、qP、细胞密度、干重、胞外多糖和藻胆蛋白含量均达到最大值,显著高于对照组。其中,紫球藻的最终细胞密度、干重、胞外多糖和藻胆蛋白含量分别比对照组增加了36.0%、19.1%、71.8%和69.0%。蓝隐藻的上述参数在NaHSO3浓度为0.12 mmol/L时则比对照组增加了60.8%、45.4%、60.0%和53.1%。另一方面,NaHSO3浓度为2~3 mmol/L时显著抑制紫球藻生长及活性物质积累,NaHSO3浓度为0.48~0.96 mmol/L则不利于蓝隐藻生长及活性物质积累。研究结果表明,适合紫球藻和蓝隐藻生长及胞外多糖和藻胆蛋白积累的最佳NaHSO3浓度分别为0.5和0.12 mmol/L,该研究为2种微藻的开发利用提供了理论依据。  相似文献   

厚碳酸盐岩覆盖区RVSP三维地震勘探应用效果分析     

胡小鹏 《山东国土资源》2020,36(5):38-43

该文以中国南方一厚碳酸盐岩覆盖区的RVSP三维地震勘探实例,对RVSP三维地震勘探观测系统和数据采集参数的确定、地面等效处理和波场分离等关键处理技术及地质效果进行了阐述和分析,说明了RVSP在克服表浅层复杂地质条件及环境条件对资料的影响及提高地震资料的分辨率有其特定的优势,同时也提出了RVSP三维地震在采集和处理过程中的难点。  相似文献   

频率域海洋可控源电磁垂直各向异性三维反演   总被引：1，自引：0，他引：1       下载免费PDF全文

彭荣华  胡祥云  李建慧  刘亚军 《地球物理学报》2019,62(6):2165-2175

地层宏观电性各向异性会对可控源电磁响应产生重要影响.由于海底地层电性结构常表现为电导率各向异性，若仅对海洋可控源电磁（MCSEM）数据进行常规各向同性反演，有可能无法获得准确的反演解释结果，从而削弱MCSEM技术的可靠性.本文实现了电导率垂直各向异性（VTI）条件下频率域海洋可控源电磁数据三维反演算法.其中，三维正演采用基于二次场控制方程的交错网格有限体积法，并利用直接矩阵分解技术来求解离散所得的大型线性方程组，有利于快速计算多场源的响应.反演采用具有近似二次收敛性的高斯牛顿算法对目标函数进行最优化.最后，对具有VTI电性各向异性特征的盐丘构造模型的MCSEM合成数据分别进行了电导率各向同性和垂直各向异性三维反演，结果表明：各向同性三维反演算法无法对受VTI介质影响的MCSEM数据进行正确的反演解释，而垂直各向异性三维反演能够获得更为可靠的地下电阻率结构和异常体分布，展现出对海底电性各向异性结构更为优良的反演解释能力.  相似文献   

APPLYING 3D INVERSION OF SINGLE-PROFILE MAGNETOTELLURIC DATA TO IDENTIFY THE SHADE AND YUNONGXI FAULTS          下载免费PDF全文

JIANG Feng  CHEN Xiao-bin  DONG Ze-yi  CUI Teng-fa  LIU Zhong-yin  WANG Pei-jie 《地震地质》2019,41(6):1444-1463

Many synthetic model studies suggested that the best way to obtain good 3D interpretation results is to distribute the MT sites at a 2D grid array with regular site spacing over the target area. However, MT 3D inversion was very difficult about 10 years ago. A lot of MT data were collected along one profile and then interpreted with 2D inversion. How to apply the state-of-the-art 3D inversion technique to interpret the accumulated mass MT profiles data is an important topic. Some studies on 3D inversion of measured MT profile data suggested that 2D inversions usually had higher resolution for the subsurface than 3D inversions. Meanwhile, they often made their interpretation based on 2D inversion results, and 3D inversion results were only used to evaluate whether the overall resistivity structures were correct. Some researchers thought that 3D inversions could not resolute the local structure well, while 2D inversion results could agree with the surface geologic features much well and interpret the geologic structures easily. But in the present paper, we find that the result of 3D inversion is better than that of 2D inversion in identifying the location of the two local faults, the Shade Fault(SDF)and the Yunongxi Fault(YNXF), and the deep structures. In this paper, we first studied the electrical structure of SDF and YNXF based on a measured magnetotelluric(MT) profile data. Besides, from the point of identifying active faults, we compared the capacity of identifying deep existing faults between 2D inversion models and 3D models with different inversion parameters. The results show that both 2D and 3D inversion of the single-profile data could obtain reasonable and reliable electrical structures on a regional scale. Combining 2D and 3D models, and according to our present data, we find that both SDF and YNXF probably have cut completely the high resistivity layer in the upper crust and extended to the high conductivity layer in the middle crust. In terms of the deep geometry of the faults, at the profile's location, the SDF dips nearly vertically or dips southeast with high dip angle, and the YNXF dips southeast at depth. In addition, according to the results from our measured MT profile, we find that the 3D inversion of single-profile MT data has the capacity of identifying the location and deep geometry of local faults under present computing ability. Finally, this research suggests that appropriate cell size and reasonable smoothing parameters are important factors for the 3D inversion of single-profile MT data, more specifically, too coarse meshes or too large smoothing parameters on horizontal direction of 3D inversion may result in low resolution of 3D inversions that cannot identify the structure of faults. While, for vertical mesh size and data error thresholds, they have limited effect on identifying shallow tectonics as long as their changes are within a reasonable range. 3D inversion results also indicate that, to some extent, adding tippers to the 3D inversion of a MT profile can improve the model's constraint on the deep geometry of the outcropped faults.  相似文献   

CTS-1E、CMG-3ESPC-120型地震计工作参数对比分析     

段绍鑫  乌尼尔  李晓东  张森  张小飞 《地震地磁观测与研究》2019,40(4):120-124

CTS-1E型、CMG-3ESPC-120型地震计安装架设在库尔勒地震台小泉沟观测点同一台基上，均使用EDAS-24GN型数据采集器进行实时数据采集，对比分析观测数据波形特征、地动噪声功率谱及动态范围等，明确2套地震计在实际观测中的性能差异，以便为地震监测数据分析及相关研究提供参考。  相似文献